IRAK-inhibitor-6-LCMS-05125-MedChemExpress
File D:\DATA\A02\MONITOR\CPK2016-713-051251-04484-LCMSA016.D
Injection Date : 20 Jul 16 3:55 pm +0800 Tgt Mass(EZX) : 396.00 Sample Name : CPK2016-713-05125 Location : P1-D-02 Acq. Operator : A02-Monitor Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\METHODS\1-POS-MON.M Analysis Method : D:\METHODS\1-POS-MON.M
Catalog No : HY-13280 Batch#05125 Easy-Access Method: '1-POS-MON' 396.00 Method Info : Mobile Phase: A: water(0.01%TFA) B : ACN Gradient: 5%B increase to 95%B within1.5min,
95%B for 1.5min,back to 5%B within 0.01min. Flow Rate: 2.0 mL/min
Column: Sunfire C18 4.6*50mm 3.5um Oven Temperature: 50 C Mass Range:103-1500
min*
00.51 1.5
2 2.5mV 23.215
23.217523.22*ADC1 A, ELSD
min*
00.51 1.5
2 2.5mAU 0
2000
*DAD1 A, Sig=214,4 Ref=off
1.406
1.573
min*
00.51 1.5
2 2.5mAU 0
1000
*DAD1 B, Sig=254,4 Ref=off 1.573
min
00.51
1.5
2 2.50
200000
400000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.571
2.804
min
00.5
1
1.5
2
2.5
50000
100000 Ion 397, MSD1 397,Target Mass 396 +H Positive, EIC=396.7:397.7
1.570
Integration Results for ADC1 A, ELSD
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------|
Integration Results for DAD1 A, Sig=214,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.41 0.01 8.50 10.46 0.30 1.57 0.01 2872.72 3327.82 99.70
Integration Results for DAD1 B, Sig=254,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.57 0.01 1374.46 1781.37 100.00
Ret. Time: 1.57 <<<< POSITIVE SPECTRA >>>>
m/z
200
400
600
800
1000
1200
1400
10000
2000030000400005000060000 ES-API Positive
399.0
817.0
815.1
397.1
199.1
Ret. Time: 2.80
m/z
200400600800100012000
2500
500075001000012500
1500017500 ES-API Positive
218.9
193.9
675.5
159.0
339.3 361.4
338.3 360.3