TEPP-46_LCMS_22344_MedChemExpress

File D:\CHEM32\1\DATA\BIZ\BIZ2016-N03-WJ5.D Tgt Mass (EZX): 372.00 Injection Date : 3 Nov 16 2:36 pm +0800 Seq. Line : 0 Sample Name : BIZ2016-N03-WJ5 Location : P1-E-02 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M

Catalog No : HY-18657 Batch#22344 Easy-Access Method: '1-POS-3MIN' 372.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min*

0.5

1

1.52

2.5mAU 0

250500750*DAD1 B, Sig=214,4 Ref=off 1.2871.331

1.7481.792

min*

0.51

1.52

2.5mAU 0

5001000

1500*DAD1 C, Sig=254,4 Ref=off 1.2871.336

1.459

min

0.51 1.5

2

2.5

50000

100000150000200000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.281

min

0.5

1

1.52

2.50

25000

5000075000100000 Ion 373, MSD1 373,Target Mass 372 +H Positive, EIC=372.7:373.7

1.280

Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.29 0.02 998.82 1098.48 98.91 373 1.33 0.02 5.89 6.26 0.58 373 1.75 0.02 2.61 2.57 0.26 233 1.79 0.02 2.55 0.19 0.25 233

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.29 0.02 1881.54 2050.81 99.49 373 1.34 0.01 6.89 7.05 0.36 373 1.46 0.02 2.75 3.00 0.15 233

Ret. Time: 1.28 <<<< POSITIVE SPECTRA >>>>

m/z

200

300

400

500

600

700

800

900

2500

50007500

10000

12500150001750020000 ES-API Positive

768.2

141.1

233.1

187.1

373.1

395.0

373.2