JK184-LCMS-22737-MedChemExpress
File D:\CHEM32\1\DATA\BIZ\BIZ2016-D07-WJ7.D Tgt Mass (EZX): 350.00 Injection Date : 7 Dec 16 3:55 pm +0800 Seq. Line : 0 Sample Name : BIZ2016-D07-WJ7 Location : P2-B-05 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M Catalog No : HY-13307 Batch#22737 Easy-Access Method: '1-POS-3MIN' 350.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min*0.5
1 1.5
2 2.5mAU
500
1000
1500
*DAD1 B, Sig=214,4 Ref=off
1.3091.3651.502min*
0.51
1.52
2.5mAU
500
1000
*DAD1 C, Sig=254,4 Ref=off
1.298
1.3651.487min 0.51 1.5
2 2.50
100000
200000
300000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.357min 0.5
1 1.5
2 2.50
50000
100000
150000
200000
Ion 351, MSD1 351,Target Mass 350 +H Positive, EIC=350.7:351.7
1.357 Integration Results for DAD1 B, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.31 0.02 1.97 1.63 0.14 317 1.37 0.01 1431.20 1929.08 99.74 351 1.50 0.03 1.80 1.05 0.13 351
Integration Results for DAD1 C, Sig=254,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.30 0.03 4.52 0.98 0.36 351 1.37 0.01 1243.95 1684.65 99.56 351 1.49 0.02 1.03 0.25 0.08 351
Ret. Time: 1.36 <<<< POSITIVE SPECTRA >>>>m/z 2003004005006007008009000
10000
20000
30000
40000
50000
60000
ES-API Positive
353.2
176.3 351.2