TGR-1202_LCMS_23911_MedChemExpress

File D:\CHEM32\1\DATA\HEC\ZG3946-033-4A-1.D Tgt Mass (EZX): Injection Date : 10 Mar 17 4:45 pm +0800 Seq. Line : 0 Sample Name : ZG3946-033-4A-1 Location : P1-B-01 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M

Catalog No : HY-12279 Batch#23911 Easy-Access Method: '1-POS-3MIN' Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min*

0.5

1

1.5

2 2.5mAU 0

5001000

15002000*DAD1 B, Sig=214,4 Ref=off 1.368

1.546

1.640

1.7051

.7181.7841.8451

.8531.922

2.264

min*

0.51

1.52

2.5mAU 0

250500

750100012501500*DAD1 C, Sig=254,4 Ref=off

1.3091.368

1.548

1.6331.6421.6901.7361.785

1.867

1.922

2.004

2.2272

.246min

0.5

1

1.5

2

2.5

5000

1000015000200002500030000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

2.027

Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)

|-------|--------|--------------|--------------|--------|------| 1.37 0.02 12.07 12.84 0.41 ND 1.55 0.01 0.94 0.18 0.03 ND 1.64 0.02 5.39 0.08 0.18 ND 1.71 0.02 0.93 0.91 0.03 ND 1.72 0.02 2.90 0.61 0.10 ND 1.78 0.02 9.11 8.70 0.31 ND 1.85 0.01 1.15 2.02 0.04 ND 1.85 0.02 5.66 2.03 0.19 ND 1.92 0.02 2873.78 2599.29 98.54 572 2.26 0.02 4.43 3.57 0.15 ND

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.31 0.02 0.28 0.05 0.02 ND 1.37 0.01 6.72 7.76 0.37 ND 1.55 0.01 0.37 0.02 0.02 ND 1.63 0.01 0.39 0.62 0.02 ND

1.64 0.02 3.40 0.64 0.19 ND 1.69 0.02 0.77 0.06 0.04 ND 1.74 0.02 1.58 1.46 0.09 ND 1.78 0.02 3.83 3.52 0.21 ND 1.87 0.02 3.35 3.36 0.18 ND

1.92 0.02 1789.17 1710.20 98.61 572

2.00 0.02 1.64 1.15 0.09 572 2.23 0.02 0.68 0.49 0.04 ND 2.25 0.02 2.23 0.22 0.12 ND

Ret. Time: 2.03 <<<< POSITIVE SPECTRA >>>>

m/z

200

300

400

500

600

700

800

900

1000

2000

300040005000

6000700080009000 ES-API Positive

574.3

573.2

572.2