MK-3697_LCMS_13111_MedChemExpress

MK-3697_LCMS_13111_MedChemExpress
MK-3697_LCMS_13111_MedChemExpress

File ..M32\1\DATA\20170214\CPK\CPK2017-213-13111.D Tgt Mass (EZX): 447.50 Injection Date : 14 Feb 17 11:52 am +0800 Seq. Line : 0 Sample Name : CPK2017-213-13111 Location : P1-C-03 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M

Catalog No : HY-12301 Batch#13111 Easy-Access Method: '1-POS-3MIN' 447.50 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min*

0.5

1

1.52

2.5mAU 0

250500750*DAD1 B, Sig=214,4 Ref=off 1.1731.221

1.348

1.410

1.5221.547

1.637

min*

0.51

1.52

2.5mAU 0

200400

600*DAD1 C, Sig=254,4 Ref=off 1.1931.207

1.353

1.4101.505

1.565

1.659

1.884

min

0.51 1.5

2

2.5

50000

100000150000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.418

min

0.5

1

1.5

2

2.5

10000

2000030000 Ion 448.5, MSD1 448.5,Target Mass 447.5 +H Positive, EIC=448.2:449.2

1.418

Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.17 0.01 0.88 -0.03 0.05 ND 1.22 0.03 2.67 0.10 0.16 145 1.35 0.02 1.58 1.08 0.09 ND 1.41 0.02 1675.84 1258.12 99.19 225 1.52 0.02 1.00 0.76 0.06 225 1.55 0.02 5.87 -0.01 0.35 363 1.64 0.02 1.62 0.15 0.10 ND

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.19 0.01 0.54 0.58 0.05 ND 1.21 0.04 0.49 0.01 0.05 145 1.35 0.02 1.69 1.19 0.17 ND 1.41 0.02 994.48 747.48 99.43 225 1.51 0.02 0.53 0.05 0.05 225 1.56 0.02 1.09 0.78 0.11 363 1.66 0.02 1.00 0.71 0.10 ND

1.88 0.03 0.40 0.19 0.04 141

Ret. Time: 1.42 <<<< POSITIVE SPECTRA >>>>

m/z

200

300

400

500

600

700

800

5000

10000150002000025000300003500040000 ES-API Positive

449.1 448.2

224.6

相关主题
相关文档
最新文档