Estramustine_phosphate_sodium_MS_15961_MedChemExpress
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 19
Acq. Instrument : HY-LCMS-02 Location : P1-A-06Injection Date : 5/4/2015 11:13:31 AM Inj : 1
Inj Volume : 3.000 μl Different Inj Volume from Sample Entry Actual Inj Volume : 10.000 μl
Acq. Method : D:\AGLIENT 1260\DATA\20150504\20150504 2015-05-04 08-45-42\100-1500MS+3MIN_ 1.5(0.02%FA).M
Last changed : 5/4/2015 8:48:45 AM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\DATA\20150428\20150428 2015-04-28 10-32-06\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)
Last changed : 5/4/2015 12:09:28 PM by Li Shan(LCMS-02) (modified after loading)
Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃
Sample Info : HY-13627 Batch#15961 A-RP-132
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2 2.5310000
2000030000400005000060000700008000090000100000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150504\20150504 2015-05-04 08-45-42\BIZ2015-504-DJL2-1.D) ES-API, Pos, Sc
1.637
1.774
1.940
2.090
MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.
Reportable Ion Abundance: > 10%.
Retention Mol. Weight Time (MS) MS Area or Ion
1.637 136113 705.70 I 704.75 I 56
2.75 I 256.00 I 254.95 I 102.00 I
1.774 23957 105.00 I 101.95 I
1.940 19747 105.00 I 10
2.10 I
2.090 694330 1042.50 I 1042.20 I 1041.70 I 1041.25 I 1040.70 I 1040.35 I 1039.75 I 1038.70 I 781.40 I 780.95 I 780.20 I 779.35 I 522.60 I 521.70 I 520.65 I 519.70 I 424.80 I 42
3.80 I 422.80 I 421.85 I 288.05 I 105.00 I
m/z
200
400
600
800
1000
1200
2040
6080100*MSD1 SPC, time=1.598:1.674 of D:\AGLIENT 1260\DATA\20150504\20150504 2015-05-04 08-45-42\BIZ2015-504-DJL2-1.D ES-AP Max: 7732
374.8
415.9
104.9
256.0
564.8 562.8
726.7
704.8
102.0
254.9
m/z
200
400
600
800
1000
1200
51015
202530
3540*MSD1 SPC, time=1.749:1.805 of D:\AGLIENT 1260\DATA\20150504\20150504 2015-05-04 08-45-42\BIZ2015-504-DJL2-1.D ES-AP 526.9
110.9 167.9
141.0 216.9
344.0
299.8
446.8 403.8
255.9
445.7
501.8 223.3
105.0
101.9
m/z
200
400
600
800
1000
1200
510
152025*MSD1 SPC, time=1.918:1.994 of D:\AGLIENT 1260\DATA\20150504\20150504 2015-05-04 08-45-42\BIZ2015-504-DJL2-1.D ES-AP 527.6 159.9
553.5 343.6
261.0 100.9
484.8
445.6
419.8 212.0
299.8
517.6
550.7 255.9
105.0
m/z
200
400600800100012000
102030
40506070*MSD1 SPC, time=2.050:2.144 of D:\AGLIENT 1260\DATA\20150504\20150504 2015-05-04 08-45-42\BIZ2015-504-DJL2-1.D ES-AP
141.1
216.9
1051.2 484.8
289.0 255.9
523.6
102.0
425.9 779.3
288.0
520.7 422.8
783.4 1042.5
781.4
1039.8
423.8 519.7
421.9
*** End of Report ***