Peretinoin_LCMS_20299_MedChemExpress
=====================================================================Acq. Operator : Su Xiao Ying(LCMS-02) Seq. Line : 56
Acq. Instrument : HY-LCMS-02 Location : P1-A-08Injection Date : 5/5/2016 2:32:07 PM Inj : 1
Inj Volume : 3.000 μl Different Inj Volume from Sample Entry Actual Inj Volume : 10.000 μl
Acq. Method : D:\AGLIENT 1260\DATA\20160505\20160505 2016-05-05 09-03-15\100-1000MS+3MIN- 1.5_(0.02%FA).M
Last changed : 5/5/2016 9:03:15 AM by Su Xiao Ying(LCMS-02)
Analysis Method : D:\AGLIENT 1260\DATA\20160505\20160505 2016-05-05 09-03-15\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)
Last changed : 5/5/2016 2:38:47 PM by Su Xiao Ying(LCMS-02) (modified after loading)
M ethod Info : HY-365_5HO1RS,M,A-RP-108，210nm,23min
Catalog No : HY-100008 Batch#20299 A-RP-134
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2
2.53mAU 0
200400600800 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT...0\DATA\20160505\20160505 2016-05-05 09-03-15\BIZ2016-505-WJ4-2.D)
2.459
2.855
2.976
3.172
===================================================================== Area Percent Report =====================================================================
Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000
Do not use Multiplier & Dilution Factor with ISTDs
Signal 1: DAD1 B, Sig=214,4 Ref=off
Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------| 1 2.459 MM 0.1491 14.04795 1.57068 0.4762 2 2.855 MF 0.0535 2897.18506 902.07666 98.2124 3 2.976 FM 0.0710 34.38771 8.07468 1.1657 4 3.172 MM 0.0751 4.29687 9.53773e-1 0.1457
Totals : 2949.91759 912.67580
===================================================================== *** End of Report ***
=====================================================================Acq. Operator : Su Xiao Ying(LCMS-02) Seq. Line : 56
Acq. Instrument : HY-LCMS-02 Location : P1-A-08Injection Date : 5/5/2016 2:32:07 PM Inj : 1
Inj Volume : 3.000 μl Different Inj Volume from Sample Entry Actual Inj Volume : 10.000 μl
Method : D:\AGLIENT 1260\DATA\20160505\20160505 2016-05-05 09-03-15\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)
Last changed : 5/5/2016 9:03:15 AM by Su Xiao Ying(LCMS-02) M ethod Info : HY-365_5HO1RS,M,A-RP-108，210nm,23min
Catalog No : HY-100008 Batch#20299 A-RP-134
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2
2.5
3
50000
100000150000200000250000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20160505\20160505 2016-05-05 09-03-15\BIZ2016-505-WJ4-2.D) ES-API, Pos, Sca
2.848
MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.
Reportable Ion Abundance: > 10%.
Retention Mol. Weight Time (MS) MS Area or Ion
2.848 342631 482.40 I 457.30 I 442.30 I 441.30 I 427.35 I 420.30 I 419.30 I 350.30 I 304.25 I 30
3.30 I 237.20 I 155.20 I 105.15 I 102.20 I
m/z
100
150
200
250
300
350
400
450
20406080100*MSD1 SPC, time=2.855:2.982 of D:\AGLIENT 1260\DATA\20160505\20160505 2016-05-05 09-03-15\BIZ2016-505-WJ4-2.D ES-API Max: 10956
344.3
305.2 139.1
282.3
237.2
304.3
155.2
105.2
469.3
458.3
366.3
443.3
482.4
427.4
441.3
419.3 303.3
*** End of Report ***