Metaxalone_LCMS_23153_MedChemExpress

File D:\CHEM32\1\DATA\BIZ\BIZ2017-105-WJ2.D Tgt Mass (EZX): 221.10 Injection Date : 4 Jan 17 4:31 pm +0800 Seq. Line : 0 Sample Name : BIZ2017-105-WJ2 Location : P2-B-08 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M Analysis Method : D:\Chem32\1\METHODS\1-STANDBY.M

Catalog No : HY-B0678 Batch#23153 Easy-Access Method: '1-POS-3MIN' 221.10

Method Info : Column: A-RP-169

min*

0.5

1

1.5

2 2.5mAU 0

5001000

*DAD1 B, Sig=214,4 Ref=off 1.418

1.5421.6281.677

1.719

1.7671.787

min*

0.51

1.5

2 2.5mAU 0

2040*DAD1 C, Sig=254,4 Ref=off 1.675

1.719

1.9301

.941min

0.51 1.5

2

2.5

200000

400000600000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.698

min

0.5

1

1.5

2 2.50

50000

100000

150000200000 Ion 222.1, MSD1 222.1,Target Mass 221.1 +H Positive, EIC=221.8:222.8

1.605

1.698

Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)

|-------|--------|--------------|--------------|--------|------| 1.42 0.01 0.56 0.72 0.03 130 1.54 0.02 4.71 4.24 0.25 321 1.63 0.02 3.03 3.30 0.16 222 1.68 0.02 0.84 1.07 0.04 222 1.72 0.02 1879.85 1674.55 98.17 222 1.77 0.01 9.07 14.49 0.47 222 1.79 0.02 16.85 14.66 0.88 222

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.68 0.01 0.43 0.57 0.71 222 1.72 0.02 58.43 53.60 96.79 222 1.93 0.02 1.00 0.88 1.66 222 1.94 0.02 0.51 0.54 0.84 222

Ret. Time: 1.70 <<<< POSITIVE SPECTRA >>>>

m/z

200

3004005006007008009000

10000

200003000040000

50000600007000080000 ES-API Positive

444.3 260.1

465.1

223.2

443.2 222.3