3-TYP-LCMS-26550-MedChemExpress

File ..Data\20170929\20170929-1\BIZ2017-929-WYQ3.D Tgt Mass (CHM): Injection Date : 29 Sep 17 5:33 pm +0800 Seq. Line : 32 Sample Name : BIZ2017-929-WYQ3 Location : P1-B-09 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 0.5 ul Acq. Method : D:\LCMS03\Data\20170929\20170929-1\1-POS-3MIN.M Analysis Method : D:\LCMS03\Data\20170929\20170929-1\1-POS-3MIN.M Catalog No : HY-108331 Batch#26550 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min 00.5

1 1.5

2 2.5mAU 0

100

200

DAD1 A, Sig=214,4 Ref=off

0.5631.246min

00.5

1 1.5

2 2.5mAU 0

100

200

DAD1 B, Sig=254,4 Ref=off

0.5631.1301.1601.1991.560min 00.51

1.52

2.5mV

10

12

ELS1 A, ELSD Signal

min 00.51

1.52

2.55000001000000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

0.581min 00.51 1.52 2.50

2500

5000

Ion 146, MSD1 146,Target Mass 146 Positive, EIC=145.7:146.7

Integration Results for DAD1 A, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.56 0.03 545.37 329.08 99.87 147 1.25 0.01 0.69 0.79 0.13 233

Integration Results for DAD1 B, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.56 0.03 592.18 337.78 99.87 147 1.13 0.02 0.29 0.20 0.05 261 1.16 0.02 0.37 0.32 0.06 261 1.20 0.01 0.05 0.07 0.01 349 1.56 0.01 0.06 0.08 0.01 233

Integration Results for MSD1 TIC, MS File

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.58 0.06 1974604.63 490551.78 100.00 147

Ret. Time: 0.58 <<<< POSITIVE SPECTRA >>>>m/z 1002003004005006007008009000

20000

40000

60000

80000

100000

ES-API Positive

148.1147.1

*** End of Report ***