Mps1-IN-2_LCMS_12771_MedChemExpress
File ..710 2017-07-10 08-26-50\CPK2017-707-12771.D Tgt Mass (CHM): Injection Date : 10 Jul 17 6:34 pm +0800 Seq. Line : 134 Sample Name : CPK2017-707-12771 Location : P1-B-02 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul
Acq. Method : D:\chem32\1\DATA\20170710\20170710 2017-07-10 08-26-50\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\DATA\20170710\20170710 2017-07-10 08-26-50\1-POS-3MIN.M SCatalog No : HY-13994 Batch#12771 A-RP-186
Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min
Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min
0.5
1
1.52
2.5mAU 0
50010001500 DAD1 B, Sig=214,4 Ref=off 1.209
1.2771.339
min
0.51
1.52
2.5mAU 0
200400600 DAD1 C, Sig=254,4 Ref=off 1.237
1.277
1.357
1.445
1.512
1.792
min
0.51 1.5
2 2.50
200000
400000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.264
min
0.5
1
1.5
2 2.50
50000
100000150000 Ion 481.6, MSD1 481.6,Target Mass 480.6 +H Positive, EIC=481.3:482.3
1.266
1.318 Integration Results for DAD1 B, Sig=214,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.02 1474.68 0.01 98.06 241 1.28 0.01 4.98 8.38 0.33 241 1.34 0.02 24.16 0.05 1.61 481
Integration Results for DAD1 C, Sig=254,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.24 0.02 1093.01 919.53 97.19 241 1.28 0.02 7.21 7.80 0.64 241 1.36 0.02 19.45 15.71 1.73 213 1.45 0.02 1.96 0.47 0.17 481 1.51 0.03 1.41 0.88 0.13 481 1.79 0.02 1.52 0.88 0.14 ND
Integration Results for MSD1 TIC, MS File
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|
MS Report from Instrument: LCMS-02
1.26 0.03 1256765.38 590349.69 100.00 241
Ret. Time: 1.26 <<<< POSITIVE SPECTRA >>>>
m/z
200
300
400
500
600
700
800
900
20000
400006000080000 ES-API Positive
480.3 481.3
241.2