Thiostrepton_LCMS_23707_MedChemExpress

File ..HEM32\1\DATA\20170301\BIZ\BIZ2017-301-WJ5.D Tgt Mass (EZX): 1663.40 Injection Date : 28 Feb 17 6:58 pm +0800 Seq. Line : 0 Sample Name : BIZ2017-301-WJ5 Location : P1-C-05 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN-2000.M Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M

Catalog No : HY-B0990 Batch#23707 Easy-Access Method: '1-POS-3MIN-2000' 1663.40 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min*

0.5

1 1.52

2.5mAU 0

5001000

*DAD1 B, Sig=214,4 Ref=off 0.867

1.612

1.734

2.108

2.296

min*

0.51

1.52

2.5mAU 0

200400

600*DAD1 C, Sig=254,4 Ref=off 0.902

1.431

1.619

1.726

2.108

2.247

2.317

min

0.51 1.5

2

2.50

10000

20000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 50

2.101

min

0.5

1

1.5

2 2.5-0.1

-0.0500.05 Ion 1664.4, MSD1 1664.4,Target Mass 1663.4 +H Positive, EIC=1664.1:1665.1 Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.87 0.04 45.72 0.30 0.99 ND 1.61 0.05 5.21 0.43 0.11 ND 1.73 0.04 15.98 -0.18 0.35 ND 2.11 0.05 4511.21 1476.25 98.04 833 2.30 0.05 23.39 0.66 0.51 ND

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.90 0.05 8.18 2.87 0.30 ND 1.43 0.09 9.40 0.08 0.34 ND 1.62 0.05 2.83 0.08 0.10 ND 1.73 0.05 2.93 0.08 0.11 ND 2.11 0.05 2695.91 889.63 98.81 833 2.25 0.04 1.33 0.09 0.05 ND 2.32 0.05 7.71 0.06 0.28 ND

Ret. Time: 2.10 <<<< POSITIVE SPECTRA >>>>

m/z

600

700

800

900

1000

500100015002000250030003500 ES-API Positive

833.0

555.8

833.3 832.8