MK-3697_LCMS_13111_MedChemExpress
File ..M32\1\DATA\20170214\CPK\CPK2017-213-13111.D Tgt Mass (EZX): 447.50 Injection Date : 14 Feb 17 11:52 am +0800 Seq. Line : 0 Sample Name : CPK2017-213-13111 Location : P1-C-03 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M
Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M
Catalog No : HY-12301 Batch#13111 Easy-Access Method: '1-POS-3MIN' 447.50 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min
Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min*
0.5
1
1.52
2.5mAU 0
250500750*DAD1 B, Sig=214,4 Ref=off 1.1731.221
1.348
1.410
1.5221.547
1.637
min*
0.51
1.52
2.5mAU 0
200400
600*DAD1 C, Sig=254,4 Ref=off 1.1931.207
1.353
1.4101.505
1.565
1.659
1.884
min
0.51 1.5
2
2.5
50000
100000150000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.418
min
0.5
1
1.5
2
2.5
10000
2000030000 Ion 448.5, MSD1 448.5,Target Mass 447.5 +H Positive, EIC=448.2:449.2
1.418
Integration Results for DAD1 B, Sig=214,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.17 0.01 0.88 -0.03 0.05 ND 1.22 0.03 2.67 0.10 0.16 145 1.35 0.02 1.58 1.08 0.09 ND 1.41 0.02 1675.84 1258.12 99.19 225 1.52 0.02 1.00 0.76 0.06 225 1.55 0.02 5.87 -0.01 0.35 363 1.64 0.02 1.62 0.15 0.10 ND
Integration Results for DAD1 C, Sig=254,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.19 0.01 0.54 0.58 0.05 ND 1.21 0.04 0.49 0.01 0.05 145 1.35 0.02 1.69 1.19 0.17 ND 1.41 0.02 994.48 747.48 99.43 225 1.51 0.02 0.53 0.05 0.05 225 1.56 0.02 1.09 0.78 0.11 363 1.66 0.02 1.00 0.71 0.10 ND
1.88 0.03 0.40 0.19 0.04 141
Ret. Time: 1.42 <<<< POSITIVE SPECTRA >>>>
m/z
200
300
400
500
600
700
800
5000
10000150002000025000300003500040000 ES-API Positive
449.1 448.2
224.6