GDC-0810_LCMS_21841_MedChemExpress

File D:\CHEM32\1\DATA\BIZ\BIZ2016-926-WJ4.D Tgt Mass (EZX): 446.00 Injection Date : 26 Sep 16 1:26 pm +0800 Seq. Line : 0 Sample Name : BIZ2016-926-WJ4 Location : P1-D-01 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M

Catalog No: HY-12864 Batch#21841 Easy-Access Method: '1-POS-3MIN' 446.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min*

0.5

1

1.5

2 2.5mAU 0

1000

2000

*DAD1 B, Sig=214,4 Ref=off 1.896

2.031

min*

0.51

1.5

2 2.5mAU 0

5001000

*DAD1 C, Sig=254,4 Ref=off 1.880

2.031

min

0.51 1.5

2 2.5

50000

100000150000200000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

2.029

min

0.5

1

1.5

2

2.5

25000

5000075000100000 Ion 447, MSD1 447,Target Mass 446 +H Positive, EIC=446.7:447.7

2.028

Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.90 0.02 5.01 4.42 0.13 233 2.03 0.02 3779.82 2897.78 99.87 447

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.88 0.03 4.98 0.23 0.25 233 2.03 0.02 1993.20 1730.62 99.75 447

Ret. Time: 2.03 <<<< POSITIVE SPECTRA >>>>

m/z

200

300

400

500

600

700

800

900

5000

10000150002000025000

3000035000 ES-API Positive

233.1

450.1

449.1

447.1