AM-2394_LCMS_22734_MedChemExpress
File D:\CHEM32\1\DATA\BIZ\BIZ2016-D07-WJ4.D Tgt Mass (EZX): 423.00 Injection Date : 7 Dec 16 3:37 pm +0800 Seq. Line : 0 Sample Name : BIZ2016-D07-WJ4 Location : P2-B-02 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M Catalog No : HY-100221 Batch#22734 Easy-Access Method: '1-POS-3MIN' 423.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min*0.5
1 1.5
2 2.5mAU
500
1000
*DAD1 B, Sig=214,4 Ref=off
1.212
1.3051.3991.469min*
0.51
1.52
2.5mAU
500
1000
*DAD1 C, Sig=254,4 Ref=off
1.3451.3991.469min 0.51 1.5
2 2.50
50000
100000
150000
200000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.391min 0.5
1 1.5
2 2.50
20000
40000
60000
80000
Ion 424, MSD1 424,Target Mass 423 +H Positive, EIC=423.7:424.7
1.391 Integration Results for DAD1 B, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.01 3.86 5.82 0.29 317 1.31 0.01 1.26
2.04 0.09 317 1.40 0.01 1326.18 1659.15 98.71 424 1.47 0.02 12.27 11.74 0.91 424
Integration Results for DAD1 C, Sig=254,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.35 0.01 2.66 2.88 0.21 317 1.40 0.01 1231.57 1544.67 98.85 424 1.47 0.02 11.66 11.08 0.94 424
Ret. Time: 1.39 <<<< POSITIVE SPECTRA >>>>m/z 2003004005006007008009000
5000
10000
15000
2000025000
ES-API Positive
462.1
212.6 317.4 203.8 425.4 424.3