LZ 20015数据

LUBRIZOL20015

LUBRIZOL7070H

API SM

ACC Base Oil Interchange Program Yubase Group-III Base Stocks

ACC Candidate Data Package

Report No.C-12240

December2007

The Lubrizol Corporation

29400Lakeland Boulevard

Wickliffe,Ohio44092

?2007The Lubrizol Corporation

●

●

●

●

●

●●●●

●

●●Section 2

Multiple Test Evaluation Procedure (MTEP)sheets (if required).

Section 5

Engine test reports which do not support the final formulation.

Section 3

Engine Test Reports -support the performance claims of the final formulation.

12/1/2007

Engine Test Waiver Sheets (if applicable).Level 2Support Data (if required).

TABLE OF CONTENTS

Final Formulation -chemical and physical characterization.Base Oil Data ACC monitoring agency summary.

Program Overview

Program Engine Test Summary -base oils and viscosity grades for each engine test run,and final formulations supported.Engine Test Results -summary.Tested Formulations that support the final formulation.Section 1

Infrared trace,other chemical or physical test reports on the final formulation.

Report number C-12240contains data to support the following final formulation:

CREDENTIAL

API SM PROGRAM TYPE

BOI SAE VISCOSITY GRADE

5W-30PERFORMANCE ADDITIVE

8.00%w Lubrizol 20015VISCOSITY MODIFIER

-non-dispersant OCP

6.90%w Lubrizol 7070H BASE STOCK SLATE Yubase Group-III

This Base Oil Interchange program is built from the following core program:

REPORT

C-12239CREDENTIAL

API SM PROGRAM TYPE

Matrix Core SAE VISCOSITY GRADE

5W-30PERFORMANCE ADDITIVE

8.00%w Lubrizol 20015VISCOSITY MODIFIER

-NON-dispersant OCP

BASE STOCK SLATE Motiva /Chevron Group-II

PROGRAM OVERVIEW

This program was conducted in accordance with the American Chemistry Council (ACC)Petroleum Additives

Product Approval Code of Practice.

Physical and chemical data of only viscosity grades on which engine tests were conducted are included in this

report.If a customer wishes to use a viscosity grade,where read-across is permitted,then the customer will need

to generate the necessary chemical and physical data.If requested by the customer,The Lubrizol Corporation

will assist in providing the data.

7.10%w Lubrizol 7070H

PROGRAM ENGINE TEST REPORT

Final

From C-12239

Base Oil Motiva Chevron Yubase

SAE Vis Grade5W-305W-305W-30

Base Oil Group II II III

Performance Level-API SM API SM

Engine Tests

Sequence IIIG-X X

Sequence IIIGA-X X

Sequence IVA X BOI BOI

Sequence VG-X BOI

Sequence VIII-X BOI

Notes:

The Core Data Set is surrounded with double lines.

X=Test run;formulation details and test report included Candidate Data Package.

PG=Test waived per ACC Code of Practice Program Guidelines.

BOI=Test waived per API Base Oil Interchange Guidelines for PCMO and Diesel Engine Oils.

VGRA=Test waived per API Guidelines for SAE Viscosity Grade Read Across Engine Testing.

Engine Test

Results Sequence IIIG,(RM-0321050101-A)

5W-30Viscosity Increase %@40C

98150max Average Cam +Lifter Wear,μm

30.960max Weighted Piston Deposits,merits

3.66 3.5min Hot Stuck Rings

0None Sequence IIIGA,(RM-0321050101-A)

5W-30100hr Drain,D4684(MRV TP-1)Temp,C

-30Original grade 100hr Drain,D4684(MRV TP-1)Viscosity,cP

21,300or next higher Sequence IVA,(RM-0321050128-A)

5W-30Average Camshaft Wear,μm

66.6290max Sequence VG,(RM-0321050101-A)

5W-30Average Engine Sludge,merits

8.627.8min Rocker Cover Sludge,merits

9.668.0min Average Engine Varnish,merits

9.098.9min Average Piston Skirt Varnish,merits

8.127.5min Oil Screen Sludge,%

220max Hot Stuck Compression Rings

0None Cold Stuck Rings

0Rate &Report Oil Screen Debris,%

0Rate &Report Oil Ring Clogging,%

0Rate &Report Sequence VIII,(RM-0321050101-A)

5W-30Bearing Weight Loss,mg

17.426max Ten-Hour Stripped Viscosity,cSt at 100C 9.3Stay-in-Grade

SUMMARY OF ENGINE TEST RESULTS FROM C-12239

API SM Requirements

Engine Test

Results Sequence IIIG,(RM-0115070500-A)

5W-30Viscosity Increase %@40C

54.6150max Average Cam +Lifter Wear,μm

3660max Weighted Piston Deposits,merits

4.42 3.5min Hot Stuck Rings

0None Sequence IIIGA,(RM-0115070500-A)

5W-30100hr Drain,D4684(MRV TP-1)Temp,C

-30Original grade 100hr Drain,D4684(MRV TP-1)Viscosity,Cp 16,500or next higher

API SM Requirements SUMMARY OF ENGINE TEST RESULTS FOR YUBASE FORMULATION

Formulations tested to support the final formulation.

Basic Candidate Formulation

Final Formulation

ACC Number:RM-321050128321050101115070500 Modification A A A

OS#OS224093OS221441OS225779OS228339 SAE Viscosity Grade5W-305W-305W-305W-30 Base Oils,Mass%

YUBASE4[Gp III]--42.7042.45 YUBASE6[Gp III]--42.7042.45 CHEVRON5R[Gp II]-44.83--CHEVRON100R[Gp II]-16.93--CHEVRON220R[Gp II]-22.84--MOTIVA TEX HVI5W[Gp II]84.00---Additives,Mass%

Lubrizol?200158.008.008.008.00 Lubrizol?7070H7.707.10 6.40 6.90 Lubrizol?6662A0.300.300.200.20

TOTAL100.00100.00100.00100.00 Chemical/Physical

D445Viscosity@100C,cSt10.5910.6310.3410.45 D2896TBN7.27.57.47.2

D5293CCS Viscosity Temperature,C-30-30-30-30

D5293CCS Viscosity,cP4,8135,9635,0394,939 D4683HTHS,cP 2.97 2.98 2.94 2.95 Elements,%

ICP Calcium0.16240.16290.16000.1634 ICP Sodium0.04870.03890.45100.0450 ICP Phosphorus0.07460.07650.07530.0756 ICP Sulfur0.21940.22770.22720.2141 ICP Zinc0.08370.08660.08510.0862 D4629Nitrogen0.08000.07920.07410.0720

Engine Tests IVA VIII,VG,

IIIG,IIIGA IIIG;IIIGA MHT

TEOST,BRT

Matrix Core From C-12239

Chemical and Physical Characterization of the Final Formulation

Final Formulation OS#OS228339 Grade5W-30

API Performance SM

Base Oils,Mass%

YUBASE4[Gp III]42.45 YUBASE6[Gp III]42.45 Additives,Mass%

Lubrizol?20015DI8.00

Lubrizol?7070H VM 6.90

Lubrizol?6662A PPD0.20

Total100

Chemical/Physical

D445Viscosity@100°C,cSt10.45

D445Viscosity@40°C,cSt59.20

D4683HTHS,cP 3.0

D5293CCS Viscosity Temperature,°C-30°C

D5293CCS Viscosity,cP4,939

D4684MRV TP-1Viscosity Temperature,°C-35°C

D4684MRV TP-1Viscosity,cP33,800

D2896TBN7.2

ICP Calcium,%0.1634

ICP Phosphorus,%0.0756

ICP Sulfur,%0.2141

ICP Zinc,%0.0862

ICP Sodium,%0.0450

D4629Nitrogen,%0.0720

Infrared Trace F6803N

D5133Gelation Index 4.8

Ball Rust Test125

D5800NOACK Volatility,%11.2

D6417Simulated Distillation,% 5.4

D6922Homogeneity&Miscibility PASS EOFT,%-54.66

EOWTT@0.6%H2O,%23.44

EOWTT@1.0%H2O,%19.54

EOWTT@2.0%H2O,%25.16

EOWTT@3.0%H2O,%23.81

D892A Sequence I0/0

D892A Sequence III0/0

D892A Sequence III0/0

D6082A High Temp Foam10/0

TEOST MHT-4,mg10.6

D6278Shear Stability,cSt8.55

BASE OIL DATA

Base Oil CHEVRON

RLOP100R

CHEVRON

RLOP220R

CHEVRON

RLOP5R

MOTIVA TEX

HVI5W YUBASE4YUBASE6

Viscosity Index94104119118121129 Viscosity@100°C,cSt 4.05 6.368 4.74 4.41 4.354 6.405 Viscosity@40°C,cSt20.31240.94123.82321.2620.5836.213 Hydrocarbon Type

Saturates(D2007),%97.69293.596.198.797.4 Sulfur(D4294),%0.00250.00020.00230.0040.00250 API Group II II II II III III

ENGINE TEST WAIVER SHEETS Sequence IVA,Sequence VG MTEP CALCULATION SHEETS None

LEVEL2SUPPORT DOCUMENTS None

Is test required? Sequence IV-A NO

Based on:cSt@100°C

New oil must be≥ 4.38

Originally tested formulation%

mass

API Group

I,II,III,IV,V

D445@100°C,

cSt

Motiva Tex HVI5W100.0II 4.41 Original BO2

Original BO3

Original BO4

Original BO blend@100%100.0 4.41

New final formulation%

mass

API Group

I,II,III,IV,V

D445@100°C,

cSt

Yubase4cSt50.0III 4.35 Yubase6cSt50.0III 6.41 New BO3

New BO4

New BO blend@100%100.0 5.28 D New-Original0.87 All measurements-same lab/operator?Y or N B N

ASTM Precision D445

Reproducibility multiplier0.00650

Reproducibility offset0.00000

Repeatability multiplier0.00110

Repeatability offset0.00000

Sequence VG

NO NO Based on:

Sulfur Saturates New oil must be -->

≤0.0339≥90Originally tested formulation

%mass API Group I,II,III,IV,V D4294,%Sulfur D2007,%Saturates Chevron 5R

53.0II 0.002393.50Chevron 100R

20.0II 0.002591.40Chevron 220R

27.0II 0.000292.00Original BO 4

Original BO blend @100%

100.00.001892.6750New final formulation

%mass API Group I,II,III,IV,V D4294,%Sulfur D2007,%Saturates Yubase 4cSt

50.0III 0.002598.70Yubase 6cSt

50.0III 0.000097.40New BO 3

New BO 4

New BO blend @100%

100.00.001398.0500D New -Original

-0.0005 5.3750N N ASTM Precision

D4294D2007Reproducibility multiplier

0.12150 4.00000Reproducibility offset

0.006750.00000Repeatability multiplier

0.02894 2.10000Repeatability offset 0/048940.00000

Is test required?

All measurements -same lab /operator?Y or N -->

Engine tests which do not support the final formulation There are no tests included which do not support the final formulation.