EMD-1214063_LCMS_14144_MedChemExpress

=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 52

Acq. Instrument : HY-LCMS-02 Location : Vial 10Injection Date : 12/10/2014 1:38:49 PM Inj : 1

Inj Volume : 3.000 μl

Acq. Method : D:\AGLIENT 1260\DATA\20141210\20141210 2014-12-10 09-15-11\100-1000MS+3MIN( 0.02%FA).M

Last changed : 12/10/2014 9:15:11 AM by Li Shan(LCMS-02)

Analysis Method : D:\AGLIENT 1260\DATA\20141209\20141209 2014-12-09 09-10-51\100-1000MS+3MIN( 0.02%FA).M (Sequence Method)

Last changed : 12/10/2014 3:02:20 PM by Li Shan(LCMS-02) (modified after loading)

Method Info : Postive,MS:100-1000,Column ID:A-RP-102,40℃

A-RP-32

Additional Info : Peak(s) manually integrated

min

0.5

1.52

2.53mAU 0

200400600

8001000 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...60\DATA\20141210\20141210 2014-12-10 09-15-11\BIZ2014-D10-DJL3.D)

1.323

1.474

1.759 1.802 A r e a : 0.657444

1.852 1.934

===================================================================== Area Percent Report =====================================================================

Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000

Do not use Multiplier & Dilution Factor with ISTDs

Signal 1: DAD1 C, Sig=254,4 Ref=off

Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %

----|-------|----|-------|----------|----------|--------| 1 1.323 MM R 0.0418 34.72801 13.84920 0.8804 2 1.474 MM R 0.0488 3897.59692 1249.82251 98.8142 3 1.759 MM R 0.0327 2.79822 1.12211 0.0709 4 1.802 MM R 0.0417 6.97172 5.31115e-1 0.1768 5 1.852 MM T 8.90e-3 6.57444e-1 1.23146 0.0167 6 1.934 MM R 0.0412 1.61809 9.61431e-2 0.0410

Totals : 3944.37041 1266.65254

===================================================================== *** End of Report ***

Catalog No : HY-14721 Batch#14144

=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 52

Acq. Instrument : HY-LCMS-02 Location : Vial 10Injection Date : 12/10/2014 1:38:49 PM Inj : 1

Inj Volume : 3.000 μl

Acq. Method : D:\AGLIENT 1260\DATA\20141210\20141210 2014-12-10 09-15-11\100-1000MS+3MIN( 0.02%FA).M

Last changed : 12/10/2014 9:15:11 AM by Li Shan(LCMS-02)

Analysis Method : D:\AGLIENT 1260\DATA\20141209\20141209 2014-12-09 09-10-51\100-1000MS+3MIN( 0.02%FA).M (Sequence Method)

Last changed : 12/10/2014 3:03:44 PM by Li Shan(LCMS-02) (modified after loading)

Method Info : Postive,MS:100-1000,Column ID:A-RP-102,40℃

Catalog No : HY-14721 Batch#14144 A-RP-32

Additional Info : Peak(s) manually integrated

min

0.5

1.5

2.5

200000

4000006000008000001000000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20141210\20141210 2014-12-10 09-15-11\BIZ2014-D10-DJL3.D) ES-API, Pos, Sca

1.484

MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.

Reportable Ion Abundance: > 10%.

Retention Mol. Weight Time (MS) MS Area or Ion

1.484 6133125 494.20 I 493.20 I 247.15 I

m/z

100

200

300

400

500

600

700

20406080100*MSD1 SPC, time=1.452:1.525 of D:\AGLIENT 1260\DATA\20141210\20141210 2014-12-10 09-15-11\BIZ2014-D10-DJL3.D ES-API,Max: 528819

495.2

247.1

494.2 493.2

*** End of Report ***