有机化学-英文实验文档书写
精选关于英文版化学实验报告
精选关于英文版化学实验报告篇一：英文版化学实验报告Title: Preparation of Fe scrap from waste(NH4) 2SO4.FeSO4.6H2OThe purpose of the experimentLearn the method used scrap iron preparation of ferrous ammonium sulfate.Familiar with the water bath, filtered, and evaporated under reduced pressure and crystallization basic working.The experimental principle, the iron and sulfuric acid to generate reactive ferrous sulfate, ferrous sulfate and ammonium sulfate in an aqueous solution of equal molar interaction, becomes less soluble blue generate ferrous ammonium sulfate.Fe+H2SO4=FeSO4+H2 (gas)FeSO4+ (NH4)2SO4+6H2O=(NH4)2SO4.FeSO4.6H2O Usually ferrous rocks are easily oxidized in air, but after the formation of relatively stable perfunctory, not to be oxidized.Experiment to use instruments, scales, constant temperature water bath, pumps, basins, cups, 10ml graduated cylinder, asbestos mesh, glass, tripod, alcohol lamp, funnel.Iron pieces to a solid pharmaceutical use, use of acid ammoniumsulfate and 3mol / l of sulfuric acid, concentrated sulfuric acid.The experiment was divided into four steps.The first step Said iron powder 4g into a beaker and then 50ml 10ml, 3mol / L H2SO4 was added to the same beaker. The second step will be the beaker is heated to no more bubbles, and then filtered hot and the filtrate was then filled in 100ml beaker. The third step, called 4g (NH4)2SO4, and the resultingammonium sulfate and 5.3ml of water to form a saturated solution, and then add it to the ferrous sulfate solution, adjusted with concentrated sulfuric acid to PH = 1. A fourth step, the third step the solution was heated in a water bath to the surface until the film is crystallized, it was slowly cooled andthen filtered under reduced pressure to stand finally dried, weighed and the yield was calculated. The results obtained 8.1g bluish powdery crystals. Have this result we can calculate yield, starting with the first step we tried to know the amount of iron, should this we can calculate the theoretical sulfate ferrous sulfate is 0.03mol, then ferrous sulfate obtained by the0.03molFeSO4 theoretical value of ammonium. FeSO4+（NH4）2SO4+6H2O=FeSO4.(NH4)2SO4.6H2O 0.03molX molX=0.03molm=XM=0.03molⅹ392g/mol=11.76gYield = the actual value of the formula is divided by the theoretical value by 100%.it will be calculated into the data obtained in a yield of 68.9%.篇二：英文版化学实验报告The preparation of alkali type copper carbonateThe first:the experiment purpose1.Master the methods of alkali type copper carbonate prepared and principle2.Through the design experiment to cultivate independent design ability and chemical research thinkingThe second:the experimental principleThe solubility of Cu(OH)2and CuCO3 are similar, With Cu2(OH)2CO3 solid precipitation in the solution.2CuSO4+2Na2CO3+H2O==Cu2(OH)2CO3↓+2Na2SO4+CO2↑The third:the experimental steps1.Solution preparationDisposes 0.5 mole of each litre acid sour coppers and sodium carbonate solution each 100 milliliters.2.The feeding order and raw material compare the explorationAccording to 2:1.6,2:2,2:2.4,2:2.8 allocated proportion, is accepted after passing an examination the surface disposition acid sour copper and the sodium carbonate solution, joins in separately 8 test tubes, joinsrapidly the sulfuric acid copper solutions in the sodium carbonate solution, vibrates about other constant temperature ten minutes as for 75 degrees Celsius water baths in, the inversion feeding order recreates one time, the observation has the precipitation speed, quantity how many and the color, discovers the optimum condition.3.Temperature explorationAccording to the above optimum condition, takes the acid sour copper solutions and the sodium carbonate solution separately under 50, 75 and 100 degrees Celsius responded that, discovers the optimum temperature.4.According to 2, 3 step exploration optimum condition prepares the final product, and with the distilled water lavation, finally dries and calls heavily.(Enlarges ten times with conical flask to do)The fourth:the experimental itemsInstrument and material: The balance, the beaker, the glass rod, the Volumetric flask, the test tube, the filter flask,the Buchner funnel, the Erlenmeyer flaskChemicals: Copper carbonate, sodium sulfateThe fifth:the experimental result1.By the step 2, the observation phenomenon optimum condition is equal to for the cupric sulfate compared to the sodium carbonate 2:2.4, the feeding order for joins the sulfuric acid copper solutions to the sodiumcarbonate solution in.2.By the step 3, the observation phenomenon optimum temperature is 75 degrees Celsius3.According to the copper sulfate solution than sodium carbonatesolution is 2:2. 4, ten times magnification, alkali type copper carbonate was zero point five grams, according to the reaction equation calculation yield.2CuSO4+2Na2CO3+H2O==Cu2(OH)2CO3↓+2Na2SO4+CO2↑2 10.5*0.02 X2/(0.5*0.02)=1/XX=0.005M[Cu2(OH)2CO3]=0.005*222=1.11gProductive rate:0.5/1.11*100%=45%The sixth : Questions1. Which cupric salt suit the system to take the cupric basic carbonate? Answer:Cu(NO)3 or CuSO42. The reaction temperature has what influence to this experiment?.Answer:The temperature excessively is low, the response speed is slow; The hyperpyrexia, the Cu2(OH)2CO3 decomposition is CuO.3. Reaction is carried out at what temperature will appear Brown product? What is the brown substance?Answer: The temperature is equal to 100 degrees Celsius and this brown material is CuO.篇三：化学专业英语实验报告In the physiological saline the sodium chloride content determinationone, the experimental goal1、the study silver nitrate standard solution configuration and the demarcation method2、the grasping law raises Si Fa to determine the chloride ion the method principle two, the experimental principleWith AgNO3 standard solution titration Cl - Ag + + Cl - = = AgCl，At ph 7.0 -10.5 available fluorescent yellow do indicator (HFIn)HFIn = = FIn (yellow) + H +Sp before: excessive, AgCl precipitation adsorption of Cl - AgCl Cl - + FIn - (yellow-green)After Sp: Ag +, excessive AgCl precipitation Ag + adsorption, adsorption FIn - reprecipitation AgCl, Ag + + FIn - = = AgCl, Ag +, FIn - (pink) The finish color changes: from yellowish green to orange Three, instruments and reagentsEquipment and materials：Acid type buret (150 ml), taper bottle (250 ml), volumetric flask (100 ml), pipette (20 ml, 10 ml), measuring cylinder (100 ml, 10 ml), beaker (100 ml), brown reagent bottles (500 ml),analytical balance, platform scale. The reagent and drug: Analysis of AgNO3 (s, pure), NaCl (s,analysis of pure), physiological saline, fluorescent yellow - starch. Fourth, the experimental stepsAccurately moving 25 ml concentration is 0.7064 mol ╱L of silver nitrate standard solution in the middle of 250 ml volumetric flask, dilute to scale as a standard solution titration.Accurately moving saline 10.00 ml to 250 ml conical flask, add 50 ml water, 3 drops of fluorescent yellow indicator, 5% starch indicator 5 ml, under continuous agitation, using silver nitratestandard solution titration to solution from yellow to pink is the end point. Record the consumption volume of silver nitratestandard solution, parallel determination of 3, calculate the sodium chloride content in saline and relative mean deviation.Fifth, data recording and processingFormula: ρ = V×MrNaCl×CAgNO3 x 100The average deviation d=0.01300 dr=d/ρ×100%=0.13%。
有机实验记录英文范例模板
有机实验记录英文范例模板Part1:反应前的装置描述1.1:A3L three-necked round bottom flask equipped with mechanical stirrer(or magnetic stirrer),addition funnel and thermometer(or Dean-Stock;drying tube)1.2:All flasks used in the reaction were heated under vacuum for30 minutes and purged with N2for10minutes.(无水反应装置)Part2:加料2.1:不同的顺序和表达2.1.1:A3L three-necked round bottom flask equipped with mechanical stirrer(or magnetic stirrer),addition funnel and thermometer(or Dean-Stock;drying tube)were charged with A(10mL,1mole),B(2g,mole)and C(50mL),2.1.1.1:a solution of D(10g,1mole)in E(20mL)was added dropwise (via addition funnel or syringe)at10oC(or while maintaining gentle reflux;while keeping inner temperature between10oC–30oC)under N2（液体滴加到反应液中）2.1.1.2:D(10g,1mole)was added in portions during a period of1hr (固体分批加入到反应液中)2.1.1.3:D(10g,1mole)and E(20mL)were added in turn.2.2:To a solution(mixture,suspension or slurry)of A(10mL,1mole) and B(2g,mole)in C(50mL)2.2.1:was added dropwise a solution of D(10g,1mole)in E(20mL)with stirring at10oC(or while maintaining gentle reflux;while keeping inner temperature between10oC–30oC)under N22.2.2:was added D(10g,1mole)in portions duringa period of1hr 2.2.3:were added D(10g,1mole)and E(20mL)in turn2.3:2.3.1:A solution of D(10g,1mole)in E(20mL)was added dropwise intoa solution(mixture or suspension)of A(10mL,1mole)and B(2g,mole) in C(50mL)at10oC(or while maintaining gentle reflux;while keeping inner temperature between10oC–30oC)under N2.2.3.2:D(10g,1mole)was added into a solution(mixture or suspension) of A(10mL,1mole)and B(2g,mole)in C(50mL)in portions2.3.3:D(10g,1mole)and E(20mL)were added into a solution(mixture or suspension)of A(10mL,1mole)and B(2g,mole)in C(50mL)in turn2.4:2.4.1:A solution of BuLi or BH3/THF(10mL,1mole,2.5M in hexane)was cannulated into addition funnel or into a solution A in solvent B2.4.2:A solution of BuLi or BH3/THF(10mL,1mole,2.5M in hexane)was added into a solution of A in solvent B via cannula,dropping funnel or syringe over a period of hrsPart3:反应3.1:无溶剂反应A(1g,1mol)and B(1g,1mol)were dissolved insolvent C,evaporated to dryness and heated for x hours at x oC3.2:催化量的反应A(20mL,142mmol)and catalytic amount(a traceamount or two drops)of B were added into a solution of C(4.549g,46.4mmol)in D(120mL)at0 oC3.3:闷罐反应或封管反应A solution of A(x g,x mol)in methanol(x mL)saturated with NH3(or other gas such as:CO,CO2,H2S)was stirred under50Psi at x oC for x hours in a50mL of sealed tube or autoclave.3.4:有气体参与的反应3.4.1:A solution of A(x g,x mol)in methanol(xmL)saturated with HCl was stirred at x℃.3.4.2:Ozone was bubbled into a solution of A(x g,x mol)in MeOH(x mL) at x oC for15minutes.After excess O3was purged by N2,Me2S(x mL)was added at x oC.3.4.3:Gas was bubbled into a solution of A(x g,xmol)and B(x g,x mol) in solvent C(x mL)at x oC for x hours.3.5:混合溶剂参与的反应3.5.1:To a solution of A(x g,x mol)in a mixture of solvent B(mL)and solvent C(x mL)(or a mixed solvent of B and C)was added D(x g,x mol) at x oC,the reaction mixture was allowed to stir(reflux or heat)for x hrs.3.5.2:To a solution of A(x g,x mol)in10:1aqueous acetone(x mL) was added B(x g,x mol)followed by addition of C(x g,x mol),the reaction mixture was allowed to stir(reflux or heat)for x hrs.3.6:分水器分水的反应3.6.1:A(x g,x mol)and B(x g,x mol)in benzene or toluene(x mL)were refluxed for x hours with azeotropical removal of water.3.6.2;A mixture of A,B and TsOH.H2O(56.91g,0.3mol)in toluene(400 mL)was heated to reflux and remove water by Dean-Stark trap.3.7:氢化反应To a solution of A(x g,x mol)in EtOH(x mL)was added Pd-C or Ra-Ni or Pd(OH)2/C(10%,x g)under N2.The suspension was degassed under vacuum and purged with H2several times.3.7.1:The mixture was stirred under H2(x psi)at x℃for x hours.[氢化瓶或高压釜]3.7.2:The mixture was stirred under H2balloon at x℃for x hours.[常压氢化如气球反应]3.7.3:A mixture of A(x g,x mol)and Ra-Ni(x g)in EtOH(x mL)was hydrogenated under50Psi of hydrogen pressure for xhours at room temperature.Part4:反应条件或过程描述4.1:The reaction mixture(solution or suspension)was stirred at5oC for 2hrs and then kept at room temperature(or ambienttemperature)for another2hrs(or overnight)4.2:The reaction mixture(solution or suspension)was refluxed(heated to reflux)or heated at60oC for2hrs(or overnight)4.3:The reaction mixture(solution or suspension)was allowed to reflux (or heat to reflux)for2hrs(or overnight)4.4:The reaction mixture(solution or suspension)was allowed to warm to temperature during2hrs and reflux(or heat toreflux)for2hrs(or overnight)Part5:反应监测5.1:Taking sample from the reaction mixture(solution or suspension)by dropping tube or syringe.After workup,check the reaction via TLC,LC-MS or HPLC etc..(预处理)5.2:反应状态或终点描述5.2.1:The reaction was complete(incomplete or messy)detected (determined or confirmed)by TLC(PE/EtOAc4:1),LC-MS,HPLC or NMR5.2.2:TLC(PE:EtOAc=1:1)or HPLC(107757-088-1)showed or indicated that the reaction was complete.5.2.3:TLC(PE:EtOAc=1:1)or HPLC(107757-088-1)showed the starting material was consumed completely.5.2.4:TLC(PE:EA=1:1)or HPLC(107757-088-1)showed the reaction didn’t work at all or most of starting material was still remained.5.2.5:The starting material was consumed completely,but no desired compound was detected or determined by MS(106657-078-1)or LC-MS (106657-078-1).5.2.6:Several spots were shown on TLC.5.2.7:Only a trace amount of desired compound was detected by MS (106657-078-1)or LC-MS(106657-078-1)or HPLC(106657-078-1)or TLC (PE:EtOAc=1:1).5.2.8:The desired compound could not be isolated,separated or purified by chromatography or prep.HPLC due to poor yield or poor solubility.5.2.9:1H NMR(106675-010-2)or MS confirmed the obtained(or isolated) compound is not the desired compound.The reaction was failed.Part6:反应淬灭6.1:An aqueous solution of A(10mL)was added dropwise into the reaction mixture once the reaction mixture(solution orsuspension)was allowed to warm(or cool)to-5oC or room temperature(ambient temperature).6.2:The hot(or cold)reaction mixture(solution orsuspension)was poured into water(ice water)or poured onto ice.6.3:The reaction mixture(solution or suspension)was concentrated (distilled)under reduced pressure(in vacuum)or evaporated to remove MeOH(THF;DMF etc.)or excess SOCl2(reagent).Then the reaction residue (or the residual)was diluted with solvent and poured into water(ice water) or poured onto ice.Part7:分液提取7.1:The residue was partitioned between ethylacetate(100mL)and1N aq. HCl(50mL).The separated organic layer was washed with water,dried over (Na2SO4or MgSO4)and evaporated to dryness.7.2:After quenching the reaction,the reaction mixture was poured into separatory funnel and separated.7.3:The aqueous layer(or phase)was extracted with organic solvent(40 mL)twice(or X times).The combined organic layers were(or the organic layers were combined and)washed with an aqueous solution of A(50mL) or water and dried over Na2SO4or MgSO4.7.4:The combined aqueous layers were extracted with solvent(40mL)twice (or X times)to remove neutral impurities.The aqueous phase was acidified (or basified)with aqueous HCl(or NaHCO3)till PH=X and extracted with organic solvent.7.5:The combined organic layers were(or theorganic layers were combined and)washed with an aqueous solution of A(50mL)or water and dried over Na2SO4or MgSO4.Part8:浓缩蒸发8.1:After filtration via filter paper or Celitepad,the organic layer (or extract)was concentrated under reduced pressure(or in vacuum)or evaporated to dryness to provide(afford;giveor yield)an oil(or foam) (which solidified on standing)or a white solid.8.2:The organic layer(or extract)was filtered and concentrated under reduced pressure(or in vacuum)or evaporated to dryness to provide (afford or give)A(10g,0.5mole)an oil(or foam)(which solidified on standing)or a white solid.8.3:After removal of solvent by evaporation or concentration,A(10g, 0.5mole)was obtained(or prepared)an oil(orfoam)(which solidified on standing)or a white solid.8.4:The extract in CH2Cl2was evaporated to dryness and then swapped with toluene to remove residual CH2Cl2.Part9:几种常见的后处理描述9.1:The reaction mixture or solution was concentrated to dryness.[适用于反应液不需要quench]9.2:After the reaction mixture was cooled to0℃,the reaction mixture was quenched by addition of xmL of H2O,followed by x mL of15%aqueous NaOH.After being stirred at room temperature for x hour,the solid was removed by filtration(orthe mixture was filtered)through Celite pad to remove by-product).The filtrate was concentrated to dryness to give crude product.[LiAlH4反应的经典后处理]9.3:The mixture was diluted with water(x mL),neutralized with solid K2CO3until no CO2was evolved.[适用于酸性反应液的后处理]9.4:The suspension was filtered through a pad of Celite or silica gel and the pad or filter cake was washed with EtOH(xmL×x).The combined filtrates were concentrated to dryness to give product(x g,x%)as.[适用氢化反应的后处理,或者难于过滤的反应液的后处理,但要注意的是这里需要的是滤液而不是固体才能添加助滤剂]9.5:The reaction mixture was poured into x mL of ice-water carefully and the organic layer or phase was separated.[产物在有机相里]9.6:The reaction mixture was poured into x mL of ice-water carefully and the aqueous phase was washed with Et2O(x mL×x)[产品在水相]and acidified with1NHCl to pH=3.The resulting precipitate was collected by filtration or the resulting solution was extracted with EA(x mL×x).9.7:The reaction mixture was filtered and the filter cake was washed with x mL of solvent,dried in vacuum to give or afford product.[这里需要的是固体而不是滤液]9.8:The reaction mixture was quenched with x mL of saturated aqueous NH4Cl. The resulting solution was extracted with EA(xmL×x).[适用于丁基锂等活泼金属有机物的后处理]9.10:The residue was triturated with ether and filtered to afford a white solid.(磨碎)9.11:The crude product was purified by prep.HPLC to give A as a colorless thick oil which was solidified on standing.(静止固化)9.12:After prep.HPLC purification,the eluent was concentrated or evaporated to remove organic solvents.The residual aqueous solution was lyophilized to give a white solid.(冷冻干燥)9.13:After concentration,the crude product was used directly for the next step without purification.Part10:产品的纯化10.1:The crude product was purified by silica gel chromatography eluted with PE:EtOAc=10:1to give product(x g,x%)as yellow solid.10.2:The crude product was purified by recrystallization(or recrystallized)from x solvent(x mL).10.3:The crude product was distilled in vacuum(xoC,x pressure)to afford pure product(x g,x%)as colorless liquid.10.4:The crude product was pre-purified by column chromatography followed by prep.HPLC purification or re-crystallization to afford pure product.。
英文版化学实验报告
英文版化学实验报告英文版化学实验报告IntroductionIn the field of chemistry, experimental reports play a crucial role in documenting and sharing scientific findings. The purpose of this article is to provide a comprehensive guide on how to write an effective English version of a chemistry experimental report. By following a structured approach and using appropriate language, scientists can effectively communicate their research findings to a wider audience.Experimental ProcedureThe experimental procedure section is an essential component of a chemistry report as it outlines the steps taken to conduct the experiment. In an English version of the report, it is important to use clear and concise language to describe each step. Additionally, it is crucial to include any specific measurements, equipment used, and any modifications made to the original procedure. This section should provide enough detail for readers to replicate the experiment.Results and Data AnalysisThe results and data analysis section is where the experimental findings are presented. When writing an English version of this section, it is important to use appropriate scientific terminology and units of measurement. Any tables, graphs, or figures should be clearly labeled and referred to in the text. Additionally, it isimportant to provide a thorough analysis of the data, discussing any trends, patterns, or anomalies observed.Discussion and ConclusionThe discussion and conclusion section is where the experimental results are interpreted and analyzed in the context of the research question or hypothesis. In an English version of this section, it is important to use logical and coherent language to present the findings. Any limitations or sources of error should be acknowledged, and suggestions for further research can be made. The conclusion should summarize the main findings and their significance.Safety ConsiderationsIn any chemistry experiment, safety considerations are of utmost importance. In an English version of the report, it is crucial to include a section dedicated to safety precautions taken during the experiment. This section should outline any hazardous materials used, safety equipment utilized, and any potential risks associated with the experiment. Clear and concise language should be used to ensure the reader understands the importance of safety protocols. ReferencesIn scientific research, it is essential to provide proper credit to the sources of information and ideas used. In an English version of the report, a references section should be included to list all the sources consulted during the experiment. The references should be formatted according to the appropriate citation style, such as APA or MLA. It is important to accurately cite all sources,including books, journal articles, and online resources, without including any direct links.ConclusionWriting an English version of a chemistry experimental report requires attention to detail and clear communication. By following a structured approach and using appropriate scientific terminology, researchers can effectively present their findings to a wider audience. The experimental procedure, results and data analysis, discussion and conclusion, safety considerations, and references sections are all crucial components of a comprehensive chemistry report. By adhering to these guidelines, scientists can contribute to the advancement of scientific knowledge and promote effective communication within the scientific community.。
英文有机化学实验-甲基橙的合成
H2N
SO3H + NaOH
H2N
SO3Na + H2O
Sulfanilic acid, insoluble in acid solution and soluble in basic solution, is an amphoteric compound（两性化合物）.
Its acidity is slightly stronger than its basicity.
⑤ Concentrated hydrochloride acid
⑥ Glacial acetic acid（冰乙酸 FW 60）7.2mL（7.5g 0.125mol）
⑦ Sodium chloride
➢4 Procedure实验流程 4.1
Sulfanilic acid （1.7g，0.01mol）
✓1.2 Master the technique of recrystallization.
➢2. Principle
Reactions
H2N
NaOH SO3H
H2N
SO3Na NaNO2, HCl
HO3S
N2Cl
N(CH3)2 HAc
HO3S
NN
N(CH3)2
NaOH
NaO3S
NN
N(CH3)2
有机化学实验 Experimental Organic Chemistry
Synthesis of Methyl Orange（甲基橙的合成）
Synthesis of Methyl Orange
（甲基橙的合成）
➢1. Purpose
✓1.1 Study the principle and method of methyl orange from diazotized sulfanilic acid （对氨基苯磺酸重氮盐） and N,N-dimethylaniline by the diazo coupling reaction （重氮化偶联反应）。
化学实验英语作文
化学实验英语作文Title: A Chemistry Experiment: Synthesis of Aspirin。
Chemistry experiments are not only fascinating but also crucial for understanding the principles of chemical reactions and their applications in real-life scenarios. In this essay, we delve into the synthesis of aspirin, a commonly used medication, detailing the procedure, observations, and significance of the experiment.The synthesis of aspirin involves the reaction between salicylic acid and acetic anhydride in the presence of a catalyst, typically sulfuric acid. The reaction yields aspirin (acetylsalicylic acid) and acetic acid as byproducts. The process can be summarized by the following chemical equation:\[C_7H_6O_3 + (CH_3CO)_2O \rightarrow C_9H_8O_4 +CH_3COOH\]This reaction is a classic example of esterification, wherein an alcohol (the -OH group in salicylic acid) reacts with a carboxylic acid derivative (acetic anhydride) toform an ester (aspirin) and a carboxylic acid (acetic acid).The experimental procedure begins with measuring the required amounts of salicylic acid and acetic anhydride. These are then mixed in a flask along with a few drops of concentrated sulfuric acid, which acts as a catalyst. The mixture is gently heated under reflux, allowing thereaction to proceed efficiently. Refluxing prevents theloss of volatile reactants and ensures a higher yield ofthe desired product.During the reaction, one can observe changes in the appearance of the mixture. Initially, the mixture may be a white powder or small crystals of salicylic acid. As the reaction progresses, the mixture becomes more homogeneous, and the formation of aspirin can be visually confirmed bythe appearance of white crystals. The reaction is typically complete within a couple of hours.After the completion of the reaction, the mixture is cooled, and the aspirin crystals are collected via filtration. The crude product obtained may still contain impurities, such as unreacted starting materials or side products. Purification techniques, such as recrystallization, can be employed to obtain pure aspirin crystals.The purified aspirin crystals are then dried and weighed to determine the yield of the reaction. Theoretical yield calculations can be performed based on the stoichiometry of the reaction, allowing for the comparison of actual versus expected yields. Factors affecting yield, such as the purity of reagents, reaction conditions, and the efficiency of purification techniques, can be analyzed and discussed.The significance of this experiment extends beyond the synthesis of a common pharmaceutical compound. It provides insights into fundamental chemical principles, such as stoichiometry, kinetics, and the role of catalysts in chemical reactions. Moreover, it highlights the importanceof practical skills, such as accurate measurement, observation, and data analysis, in experimental chemistry.Furthermore, the synthesis of aspirin illustrates the application of chemistry in everyday life. Aspirin, withits analgesic, anti-inflammatory, and antipyretic properties, is one of the most widely used medications worldwide. Understanding its synthesis not only enhances our knowledge of chemistry but also underscores the importance of pharmaceutical chemistry in healthcare.In conclusion, the synthesis of aspirin is a classic chemistry experiment that offers valuable insights into chemical reactions, purification techniques, and the application of chemistry in the synthesis of pharmaceutical compounds. Through hands-on experience and analysis, students can deepen their understanding of chemistry while appreciating the relevance of chemical principles in society.。
化学实验报告 英文版
化学实验报告英文版Chemical Experiment ReportAbstract:This report presents the findings and analysis of a chemical experiment conducted to investigate the effects of temperature on the rate of reaction between hydrochloric acid (HCl) and sodium thiosulfate (Na2S2O3). The experiment involved varying the temperature of the reactants and measuring the time taken for the reaction to occur. The results indicate a clear correlation between temperature and reaction rate, with higher temperatures leading to faster reactions.Introduction:Chemical reactions are influenced by various factors, including temperature, concentration, and catalysts. The purpose of this experiment was to examine the impact of temperature on the rate of a chemical reaction. The reaction between hydrochloric acid and sodium thiosulfate was chosen due to its well-documented reaction kinetics.Methodology:The experiment was conducted using a simple setup consisting of a conical flask, a stopwatch, and a thermometer. Initially, 50 mL of 1 M hydrochloric acid was poured into the flask, followed by the addition of 10 mL of 0.1 M sodium thiosulfate. The stopwatch was started as soon as the sodium thiosulfate was added, and the time was recorded when the solution turned opaque due to theformation of a yellow precipitate. The experiment was repeated at different temperatures by immersing the flask in water baths maintained at specific temperatures.Results and Discussion:The experiment was carried out at four different temperatures: 20°C, 30°C, 40°C, and 50°C. The average reaction times at each temperature were recorded and are presented in Table 1 below:Temperature (°C) Reaction Time (s)20 12030 9040 7050 50Table 1: Average reaction times at different temperaturesFrom the results, it is evident that as the temperature increased, the reaction time decreased. This indicates that higher temperatures accelerate the rate of the reaction between hydrochloric acid and sodium thiosulfate. The relationship between temperature and reaction rate can be explained by the collision theory. According to this theory, particles must collide with sufficient energy to overcome the activation energy barrier for a reaction to occur. As temperature increases, the average kinetic energy of the particles also increases, leading to more frequent and energetic collisions.Furthermore, the reaction between hydrochloric acid and sodium thiosulfate isexothermic, meaning it releases heat. As the reaction progresses, the released heat raises the temperature of the solution, further increasing the reaction rate. This positive feedback mechanism contributes to the observed trend of faster reactions at higher temperatures.Conclusion:In conclusion, this experiment demonstrates the significant influence of temperature on the rate of the reaction between hydrochloric acid and sodium thiosulfate. As temperature increases, the reaction time decreases due to more energetic collisions and the exothermic nature of the reaction. These findings have practical implications in various fields, such as industrial chemistry and environmental science, where controlling reaction rates is crucial.Further research could explore the effect of temperature on other chemical reactions and investigate the specific activation energy values for different reactants. Additionally, studying the impact of other factors, such as concentration and catalysts, on reaction rates would provide a comprehensive understanding of chemical kinetics.。
有机化学实验 英文
有机化学实验英文Organic Chemistry Experiment.Organic chemistry experiments are an essential part of the study of organic compounds and their properties. These experiments involve the synthesis, purification, and characterization of various organic compounds, as well as the study of their reactivity and behavior under different conditions. Students typically perform a wide range of experiments, including the synthesis of simple organic compounds, the identification of unknown compounds, and the study of organic reactions and mechanisms.In the laboratory, students may be tasked with carrying out procedures such as distillation, extraction, chromatography, and spectroscopic analysis to isolate and characterize organic compounds. They may also explore the principles of organic synthesis by performing reactions such as esterification, Grignard reactions, and Friedel-Crafts alkylation.Furthermore, safety considerations and proper handling of chemicals are important aspects of organic chemistry experiments. Students are expected to adhere to strict safety protocols and use appropriate personal protective equipment to minimize the risk of accidents or exposure to hazardous substances.Overall, organic chemistry experiments provide students with hands-on experience and a deeper understanding of the principles and applications of organic chemistry. Through these experiments, students gain practical skills, develop critical thinking abilities, and learn to apply theoretical knowledge to real-world problems in the field of organic chemistry.。
化学实验报告 英文
化学实验报告英文Chemistry Experiment ReportIntroduction:In the field of science, experiments play a crucial role in deepening our understanding of various phenomena. This report aims to present the findings and observations from a recent chemistry experiment conducted in the laboratory. The experiment focused on the reaction between two chemicals and explored the effects of different variables on the reaction rate.Experimental Procedure:The experiment began by carefully measuring and preparing the required chemicals: sodium hydroxide (NaOH) and hydrochloric acid (HCl). These chemicals were chosen due to their well-known reaction, which produces salt and water. The experiment aimed to investigate how factors such as concentration, temperature, and catalysts influenced the reaction rate.To start the experiment, a fixed volume of NaOH solution was poured into a conical flask. The concentration of NaOH was varied in different trials, ranging from 0.1 M to 1.0 M. The flask was placed on a magnetic stirrer to ensure uniform mixing. Then, a burette was used to add a fixed volume of HCl solution to the flask. The reaction was monitored by observing the formation of a white precipitate, indicating the completion of the reaction.Results and Discussion:The experiment revealed several interesting findings. Firstly, it was observed thatas the concentration of NaOH increased, the reaction rate also increased. This can be attributed to the higher number of NaOH particles available to react with HCl, leading to more frequent collisions and faster reaction kinetics. Furthermore, the effect of temperature on the reaction rate was investigated. It was found that as the temperature increased, the reaction rate also increased. This can be explained by the kinetic theory of gases, which states that at higher temperatures, particles possess greater kinetic energy and move more rapidly. Consequently, more collisions occur, resulting in a faster reaction rate.The influence of catalysts on the reaction rate was also examined. A small amount of catalyst, in the form of manganese(IV) oxide (MnO2), was added to the reaction mixture. It was observed that the presence of the catalyst significantly increased the reaction rate. Catalysts provide an alternative reaction pathway with lower activation energy, allowing the reaction to proceed more rapidly.Conclusion:In conclusion, this experiment provided valuable insights into the factors affecting the reaction rate between NaOH and HCl. The concentration of the reactants, temperature, and the presence of catalysts were identified as key variables influencing the rate of the reaction. Understanding these factors is crucial in various industrial processes where reaction rates play a vital role.It is important to note that this experiment focused on a specific reaction and variables. Further research could explore the effects of other factors, such aspressure and surface area, on the reaction rate. Additionally, investigating the reaction kinetics using mathematical models could provide a more comprehensive understanding of the underlying mechanisms.Overall, this experiment highlights the significance of chemistry in unraveling the mysteries of the natural world. By conducting experiments and analyzing the results, scientists can uncover fundamental principles that govern chemical reactions, paving the way for advancements in various fields, including medicine, energy, and materials science.。
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无论中文还是英文的实验记录都至少应该描述以下六点内容，同时实验记录上还应该注 明原料的来源，反应现象，分析数据，产品去向等相关细节。 实验装置 投料 反应过程 反应结束 淬灭处理 纯化产品
3 基本表达
3.1 实验装置
例句：一个装有机械搅拌的三口圆底烧瓶。 A three (necked-round bottom) Morton flask which was equipped with mechanical stirrer （magnetic stirrer, addition funnel, thermometer，Dean-Stark，drying tube，syringe）. 例句：实验前所有实验中要使用的烧瓶都需要在真空状态下加热半小时并用氮气吹 10 分钟。 All flasks which were used in reaction were heated under vacuum for 30 minutes and purged with N2 for 10 minutes.
3.5 淬灭处理
例句：将反应液降到室温，滴加 NaHCO3 水溶液淬灭反应 An aqueous solution of NaHCO3 was added dropwise into the reaction mixture once the reaction mixture(solution) (suspension) could warm(cool) to room(ambient) temperature. 例句：淬灭反应后，将反应液倒入分液漏斗分离 After quenching the reaction, the reaction mixture was poured into separatory funnel and separated. 例句：将热的反应液倒入冰水中淬灭 The hot reaction mixture was poured (onto ice) into ice water. 例句：将反应液减压蒸去 DCM 和多余的 SOCl2，然后将剩下的用 EtOH 稀释并倒入水中。 The reaction mixture was concentrated(distilled)under reduced pressure(in vacuum) (evaporated) to remove DCM and excess SOCl2，then the reaction residue(the residual) was diluted with EtOH and poured into water. 例句：将残渣用 EA 稀释，1N 盐酸洗涤，清水洗涤，Na2SO4 干燥后旋干 The residual was partitioned between EA and 1N aqueous HCl. The organic layer was washed with water, dried over Na2SO4 and evaporated dryness. 例句：水层用 EA 萃取两次，合并有机层用盐水洗涤，Na2SO4 干燥。 The aqueous layer(phase) was extracted with EA twice. The combined organic layers were washed with brine and dried over Na2SO4. 例句：合并水层，用 EA 萃取除去杂质后，将水层用盐酸调节 pH 至 3~4，用 EA 萃取 The combined aqueous layers were extracted with EA twice to remove neutral impurities. The aqueous phase was acidified(basified) with HCl till PH=3~4 and extracted with EA. 例句：用滤纸过滤，减压浓缩除去有机溶剂得到白色固体 After filtration via filter paper (celite-pad), the organic layer was concentrated under reduced pressure to dryness to provide(afford, give, yield) white solid(oil, foam) (which solidified on standing). 例句：通过蒸馏或者减压浓缩除去溶剂后得到白色固体 After removal of solvent by evaporation or concentration, the desired compound was obtained(prepared) a white solid.
3.2 投料
例句：将丝氨酸，水，碳酸氢钠加入到一个装有磁力搅拌器，温度计，滴液漏斗的三口瓶中。 A three necked-round bottom flask which was equipped with magnetic stirrer, addition funnel and thermometer which was charged with L-Serine, H2O, NaHCO3.
3.4 反应结束
例句：TLC 结果表明反应结束 The reaction was complete (incomplete) (messy) detected (determined) (confirmed) by TLC(LC-MS) (HPLC). 例句：HPLC 结果表明反应结束 HPLC showed(indicated) that the reaction was complete. 例句：HPLC 表明原料已经完全反应 HPLC showed(indicated) that the starting material was consumed completely. 例句：HPLC 表明反应没有发生，大多数原料没有反应 HPLC showed(indicated) that the reaction didn’t work at all and the most of starting material was remained.
3.3 反应过程
例句：反应液置于 50℃下保温反应两小时后，室温反应过夜 16 小时后用吸管取样通过 TLC 监控情况。 The reaction mixture was stirred at 50℃ for 2 hours and then kept at room temperature for another 16 hours overnight).Taking sample form the reaction mixture by dropping tube(syringe), check the reaction via TLC(LC-MS) (HPLC). 例句：将反应液在 50℃小保温反应 16h The reaction mixture(suspension)(solution)was stirred at 50℃ for 16 hour
例句：LC-MS 表明虽然原料完全被消耗，但是没有观察到目标产品的离子响应 The starting material was consumed completely but no desired compound was detected(determined) by LC-MS. 例句：只有少量的目标产品被 LC-MS 检测到 Only a trace amount of desired compound was detected bu LC-MS. 例句：目标产物的收率太低导致无法通过柱层析分离 The desired compound could not be isolated(separated) (purified) by chromatography(prepHPLC) due to pty). 例句：HNMR 表明分离的化合物不是目标产物,反应失败。 HNMR confirmed (indicated) that the isolated(obtained) compound is not the desired compound. The reaction was failed.
有机化学实验文档
1 前言
科学实验原始记录主要用于证明实验具有可重复性，详细的实验记录也是表达研究成果 的依据，所以无论是中文还是外文的实验文档都应该准确详细的描述研究过程，目前国内有 机化学学术领域可参考的中文文档太少，已有的中文文献普遍存在实验难以重复，高质量的 中文文献可遇不可求，但发布在权威化学期刊的文献大多质量较高，这些权威期刊都是用英 文发表，即使国内的研究成果也是通过英文发表在这些期刊上，基于目前这种尴尬的局面， 在有机化学领域读写英文文档成为从业者的基本技能。
例句：在 10℃氮气保护下滴加三乙胺的二氯甲烷溶液 A solution of TEA in DCM was added dropwise via(by) addition funnel(syringe) at -10℃(while keeping inner temperature between -10℃~0℃) (while maintaining gentle reflux)under N2. 例句：1h 内分批加入 NaH NaH was added in portions during a period of 1 hours 例句：依次加入(Boc)2O 和 Pyridine (Boc)2O and Pyridine were added in turn. 例句：将 DMAP 和 HOBt 溶解在 DCM 中 To a solution(mixture,slurry,suspension) of DMAP and HOBt in DCM. 例句：在 0℃下将 TFAA 的 DCM 溶液滴加到 Fmoc-Asn-OH 的 DCM 溶液中 A solution of TFAA in DCM was added dropwise into a solution of Fmoc-Asn-OH in DCM at 0℃ while keeping inner temperature between 0℃~5℃. 例句：在 0℃下将 NaBH4 分批加入到化合物 1 的甲醇溶液中 NaBH4 was added into a solution of compound 1 in MeOH in portions(in turn) at 0℃. 例句：在 0℃下通过导管将 n-BuLi 的 hexane 溶液加入到反应液中 A solution of n-BuLi in hexane was cannulated into the reaction solution at 0℃. A solution of n-BuLi in hexane was added into the reaction solution via(by) cannula(dropping funnel)(syringe) at 0℃.