ASTM D1193-2006试剂纯水规范

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水质指标测定方法手册

水质指标测定方法手册第一部分总则1.1 目的此手册的目的是规范化验室分析工作，保证实验条件、仪器设备、人员操作符合国家标准的规定，确保化验室检验的准确性。

1.2 宗旨此手册的宗旨是以先进的、科学的分析方法，以准确的分析数据来帮助操作员工了解本废水处理系统实际的运行情况视实调整，以取得最好的工艺处理效果，达到指导的目的。

1.3 依据本手册介绍的所有指标检测方法均使用国家标准方法或是行业规定标准方法；第二部分注意事项1.1进入实验室工作和学习的人员需遵守实验室安全管理规章制度，克服麻痹大意思想，掌握基本的安全知识和救助知识，非工作需要未经许可不得擅自进入实验室。

1.2工作人员进入实验室后需着工作服，严格实行检验方法标准，遵守操作规程和一切规章制度不得擅自修改。

1.3 水质分析过程需用到浓硫酸，浓盐酸、硫酸汞等腐蚀、有毒药品，这些危险品及有毒药品要按规定设专用库房，做到专室专柜储存，并指定专人、双人双锁妥善保管，严格以上物品的管理；1.4 开启使用硫酸、盐酸等腐蚀刺激性药品时，要带上耐酸手套和防护眼镜，先用湿布盖上瓶口再开动瓶塞，以防溅出，烧伤眼睛和皮肤等。

因为浓盐酸是具有挥发性的，操作应在通风橱内进行。

1.5 为确保分析结果的准确性，建议购买环境标准样品，化验室分析人员定期拿环境标准样品进行实际测试，将测试结果与参考值进行比较。

1.6 实验人员严格按规定方法取样、制样、留样，经常检查有关设备的取样管等，确保取样有代表性，留样标记要清楚。

1.7 正确使用并维护好相关仪器，定期对其进行校正。

1.8 测定方法用到标准曲线的，严格上要求每次重新配制药品后需重新绘制标准曲线。

第三部分操作手册水质篇第一章、PH的测定 (4)第二章、悬浮物（SS）的测定 (8)第三章、色度的测定 (10)第四章、化学需氧量（COD）的测定 (11)第五章、五日生化需氧量（BOD5）的测定 (14)第六章、溶解氧的测定 (18)第七章、挥发性脂肪酸（VFA）的测定 (21)第八章、总氮（TN）、总磷（TP）的测定 (23)第九章、氨氮的测定 (34)污泥篇第一章、颗粒污泥总浓度（TSS）、挥发性污泥浓度（VSS）、灰分测定 (40)第二章、比产甲烷活性的测定 (41)第三章、好氧活性污泥的测定 (44)水质篇第一章、PH的测定玻璃电极法1、适用范围1.1、本法适用于饮用水、地面水及工业废水pH值的测定。

水和盐水比重标准测试方法(中文版)

水和盐水比重标准测试方法1.适用范围这些方法包含了如下不含可分离油的水和盐水的比重的测定：节次测试方法A—比重瓶法 7至11测试方法B—天平法 12至16测试方法C—锥形瓶法 17至20测试方法D—液体比重计法 21至251.2 方法A和B适用于清水或含适量特殊物质的水。

方法B更适合做海水样品或盐水，法B比具有相同适用范围的法D具有更高的灵敏度。

方法C适用于分析含泥浆或淤泥的水。

1.3 使用者有责任确保该方法用于未经测试基质的水的有效性。

1.4 该方法在22℃测试了数值介于1.0252至1.2299范围的比重（表1－4）；所有的数据在15.6℃（60 o F ）经过了校正。

1.5该标准不旨在阐述所有的安全问题, 只是在和使用方法有联系时稍有提及。

使用者有责任在使用前确定相关的安全与健康措施并确定常规的使用范围。

2．参考文献2.1 ASTM标准D1066试样蒸汽操作2D1129 关于水的术语2D1193 试剂水的规范2D3370 封闭管道中试样水的操作2E1 ASTM 温度计的规范3．专业术语3.1定义：3.1.1盐水——含有浓度约大于30000mg/L的可溶物质的水。

3.1.2有关该方法中使用的术语的定义，见术语D1129。

4．用途及重要性4.1比重是和密度和粘度相关的液体的一个重要的性质。

和一个标准液通常是水相比较，比重可以确定一种液体在一定温度下的性质。

这可以使使用者确定测试液比标准液轻还是重。

5．试剂5.1水的纯度——若没有指明，所涉及的水均是符合类型II，D1193规范的试剂水。

6．取样6.1按操作D3370和D1066收集试样。

6.2考虑到缺少取污泥试样的标准检测方法，没有提及取该类物质的方法。

测试方法A—比重瓶法7．试验方法概要7.1 将试样引入比重瓶，在期望的温度下稳定，称量。

通过该重量值和先前确定的在同样的温度下、将该比重瓶充满试剂水的重量值计算比重。

8．仪器的准备8.1 水浴——恒温水浴保持温度在15.6±1℃（60±1.8 o F）。

分析实验室用水ppt课件

实验室废水应按照不同类型进行分类收集，避免不同性质废水的混合，降低处理难度。
废水回收利用
对于可回收利用的废水，应进行适当的处理后再利用，实现废水资源化。
实验室废水的处理与排放
处理方法
根据废水的性质和污染物种类，选择合适的处理方法，如物理处理、化学处理、生物处理等。
处理效果评估
对处理后的废水进行质量评估，确保水质达到国家或地方规定的排放标准。
膜分离技术
采用超滤、纳滤、反渗透等膜分离技术，实现实验室用水的高效净化与分离。
智能化处理技术
结合物联网、大数据等技术，实现实验室用水处理过程的自动化、智能化管理，提高处理效率。
实验室用水管理模式创新展望
用水定额管理
制定实验室用水定额标准，合理分配水资源，促进节约用水。
水资源循环利用
建立实验室内部的水资源循环利用系统，减少废水排放，提高水
反渗透法
利用半透膜的选择透过性，使水分子通过而杂质被截留，得到高纯度
的水。
电渗析法
在外加电场作用下，利用离子交换膜的选择透过性，去除水中的离子
和杂质。
实验室用水的储存与输送
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储存容器
使用清洁、密封良好的容器储存实验室用水，避免污染和蒸
发损失。
定期清洗
定期对储存容器和输送管道进行清洗和消毒，确保水质不受
排放要求
实验室废水在排放前必须满足相关法规和标准的要求，不得随意排放未经处理的废水。
监管与记录
实验室应建立废水处理和排放的监管制度，对废水处理过程进行详细记录，以备查验。
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实验室用水的未来发展趋势与展望
实验室用水处理技术发展趋势

ASTM-D类最新标准目录(一)

ASTM-D类最新标准目录(一)ASTM D类最新标准目录( 一）D4-86(2004) 沥青含量试验方法D5-06e1 沥青材料的渗透性试验方法D6-95(2000)e1 油及沥青混合物加热损失试验方法D8-02 与道路和路面材料相关的术语D9-05 与木材相关的术语D12-88(1998) 未加工的桐油D13-02 松节油规范D16-03 与涂料、清漆、亮漆和有关产品相关的术语D20-03 路面焦油的蒸馏试验方法D25-99(2005) 圆木桩D29-98 虫胶树脂的抽样和试验方法D34-91(2003) 白颜料化学分析指南D36-95(2000)e1 沥青软化点试验方法(沥青软化点测定器)D38-94(2000)e1 木材防腐剂的抽样试验方法D41-05 铺屋面、防潮及防水用沥青底层D43-00 屋顶、防潮及防水材料用杂酚油底漆D49-83(2002) 铅丹的化学分析D50-90(2005) 含铁和锰的黄色、橙色、红色和褐色涂料的化学分析试验方法D56-05 泰格密闭闪点试验器测定闪点的试验方法D61-75(2004) 硬沥青的软化点的试验方法(水中方块试验法)D69-01 磨擦带的试验方法D70-03 半固态沥青材料的比重和密度的试验方法D71-94(2004) 固体硬沥青和地沥青的相对密度试验方法(变位法)D75-03 集料的抽样D76-99(2005) 纺织材料的抗拉试验机D79-86(2004) 氧化锌颜料D81-87(2003) 碱性碳酸盐铅白颜料D83-84(2002) 铅丹颜料D85-05 赭色颜料规范D86-05 大气压下石油产品蒸馏试验方法D87-04 石蜡熔点的试验方法(冷却曲线)D88-94(2005) 赛波特粘度的试验方法D91-02 润滑油的沉淀值试验方法D92-05a 用克利夫兰德开杯法测定石油产品的闪点和燃点的试验方法D93-02a 用潘斯基-马丁斯仪闭杯闪点测定器测定闪点的试验方法D94-02 石油产品的皂化值试验方法D95-05e1 蒸馏法测定石油产品及沥青材料中水的试验方法D97-05a 石油的倾点的试验方法D98-05 氯化钙D113-99 沥青材料的延展性的试验方法D115-02 电绝缘用含清漆试验溶剂的试验方法D116-86(2006) 电气设备用上釉陶瓷材料的试验D117-02 产自石油的电绝缘油的试验方法和规范导则D120-02a 橡胶绝缘手套D121-05 煤和焦炭术语D123-03 与纺织材料相关的术语D124-88(1998) 脱胶的豆油D126-87(2002) 含铬酸铅和氧化铬绿的黄、橙和绿色颜料的化学分析方法D127-05 石油蜡包括凡士林滴熔点的试验方法D128-98(2003)e1 润滑脂分析试验方法D129-00(2005) 石油产品中硫含量试验方法(通用氧弹法)D130-04e1 用铜条变色法检测石油产品对铜腐蚀性的测试方法D139-95(2001)e1 沥青材料浮选试验的检测方法D140-01 沥青材料的抽样D143-94(2000)e1 洁净木材小样品的试验D146-04 防水与屋面材料用沥青浸渍的油毡和编织物的抽样与试验方法D149-97a(2004) 固体电绝缘材料在工业电源频率下的介电击穿电压和介电强度的试验方法D150-98(2004) 固体电绝缘材料的(恒久电介质)的交流损耗特性和介电常数的测试方法D153-84(2003) 颜料比重测试方法D154-85(2001) 清漆试验D156-02e1 石油产品赛波特比测试方法(赛波特比色计法)D167-93(2004)e1 块焦比重和孔隙度的试验方法D168-94(2000) 杂酚油焦炭渣的测试方法D173-03 屋顶和防水材料用饱和沥青棉织物D176-00 电绝缘用固体充填化合物与浸渍剂的试验方法D178-01(2005) 橡胶绝缘垫子D185-84(1999 颜料,糊剂及涂料中粗颗粒的试验方法D187-94(2003)e1 煤油燃烧质量的测试方法D189-05 石油产品康拉孙残碳测试方法D197-87(2002) 粉煤的取样方法与细度试验方法D198-05a 结构尺寸木料静力试验法D202-97(2002)e1 电绝缘用未浸渍纸的抽样和试验方法D204-02 缝线的测试方法D209-81(2003) 灯黑颜料D210-05 骨炭颜料D211-67(2002) 铬黄和铬橙颜料D215-91(2002) 白色亚麻籽油涂料的化学分析D217-02 润滑剂针入度的测试方法D225-04 表面有矿物颗粒的沥青屋面板D226-06 铺顶和防水用沥青饱和有机毡D227-03 铺顶和防水用焦油沥青饱和有机毡D228-06 沥青屋面卷材,盖板和瓦的试验方法D229-01 电绝缘用硬质薄板及板材的试验方法D233-02 松脂的抽样和测试试验方法D234-82(1998) 生亚麻子油D235-02 矿物溶剂油(石油溶液油)(烃干洗溶液)规格D237-57(1997) 橙色紫胶和其他虫胶D240-02 弹式量热器测定液烃燃料燃烧热的试验方法D242-04 沥青铺路混合料用矿物填料D243-02 规定残渣渗透性测试方法D244-04 乳化沥青的测试方法D245-06 制定目测分等木材的结构等级及有关允许性能的规程D246-04 杂酚油和杂酚油-煤焦油溶液的蒸馏试验方法D256-06 塑料及电绝缘材料的抗冲击性的测试方法D257-99(2005) 绝缘材料的直流电阻或电导的试验方法D260-86(2001) 熟亚麻籽油D261-75(1999) 铁蓝颜料D262-81(1999) 群青蓝颜料D263-05 氧化铬绿颜料D267-82(2003) 黄青铜粉规格D268-01 涂料及其相关涂层和原料用挥发性溶剂及化学中间体的抽样和测试D269-97(2002) 松香和松香衍生物中不溶物的试验方法D276-00a 纺织品中纤维的鉴定方法(AATCC方法20)D279-02 颜料渗出的试验方法D280-01 颜料吸收的水份(及试验条件下挥发的其他物质)的测试方法D281-95(2002) 用刮刀磨损法测定颜料油吸附性的试验方法D283-84(1999) 一氧化铜和铜涂料化学分析试验方法D287-92(2006) 原油和石油产品API比重的试验方法(液体比重计法)D291-86(2002) 烟煤立方英尺重量的试验方法D293-93(2004) 焦炭筛析分析试验方法D295-99(2004) 电绝缘用棉质漆布的试验方法D297-93(2002)e2 橡胶制品的测试方法.化学方法D299-04e1 石棉纱的标准规范D301-95(2004) 可溶性硝化纤维素的试验方法D304-05 n-丁醇(丁醇)D305-84(2003) 黑色涂料中的溶剂萃取材料的试验方法D312-00 屋顶用沥青D315-95(2004)e1 机织石棉带的标准规范D319-04 合成的戊醇D322-97(2002)e1 蒸馏法测定汽油发动机废机油中汽油稀释剂的试验方法D323-99a 石油产品蒸气压力的测试方法D329-02 丙酮D330-93(2001) 2-丁氧基乙醇D331-05 2-乙氧基乙醇D332-87(2004) 白色颜料着色力的试验方法D333-01 透明漆和着色漆的试验方法D341-03 液体石油产品粘度-温度关系曲线图D344-97(2004) 用擦试外规评定法对涂料相对遮盖力的测试方法D345-02 道路和结构用氯化钙的抽样和试验方法D346-04e1 实验室分析用焦炭试样的收集和制备e Equivalent of SoilsD427-04 用水银法测量土壤收缩系数的测试方法 Test Method for Shrinkage Factors ofSoil s by the Mercury MethodD429-03e1 橡胶特性与硬质基底粘附性的试验方法 Standard Test Methods for RubberPro perty—Adhesion to Rigid SubstratesD430-06 橡胶变质的动态疲劳试验方法 Standard Test Methods for RubberDeterioration-Dynamic FatigueD434-95 Standard Test Method for Resistance toSlippage of Yarns in Woven Fabrics Using a Standard SeamD440-86(2002) 煤的跌落粉碎试验 Standard Test Method of Drop ShatterTest for Coal D441-86(2002) 煤的滚筒试验 Standard Test Method of Tumbler Test for CoalD444-88(2003) 锌黄颜料(铬酸锌黄)的化学分析方法 Standard Test Methods for Chemical Analysis of Zinc YellowPigment (Zinc Chromate Yellow)D445-06 透明和不透明液体运动粘度的测试方法.(包括动态粘度的计算) Standard Test Method for Kinematic Viscosity ofTransparent and Opaque Liquids (and the Calculation of Dyn amicViscosity)D446-06 玻璃毛细管运动粘度计操作说明书和规范 Standard Specifications and OperatingI nstructions for Glass Capillary Kinematic ViscometersD448-03a 道路和桥梁建筑的集料尺寸分类 Standard Classification for Sizes ofAggregate for Road and Bridge ConstructionD449-03 防潮和防水用沥青规范 Standard Specification for AsphaltUsed in Dampproofi ng and WaterproofingD450-96(2006) 铺屋面,防潮与防水用硬煤沥青 Standard Specification for Coal-TarPitch Used in Roofing, Dampproofing, and WaterproofingD451-91(2002) 沥青屋顶制品用粒状矿物铺面材料筛分分析试验方法 Standard Test Method for SieveAnalysis of Granular Mineral Surfacing For Asphalt RoofingProductsD452-91(2002) 沥青层面制品表面修整用非粒状矿物的筛分试验方法 Standard Test Method for SieveAnalysis of Surfacing for Asphalt Roofing ProductsD453-94(2000)e1 杂酚油-煤焦油溶液中焦油酸含量的测试方法 Standard Test Method for Tar Acids inCreosote-Coal Tar SolutionsD454-04 用加热及空气压力测定橡胶变质的试验方法 Standard Test Method for RubberDet erioration by Heat and Air PressureD459-00 肥皂和其它洗涤剂的术语规范 Standard Terminology Relating toSoaps and Oth er DetergentsD460-91(2005) 肥皂和其它洗涤剂粒度的试验方法 Standard Test Methods for Samplinga nd Chemical Analysis of Soaps and Soap ProductsD464-05 松脂油产品包括妥尔油和其他相关产品的皂化值的试验方法 Standard Test Methods for Saponification Number of Naval Store Products Including Tall Oil and Other Relate d ProductsD465-05 松脂制品包括妥尔油及其它相关产品酸值的试验方法 Standard Test Methods for A cid Numberof Naval Stores Products Including Tall Oil and Other RelatedProductsD470-05 电线和电缆用交联绝缘与套管的测试方法 Standard Test Methods for Crosslinked Insulations and Jackets for Wire and CableD471-98e2 液体对橡胶性能影响的测试方法 Standard Test Method for RubberProperty-E ffect of LiquidsD473-02 萃取法测定原油和燃料油中沉积物的试验方法 Standard Test Method for Sedimen t inCrude Oils and Fuel Oils by the Extraction MethodD476-00(2005) 二氧化钛颜料规范 Standard Classification for DryPigmentary Titanium Dioxide ProductsD478-02 锌黄(铬酸锌)颜料 Standard Specificationfor Zinc Yellow (Zinc Chromate) Pig mentsD480-88(2003) 铝粉和铝粉浆的抽样和试验方法 Standard Test Methods for Samplingand Testing of Flaked Aluminum Powders and PastesD482-03 石油产品灰分的测试方法 Standard Test Method for Ash fromPetroleum Produ ctsD483-04 石油制植物喷洒油不磺化残渣的试验方法 Standard Test Method for Unsulfonate dResidue of Petroleum Plant Spray OilsD490-92(2005) 道路柏油 Standard Specification for Road TarD494-04 Standard Test Method for Acetone Extraction ofPhenolic Molded or Laminat ed Products Standard TestMethod for Acetone Extraction of Phenolic Molded or Lami natedProductsD495-99(2004) 固体电绝缘材料的耐高压低电流干电弧性能的测试方法 Standard Test Metho d forHigh-Voltage, Low-Current, Dry Arc Resistance of Solid ElectricalInsulationD500-95(2003) 磺化油和硫化油的化学分析和试验方法D501-03 碱性洗涤剂的抽样和化学分析试验方法D502-89(2003) 肥皂和其它洗涤剂粒度的试验方法D509-05 松香分级和抽样试验方法D511-03 水中钙镁离子的测试方法D512-04 测定水中氯离子含量的试验方法D513-02 水中二氧化碳溶解量和总量的试验方法D516-02 水中硫酸铁的试验方法D517-98(2003) 沥青厚板材D518-99 橡胶变质表面龟裂的试验方法D519-04 羊毛条中纤维长度的试验方法D520-00(2005) 锌粉颜料规范D521-02 锌粉(金属锌粉)的化学分析试验方法D522-93a(2001) 用锥形心轴仪测定涂覆有机涂层延伸率的试验方法D523-89(1999) 镜面光泽的试验方法D524-04 石油产品中兰氏残炭的试验方向D525-05 汽油氧化稳定性的试验方法(诱导期方法)D528-97(2002) 纸和纸板的机器定向试验方向D529-04 沥青材料的加速风化试验条件和程序的测试方法(碳弧法)D531-00(2005) 普西和琼斯橡胶压缩试验方法D542-00 透明有机塑料的折射指数的试验方法D543-06 塑料耐化学试剂性能的试验方法D545-99(2005) 混凝土用预制伸缩缝纫填料的试验方法(非挤压和弹性型)D546-05 道路和铺砌材料用矿物填料筛分的测试方法D548-97(2002) 纸张水溶解酸碱度的试验方法D555-84(1998) 干性油试验D558-04 土壤水泥混合物的水分与密度关系的试验方法D559-03 压实的掺土水泥混合物的湿润与干燥的试验方法D560-03 压实的掺土水泥混合物的冻融试验方法D561-82(2003) 涂料用炭黑颜料D562-01(2005) 斯氏粘度计测定涂料稠度的试验方法D563-88(1996)e1 醇酸树脂和树脂溶液中苯酐含量的试验方法D564-87(2002) 液体涂料催干剂的试验方法D565-99(2005) 白色矿物油中可碳化物质的试验方法D566-02 润滑脂滴点的试验方法D570-98(2005) 塑料吸水率的试验方法D572-04 用加热法和氧化法进行的橡胶变质的试验方法D573-04 在空气烤炉中作橡胶变质的试验方法D575-91(2001) 橡胶压缩特性的试验方法D578-05 玻璃纤维丝D579-04 原织物玻璃纤维D580-04 机织玻璃纤维带D581-99 机织玻璃纤维套管的编织D584-96(2005) 原毛中羊毛含量实验室测试方法D585-97(2002) 纸张、纸板、纤维板和相关产品的单批取样和验收方法D586-97(2002) 纸中灰分含量的试验方法D589-97(2002) 纸的不透明度的测试方法D590-93(2002) 纸中石油蜡的测试方法D596-01 水分析结果的报告D600-90(2001) 液体涂料催干剂D601-87(1998) 奥气油(永久液体)D602-81(2003) 硫酸钡颜料规范D605-82(2003) 硅酸镁颜料(滑石)D607-82(2003) 湿磨云母颜料D608-05 邻苯二甲酸二丁酯D609-00 涂料、油漆以及改性涂料与相关涂料产品的测试用冷轧钢板的制备D610-01 涂漆钢表面锈蚀程度评价的试验方法D611-04 石油产品和烃类溶剂苯胺点和混合苯胺点的试验方法D612-88(2004) 石蜡中可碳化物质的试验方法D613-05 十六烷法测定柴油燃料燃烧质量的试验方法D618-05 塑料及电绝缘材料的调理方法D619-99(2004) 电绝缘用硫化纤维的测试方法D622-99(2005) 汽车空气制动和真空制动系统用橡胶软管试验方法D623-99e1 橡胶特性-压缩中热的产生及挠曲疲劳的试验方法D624-00e1 橡胶的热塑性弹性的耐老化性的抗撕裂强度的试验方法D628-95(2004)e1 石棉套管的标准规范D629-99 纺织品定量分析试验方法D632-01 氯化钠D633-97(2005) 道路柏油的体积修正表D635-06 自承塑料在水平状态时的燃烧速率或者燃烧蔓延程度及燃烧时间的试验方法D638-03 塑料拉伸性能的试验方法D642-00(2005) 船用集装箱、组合件和单体加载的抗压缩能力的测试方法D643-97(2002) 用厦泊测试仪测试纸的折痕持久性的标准试验方法D644-99(2002) 用烘干法测定纸和纸板中水分的测试方法D645/D645M-97(2002) 纸和纸板厚度的测试方法D646-96(2001) 纸张及纸板的基本重量的试验方法(单位面积的重量)D648-06 在挠曲负荷下塑料的挠曲温度的试验方法D653-05 土壤、岩石和其内部所含液体的相关术语D660-93(2005) 外用漆龟裂程度评价方法D661-93(2005) 外用漆破裂程度评价的试验方法D662-93(2005) 外用漆侵蚀程度评价的试验方法D664-06 电位滴定法测定石油产品酸值的试验方法D665-06 水存在下抑制的矿物油防锈特性的试验方法D668-99(2004) 电绝缘用硬条和硬管尺度测量的测试方法D669-03 层压薄板与层压板的平行于层片的耗散系数和介电常数的试验方法D685-93(2002) 检测调理纸和纸制品D686-93(2002) 纸中矿物填料和矿物涂料的定性测试方法D689-03 纸张的内部耐撕裂的试验方法D692-00(2004) 沥青铺路砌混合用粗集料D693-03a 碎石路面用压碎集料D695-02a 硬质塑料抗压特性的试验方法D696-03 从-30摄氏度到30摄氏度的塑料线性热膨胀系数的试验方法D698-00ae1 实验室中用12000ft-lbt/ft(600KN-m/m)作用力测定土壤压力特性的试验方法D704-99(2004) 三氯氰胺甲醛模制化合物D705-99(2004) 脲甲醛模制化合物D706-05 乙酸纤维素模制和挤压化合物D707-05 醋酸丁酸纤维素模制与挤压料规格D709-01 层压热固材料D710-97(2002) 电绝缘用硫化纤维薄板、条和管D711-89(2004) 路标漆不粘着时间的试验方法D713-90(2004) 路标漆进行路面使用的试验方法D714-02e1 涂料起泡程度的试验方法D715-86(2003) 硫酸钡颜料分析的标准试验方法D716-86(2003) 评定云母颜料的标准试验方法D717-86(2003) 硅酸镁颜料分析的标准试验方法D718-86(2003) 硅酸铝颜料的分析标准试验方法D720-91(2004)e1 煤自由膨胀指数的试验方法D721-05 石油蜡含油量的试验方法D722-93(2002) 纸的抗油脂性标准试验方法D724-99(2003) 纸表面可湿性的测试方法(接触角法)D726-94(2003) 空气中无孔纸的透气性的测试方法D727-96(2001) 真空方法测定屋顶和地板油毡煤油值的试验方法D731-95(1999) 热固模塑料粉末的模塑指数的试验方法D732-02 用穿孔工具测量塑料剪切强度的测试方法D737-04 纺织纤维透气率的试验方法D740-05 丁酮规范D746-04 用冲击法测定塑料及弹性材料的脆化温度的试验方法D747-02 用悬臂梁法对塑料表观弯曲系数的测试方法D748-00(2005)e1 固定式云母介电电容器用天然云母块和云母薄片D750-00 用碳弧型装置和风化装置对橡胶变质的测试方法D751-06 涂层织物的测试方法D763-01 未加工棕土和焙烧棕土颜料D765-87(2003) 未加工黄土和焙烧黄土颜料技术规范D768-01 黄色氧化铁的水合物D769-01 黑色合成氧化铁D770-05 异丙醇规范D772-86(2005) 外部涂料剂落程度评价的试验方法D774/D774M-97(2002) 纸张抗破碎强度的测试方法D776-92(2001) 干热对纸和纸板特性的影响的试验方法D777-97(2002) 经过处理的纸和纸板易燃性的标准试验方法D778-97(2002) 纸萃液(热萃取和冷萃取法)氢离子浓度(pH)的标准试验方法D779-03 纸、纸板和其他印刷材料用干烧指示器法测试耐水性的测试方法D780-95(2003) 纸印刷油墨渗透性的测试方法(蓖麻油试验)D784-03 电绝缘材料用橙色紫胶和其他印度虫胶D785-03 塑料和电绝缘材料的洛氏硬度的测试方法D787-96(2003) 乙基纤维模制和挤压化合物D788-05 甲基丙烯酸酯模制和挤压化合物的分类系统D789-06 聚酰胺相对粘度,熔点和含水量的测试方法D790-03 未增强和增强塑料及电绝缘材料的挠曲性的试验方法D792-00 用位移法测定塑料密度和比重(相对密度)的标准试验方法D800-05 工业用金属除垢剂化学分析试验方法D801-02 二聚戊烯抽样和测试的试验方法D802-02 松油抽样和测试的试验方法D803-03 妥儿油的测试试验方法D804-02 松脂制品包括妥儿油及相关产品的术语D806-00(2006) 掺土水泥混合物中水泥含量的试验方法D807-05 工业锅炉用水引起脆裂倾向的评价方法(美国矿业局的脆变检查器方法)D808-05 新的和使用过的石油产品中氯含量的试验方法(氧弹法)D813-06 测定橡胶龟裂扩展的试验方法D814-95(2005) 橡胶特性挥发性液体蒸汽渗透性的试验方法D816-06 橡胶胶水的试验方法D817-96(2004) 乙酸丙酸纤维素和醋酸丁酸纤维素的试验方法D820-93(2003) 含合成洗涤剂肥皂的化学分析试验方法D822-01 用经过过滤明光碳弧灯和水中曝光装置对涂料及相关涂层和材料上做的导电试验D823-95(2001) 色漆,清漆,喷漆及有关产品制成厚度均匀漆膜试片的方法D824-94(2002) 用皱文纸测定吸水率的测试方法D828-97(2002) 纸和纸板拉力破坏强度的测试方法D829-97(2002) 纸和纸制品湿抗拉断裂强度的标准试验方法D831-94(2004) 电缆及电容器油的气体含量的测试方法D832-92(2001)e1 低温状态下的橡胶试验D841-02 甲苯的硝化定级D843-06 硝化二甲苯D847-04 苯,甲苯,二甲苯,溶剂石脑油和类似的工业芳烃酸度的试验方法D848-03 工业芳烃的酸洗颜色的标准试验方法D849-05 工业芳烃对铜条腐蚀的标准试验方法D850-03 工业芳轻及相关物质的蒸溜法D852-02 苯凝固点的试验方法D853-04 工业芳烃中硫化氢和二氧化硫含量(定性)的标准试验方法D854-06 土壤比重的试验方法D857-02 水中铝含量的测试方法D858-02 水中锰含量的试验方法D859-05 水中二氧化硅的测试方法D861-01a 用特克斯制命名纤维,纱的半制品,纱和其它纺织品线度D865-99(2005) 橡胶的空气中加热变质试验方法(试管法)D866-99(2004) 电线及电缆用丁苯合成橡胶套D868-85(2003) 路标漆渗色程度评价的试验方法D869-85(2004) 涂漆沉降程度评价试验方法D870-02 水浸渍法涂层耐水试验D871-96(2004) 测试乙酸纤维素的试验方法D873-02 航空燃料的氧化稳定性的测试方法D874-06 润滑油和添加剂中硫酸盐类灰分的测试方法D876-00 电绝缘用刚性氧化乙烯聚合物管的测试方法D877-02e1 用圆盘电极测定电绝缘液体介电击穿电压的试验方法D878-01e1 绝缘油中无机氯化物和硫酸盐的测试方法D880-92(2002) 船用集装箱的冲击试验的试验方法D882-02 塑料薄板材抗拉特性的试验方法D883-00 塑料相关术语D885-06 由人造有机纤维制成的轮胎帘子线,轮胎帘布和工业长纱线的测试D887-82(2003)e1 水沉积物抽样D888-05 水中溶解氧的试验方法D889-99(2004) 松香中油挥发性的试验方法D890-98(2003) 液体松脂中水含量的试验方法D891-95(2004) 液态工业化合物的比重,表观比重的测试方法D892-05 润滑油发泡特性的标准试验方法D893-05a 用过的润滑油中不溶物的试验方法D896-04 胶粘剂耐化学试剂粘法的试验方法D897-01e1 胶粘剂粘结力的抗拉性的测试方法D898-05 胶粘剂固体单位面积涂用重量的试验方法D899-00 单位面积涂用液体胶粘剂的重量的测试方法D902-00 电绝缘用挠性涂树脂玻璃布和玻璃布带的测试方法D903-98(2004) 胶粘剂粘结抗剥落或爆皮强度的试验方法D904-99(2005) 人造光(碳弧型)和自然光对胶粘剂试样的曝光D905-03 用压缩荷载法测定胶粘剂的抗剪切强度性能的试验方法D906-98(2004) 用拉力负荷法测定胶合板结构中胶粘剂剪切强度特性的试验方法D907-05e1 胶粘剂术语D909-01e1 增压进料法测定航空汽油抗震性的试验方法(联邦试验方法No.791b) D910-04a 航空汽油技术规范D912-81(1999) 防污涂料用氧化亚铜D913-03e1 路标漆耐磨程度的评价方法D914-00(2006) 乙基纤维的试验方法D918-99(2003) 纸和纸板的抗粘结性试验方法D919-97(2002) 纸和纸板的铜值测试方法D922-00a(2006) 非硬质聚氯乙烯管D923-97 电绝缘液体的抽样方法D924-04 电绝缘液体的损耗因数(或功率因数)和介电常数(电容率)的测试方法D925-06 橡胶特性.表面着色(接触、色移和扩散)的试验方法D926-04 用平行板法测量橡胶的塑性和弹性D928-03 碳酸氢钠D932-85(2002) 水和水沉积物中嗜铁细菌含量试验方法D933-84(2003) 水沉积物的检验和分析结果的报告方法D934-80(2003) 用X射线衍射法作水沉积物中结晶化合物的识别方法D937-04 石油脂的针入度试验方法D938-05 石油蜡(包括凡士林)凝固点的测试方法D942-02 氧弹法测定润滑脂氧化稳定性的试验方法D943-04a 防腐蚀矿物油氧化特性的试验方法D945-06 用机械示波器测定在压缩应力和剪切应力下橡胶特性的试验方法D946-82(2005) 路面建造用按贯入度级配的沥青膏D950-03 胶粘剂抗冲击强度的试验方法D951-99(2004) 用喷射法测定船运集装箱的耐水性的试验方法D952-02 薄板塑料和电绝缘材料粘结强度的试验方法D953-02 塑料支承强度的测试方法D955-00 模制塑料模型尺寸收缩率的测量方法D957-95(2006)e1 塑料生产用模型表面温度的测定D960-02a 生蓖麻油D961-86(2001) 脱水蓖麻油D962-81(2003) 涂料用铝粉和铝浆颜料D964-03 防污漆用铜粉D968-05 用落沙磨蚀法测定有机涂层耐磨性的试验方法D969-85(2003) 路标漆渗色程度的实验室试验方法D971-99a(2004) 环法测定油水界面张力的试验方法D972-02 润滑脂和润滑油蒸发损失的测试方法D974-04 用颜色指示剂滴定法测定酸碱值的标准试验方法D975-06 柴油技术规范D976-04be1 馏分燃料正十六烷指数的计算方法D977-05 乳化沥青D979-01(2006)e1 沥青铺面混合料的取样方法D982-05 Standard Test Method for Organic Nitrogen in Paper andPaperboard D984-97(2002)。

(完整版)ASTMD类最新标准目录(四).doc

ASTM D类最新标准目录（四）.docD1720-03 硝酸纤维素溶液中活性溶剂稀释比的试验方法D1721-97(2001) 磷酸三甲苯酯高锰酸盐时间的测试方法D1722-98(2004) 水溶性溶剂的水混溶性试验方法D1725-04 树脂溶液粘度的测试方法D1726-03 液体环氧树脂中水解氯含量的试验方法D1729-96(2003) 不透明材料色差的目测评估D1730-03 涂漆铝和铝合金表面预处理D1731-03 涂漆热浸铝表面预处理D1732-03 涂漆镁合金表面预处理D1734-93(2003) 涂料面漆测试用水泥板和瓦工板的制备D1735-04 用水雾仪作涂层耐水性试验D1739-98(2004) 降尘(可沉降粒状物)的收集和测量的试验方法D1740-01 航空涡轮机燃料发光计值的试验方法D1742-06 贮存过程中油从润滑脂中分离的试验方法D1743-05ae1 润滑脂防腐蚀性能的测试方法D1746-03 塑料薄板透明度的试验方法D1747-99(2004)e1 粘性材料折射指数的测试方法D1748-02 在湿润箱中用金属保护剂防止金属生锈的试验方法D1749-93(2002) 纸和纸制品试验方法的实验室间评估D1751-04 混凝土铺面和结构建筑用预制伸缩缝填料(非挤压的弹性沥青型)D1752-04a 混凝土铺面和结构建筑用预制微孔橡胶与软木伸缩缝填料D1754-97(2002) 加热和空气对沥青材料影响的试验方法(薄膜炉试验)D1755-92(2001) 聚氯乙烯树脂规范D1756-02 煤中二氧化碳的测试方法D1757-03 煤灰和焦灰中硫含量的测试方法D1758-06 用木桩现场试验评定木材防腐剂D1760-01 木材产品的加压处理D1761-06 木结构用机械紧固件的测试方法D1762-84(2001) 木炭的化学分析D1763-00(2005) 环氧树脂D1765-05ae1 橡胶制品用碳黑的分类系统D1766-05 橡胶化学制品的试验方法.溶解性D1767-89(2003) 肥皂或合成洗涤剂中乙二胺四乙酸盐(EDTA)含量的测试方法D1768-89(2003) 用紫外线吸收法对合成洗涤剂中烷基苯磺酸钠含量的测试方法D1770-94(2000)e1 羊毛条中毛结,植物性物质与有色纤维含量测试方法D1776-04 试验用调湿织物D1777-96(2002) 测量纺织材料的厚度D1779-98(2004) 传声材料附着力试验方法D1780-05 金属对金属之间胶粘剂引起蠕变的试验D1781-98(2004) 胶粘剂攀缘卷筒剥离的试验方法D1782-95(2001) 粒状阳离子交换材料使用性能的测试方法D1783-01 水中苯酚类化合物的测试方法D1784-03 硬质聚氯乙烯化合物和氯化聚氯乙烯化合物D1785-06 聚氯乙烯塑料管.40,80及120号表D1786-01(2006)e1 甲苯二异氰酸盐D1790-02 用冲击法测定塑料薄板的脆化温度的试验方法D1791-93(2004) 液态水乳化地板擦亮剂加速老化的试验方法D1792-06 乳化地板擦亮剂长期可除污性的测试方法D1793-92(2002) 地板擦亮乳剂水斑的测试方法D1795-96(2001)e1 纤维素固有粘度的测试方法D1796-04 离心法测定燃料油中水分及沉淀物的试验方法(实验室法)D1799-03a 碳黑.包装装运物抽样D1807-00(2005) 电绝缘液体折射指数和比光散度的试验方法D1813-00(2005) 皮件试样厚度测量D1814-70(2005) 测量皮件厚度的测试方法D1815-00(2005) 皮革吸水率(静态)的测试方法D1816-04 用VDE电极测量石油制绝缘油的介电击穿电压的测试方法D1817-05 橡胶化学制品的试验方法.密度D1822-06 对断裂塑料及电绝缘材料的拉伸冲击能量的测试方法D1823-95(2001) 用挤压粘度计测定在高速剪切时塑料溶胶和有机溶胶的表观粘度的试验方法D1824-95(2002) 在低剪切速率下塑料溶胶和有机溶胶的表观粘度的测试方法D1825-03 电气试验用镀铜电绝缘材料及热固层压材料的浸蚀和清洗D1826-94(2003) 用连续记录量热器测定天燃气范围中煤气热值的测试方法D1827-92(2002) 用二氧化碳置换法测定绝缘液体中气含量(非酸性物)的试验方法D1828-01e1 粘接接口和结构的空气暴露D1830-99(2005) 用弧形电极法测定电绝缘挠性薄片材料热稳定性的试验方法D1831-00(2006) 润滑脂滚轧稳定性的试验方法D1832-04 石油蜡过氧化值的测试方法D1833-87(2004) 石油蜡气味的测试方法D1834-90(2000) 蜡纸的20度镜面光泽的试验方法D1835-05 液化石油(LP)气D1836-02 商品己烷D1837-02a 液化石油气挥发性的试验方法D1838-06 液化石油气对铜片腐蚀性的试验方法D1839-91(2005) 柴油燃料中硝酸戊脂的测试方法D1840-03 紫外线分光光度法测定航空涡轮机燃料中萘烃的试验方法D1841-63(1998) 馏出的椰子脂肪酸D1842-63(1998) 馏出的玉米脂肪酸D1843-63(1998) 分馏和馏出的棉子脂肪酸D1844-86(2003) 碱式硅铬酸铅的化学分析测试方法D1845-86(2003) 铬酸锶颜料的化学分析测试方法D1847-93(1998) 环氧树脂中总氯量的试验方法D1849-95(2003) 涂料包装耐久性的测试方法D1854-02 热浇注弹性型抗喷气燃料的混凝土接缝密封料D1856-95a(2003) 用阿布松(Abson)法从溶液中回收沥青的试验方法D1857-04 煤和焦炭灰的可溶性试验方法D1858-63(2000) 杂酚油-石油溶液D1859-71(2000) 与杂酚油掺合用的石油D1860-95(2000) 木材中水份及杂酚油型防腐剂的试验方法D1863-05 组合屋面用矿物集料D1864-89(2002) 组合屋面用矿物集料中水分的测试方法D1865-89(2002) 组合屋面用矿物集料硬度的试验方法D1867-01 印制线路用镀铜热固层压板D1868-93(1998) 电绝缘系统评定中的局部放电(电晕)脉冲的检查和测量的方法D1869-95(2005) 石棉水泥管用橡胶垫圈D1871-04 单根钢丝对橡胶附着力的测试方法D1874-62(2004) 纤维板船运箱顶盖自动机密封用水可溶或溶剂可溶的液体胶粘剂D1875-03 流体胶粘剂密度的测试方法D1876-01 胶粘剂的抗剥离性的试验方法(T型剥离试验)D1879-06 暴露在高能辐射下的胶粘剂样品D1881-97(2002)e1 在玻璃器皿中发动机冷却剂的起泡倾向的试验方法D1882-96(2001) 汽车用冷却系统化学溶液对车辆有机面漆产生影响的测试方法D1883-05 实验室压实泥土的加利福尼亚承载力比的试验方法D1886-03 水中镍含量的测试方法D1889-00 水的混浊度的测试方法D1890-05 水的β粒子放射性的测试方法D1894-06 塑料薄膜及薄板的静态和动态摩擦系数的测试方法D1895-96(2003) 塑料材料的表观密度,容积因素和可倾注性的试验方法D1896-99(2004) 热固化合物传递模塑试样D1900-94(2002) 碳黑.散装装运物抽样D1901-00(2004) 卤化有机溶剂及其掺合物的相对蒸发时间的测试方法D1903-03 阿斯卡列电介液和石油制造的电绝缘液的热膨胀系数的测试方法D1907-01 用绞纱法测定纱线支数的标准试验方法D1909-04 纤维纺织品商品回潮率表D1912-00(2005)e1 家具革耐冻裂性的试验方法D1913-00(2005) 服装革抗湿性的试验方法(喷雾法)D1914-95(2004)e1 有关大气分析的换算单位和换算系数D1916-93(1997) 胶粘剂渗透性的测试方法D1917-03 橡胶性能的测试方法.丁苯橡胶生胶和混炼胶的收缩性D1918-95(2004)e1 石棉织物石棉含量的标准测试法D1921-06 塑料粒度(筛析)的试验方法D1922-06a 用摆锤法测定塑料薄膜与薄板抗扩展扯裂性的测试方法D1926-00(2006) 纤维素羧基含量的测试方法D1929-96(2001)e1 塑料引燃性能的测试方法D1931-99(2004) 电绝缘用完全硫化的硅橡胶涂层玻璃布和玻璃带D1932-04 韧性电绝缘清漆的耐热性的试验方法D1933-03 作为电绝缘材料的氮气D1934-95(2005) 用开杯法作电绝缘石油的氧化老化的试验方法D1937-05 颗粒碳黑的测试方法.质量强度D1938-02 用一次撕裂法测定塑料薄膜与薄板的抗撕裂扩展性的试验方法D1941-91(2001) 用帕夏尔斜槽(Parshall)进行水的明沟流量测量的试验方法D1943-05 水的α粒子放射性的测试方法D1945-03 气相色谱法分析天燃气的测试方法D1946-90(2006) 用气相色谱法作重整气分析D1957-86(2001) 脂肪油和脂肪酸羟基值的试验方法D1959-97 干性油及脂肪酸碘值的试验方法D1963-85(1996) 干性油,清漆,树脂及相关原料在25/25℃时比重的试验方法D1965-87(1998) 干性油,脂肪酸和聚合脂肪酸中不皂化物的测试方法D1966-69(1998) 生亚麻油油脚的标准试验方法D1968-02a 与纸和纸产品相关的术语D1969-01 2-乙基己醇(合成物)D1970-01 冰坝防护用作为陡斜屋面衬底的自粘聚合物改良型沥青板材料D1971-02 用火焰原子吸收或等离子发射光谱法对金属测定用试样的蒸煮D1972-97(2005) 塑料产品的类别标记D1974-98(2003) 封口,密封及加固纤维板海运集装箱的方法D1975-95(2001)e1 塑料注模开口桶抗环境应力断裂的试验方法D1976-02 用电感耦合氩等离子原子发射光谱法对水中元素的测试方法D1977-03 用氢氟酸/硫酸分解和原子光谱分析测定FCC平衡催化剂中镍和钒的测试方法D1978-91(2002) 电镀试样分析D1979-97 氨基树脂中游离甲醛含量的测试方法D1980-87(1998) 脂肪酸和聚合脂肪酸中酸值的试验方法D1981-02 脂肪酸加热后测量颜色的试验方法D1982-85(2004) 脂肪酸冻点测试方法D1985-03 测试连接和裂缝粘合用密封胶用混凝土块的制备D1986-91(2002) 聚乙烯蜡的表观粘度测量的测试方法D1987-95(2002) 土工织物或泥土/土工织物的生物阻塞的测试方法D1988-06 用色斑长度检测管测定天然气中的硫醇的试验方法D1990-00(2002)e1 确定实尺样品分级试验中目测级量度木材的允许参数D1991-05 橡胶化学试验方法.二巯基苯并噻唑(MBT).化验D1992-91(2001) 橡胶用合成增塑剂试验D1993-03 用多点布-埃-特氮气吸附法对沉积二氧化硅表面面积的测试方法D1994-95(2000) 测量热溶胶粘剂酸值的测试方法D1995-92(2004) 胶粘剂(压合式粘合剂)多种强度试验的试验方法D1996-97(2003) 用液体色层分离法(LC)对低浓度聚乙烯中酚醛抗氧剂和棕榈纤维酰胺润滑添加剂的测试方法D1997-91(2001) 用干燥物质作泥炭样品纤维含量的试验室测定的测试方法D1998-04 聚乙稀立式贮藏箱D2000-06 汽车用橡胶制品的分类系统D2001-92(2002) 汽油和石脑油脱戊烷的试验方法D2007-03 粘土凝胶吸附色谱法测定橡胶增量及作业油和加工油中特性基团的试验方法D2008-91(2006) 石油产品紫外线吸收率和吸收系数的试验方法D2010/D2010M-98(2004) 用二氧化铅蜡烛法评定大气中活性硫化物总含量的测试方法D2013-04 分析用煤样品的制备D2014-97(2004) 用底部加热炉对煤的膨胀性和收缩性的测试方法D2017-05 Standard Test Method of Accelerated Laboratory Test ofNatural Decay Resistance ofWoodsD2019-97(2002) 纸和纸板中杂质的测试方法D2020-92(2003) 纸和纸板的耐霉性的测试方法D2022-89(2003) 含氯漂白剂的抽样和化学分析的测试方法D2023-89(2003) 洗涤剂中甲苯磺酸钠分析的测试方法D2024-65(2003) 非离子表面活性剂的混浊点的测试方法D2026-97(2004) 稀释沥青(慢凝型)D2027-97(2004) 稀释沥青(中凝型)D2028-97(2004) 稀释沥青(快凝性)D2029-97(2003) 用露点法测定电绝缘气体中蒸汽含量的试验方法D2035-80(2003) 水的凝聚絮凝瓶试验D2036-06 水中氰化物的测试方法D2041-03a 沥青铺砌混合料最大理论比重和密度的试验方法D2042-01 沥青材料在三氯乙烯中溶解度的试验方法D2043-94(2002) 用纸对银失去光泽的测试方法D2047-04 用杰门机对擦亮涂覆地板表面静摩擦系数的测试方法D2048-92(2002) 地板擦亮膜粉化的测试方法D2050-04 有关拉链的名词术语D2051-03 拉链表面耐洗性能的测试方法D2052-05 拉链耐干洗色牢度的测试方法D2053-99(2004) 拉链耐光照色牢度的试验方法D2054-99(2004) 拉链布带耐磨擦色牢度的标准试验方法D2057-05 洗涤时拉链色牢度的测试方法D2058-03 拉链干洗后耐久性的试验方法D2059-03 拉链抗盐雾(雾状)腐蚀的试验方法D2060-00(2005)e1 测量拉链尺寸的方法D2061-03 拉链强度的测试方法D2062-03 拉链可用性的试验方法D2063-91(2002) 带连续线性封合的包装件用持久扭矩测量的测试方法D2064-91(2003) 建筑涂料抗污染性的标准试验方法D2065-03 在表面活化剂加速潮湿应力下测量组合木材产品边棱性能的测试方法D2066-06 印刷油墨色散的相对着色力测试方法D2067-97(2003) 印刷油墨分散剂中粗颗粒的测试方法D2068-04 馏出燃料油过滤器阻塞倾向的测试方法D2070-91(2001) 液压油热稳定性的试验方法D2071-87(1998) 脂族氮制品的试验方法D2072-92(1998)e1 脂族氮化合物中水的试验方法D2073-92(1998)e1 仲裁电势测定法测定脂肪胺,酰胺基胺及二元胺的总胺值,伯胺值,仲胺值和叔胺值的试验方法D2074-92(1998) 交替指示剂法测定脂肪胺中总胺值,伯胺值,仲胺值和叔胺值的试验方法D2075-92(1998) 脂肪胺,酰胺基胺及二元胺碘值的试验方法D2076-92(1998) 脂族季铵氯化物中酸值和胺值的测试方法D2077-92(1998) 脂族季铵氯化物中灰分的测试方法D2079-92(1998) 脂族季铵氯化物中不挥发物质(固体)的测试方法D2080-92(1998) 脂族季铵氯化物平均分子量的测试方法D2081-92(1998) 脂族季铵氯化物中pH值的测试方法D2082-92(1998) 脂族氮化合物中非胺物百分比的测试方法D2083-92(1998) 脂肪胺中伯,仲,叔胺百分比的计算测试方法D2084-01 橡胶性能的测试方法.用振动圆盘硫化计测量硫化作用。

ASTM D1193-2006 试剂水规范

Designation:D1193–06Federal Test MethodStandard No.7916Standard Speciﬁcation forReagent Water1This standard is issued under theﬁxed designation D1193;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon(e)indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1.Scope1.1This speciﬁcation describes the required characteristics of waters deemed suitable for use with the Standards under the jurisdiction of ASTM.1.2The alphanumeric characters ascribed to water types and grades are speciﬁed in the ASTM Format and Style Manual. These have been assigned in order of historical precedence and should not be taken as an indication of a progression in water purity.1.3Four types of waters have been speciﬁed,with three additional grades that can be applied to the four types.The grade speciﬁcations speciﬁcally address contaminants of mi-crobiological origin.1.4All applicable ASTM Standards are expected to refer-ence one or more of these reagent water types where reagent water is needed as a component of an analytical measurement process.Where a different water type or grade is needed for an ASTM Standard,it may be added to this Speciﬁcation through the ASTM Standard revision process.1.5Although these water types and associated grades have been deﬁned speciﬁcally for use with ASTM Standards,they may be appropriate for other applications.It is the responsi-bility of the users of this standard to ensure that the selected water types or grades are suitable for their intended use. Historically,reagent water Types I,II,III,and IV have been linked to speciﬁc processes for their production.Starting with this revision,these types of waters may be produced with alternate technologies as long as the appropriate constituent speciﬁcations are met and that water so produced has been shown to be appropriate for the application where the use of such water is speciﬁed.Therefore,the selection of an alternate technology in place of the technology speciﬁed in Table1 should be made taking into account the potential impact of other contaminants such as microorganism and pyrogens.Such contaminants were not necessarily considered by the perfor-mance characteristics of the technology previously speciﬁed.1.6Guidance for applications,the preparation,use and monitoring,storage,handling,distribution,testing of these speciﬁed waters and validation of the water puriﬁcation system is provided in Appendix X1of this document.1.7This standard does not purport to address all of the safety concerns,if any,associated with its use.It is the responsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2.Referenced Documents2.1ASTM Standards:2D1125Test Methods for Electrical Conductivity and Re-sistivity of WaterD1129Terminology Relating to WaterD1293Test Methods for pH of WaterD4453Practice for Handling of Ultra-Pure Water Samples D4517Test Method for Low-Level Total Silica in High-Purity Water by Flameless Atomic Absorption Spectros-copy3D5128Test Method for On-Line pH Measurement of Water of Low ConductivityD5173Test Method for On-Line Monitoring of Carbon Compounds in Water by Chemical Oxidation,by UV Light Oxidation,by Both,or by High Temperature Combustion Followed by Gas Phase NDIR or by Electrolytic Conduc-tivityD5245Practice for Cleaning Laboratory Glassware,Plas-ticware,and Equipment Used in Microbiological Analyses D5391Test Method for Electrical Conductivity and Resis-tivity of a Flowing High Purity Water SampleD5542Test Method for Trace Anions in High Purity Water by Ion ChromatographyD5997Test Method for On-Line Monitoring of Total Car-bon,Inorganic Carbon in Water by Ultraviolet,Persulfate1This speciﬁcation is under the jurisdiction of ASTM Committee D19on Water and is the responsibility of Subcommittee D19.02on General Speciﬁcations, Technical Resources,and Statistical Methods.Current edition approved March1,2006.Published March2006.Originally approved st previous edition approved in1999as D1193–99e1.2For referenced ASTM standards,visit the ASTM website,,or contact ASTM Customer Service at service@.For Annual Book of ASTM Standards volume information,refer to the standard’s Document Summary page on the ASTM website.3Determination of Trace Silica in Industrial Process Waters by Flameless Atomic Absorption Spectrometry,Judith Rawa and Earl Henn,Analytical Chemistry,V ol51, No3,March1979.Copyright©ASTM International,100Barr Harbor Drive,PO Box C700,West Conshohocken,PA19428-2959,United States.Oxidation and Membrane Conductivity DetectionD 6071Test Method for Low Level Sodium in High Purity Water by Graphite Furnace Atom Absorption Spectroscopy D 6161Terminology Used for Crossﬂow Microﬁltration,Ultraﬁltration,Nanoﬁltration and Reverse Osmosis Mem-brane ProcessesD 6529Test Method for Operating Performance of Con-tinuous Electrodeionization Systems on Feeds from 50–1000µS/cmF 1094Test Methods for Microbiological Monitoring of Water Used for Processing Electron and Microelectronic Devices by Direct Pressure Tap Sampling Valve and by the Presterilized Plastic Bag Method3.Terminology3.1Deﬁnitions —For deﬁnitions used in this speciﬁcation refer to Terminology D 1129.3.2Deﬁnitions of Terms Speciﬁc to This Standard:3.2.1reagent water —water that is used speciﬁcally as a component of an analytical measurement process and meets or exceeds the speciﬁcations for these waters.3.2.2electrodeionization —a process that removes ionized and ionizable species from liquids using electrically active media and using an electrical potential to inﬂuence ion transport,where the ionic transport properties of the active media are a primary sizing parameter.ElectrodeionizationTABLE 1Processes for Reagent Water ProductionTypeGradeProduction ProcessA ,B ,C ,DµS/cm E (max)M V ·cm F (min)pHGTOC µg/L H (max)Sodium µg/L I (max)Chloride µg/L J (max)Total Silica µg/L (max)HBC K cfu/mL (max)Endotoxin,EU/mL L (max)IPurify to 20µS/cm by dist.or equiv.,followed by mixed bed DI,0.2µm ﬁltration A0.05551850113I APurify to 20µS/cm by dist.or equiv.,followed by mixed bed DI,0.2µm ﬁltration A0.0555185011310/10000.03I BPurify to 20µS/cm by dist.or equiv.,followed by mixed bed DI,0.2µm ﬁltration A0.0555185011310/1000.25I CPurify to 20µS/cm by dist.or equiv.,followed by mixed bed DI,0.2µm ﬁltration A 0.05551850113100/10II Distillation B 1.0 1.050553II A Distillation B 1.0 1.05055310/10000.03II B Distillation B 1.0 1.05055310/1000.25II CDistillation B1.0 1.050553100/10III Distillation,DI,EDI,and/or RO,followed by 0.45µm ﬁltration.C 0.25 4.020********III A Distillation,DI,EDI,and/or RO,followed by 0.45µm ﬁltration.C 0.25 4.0200101050010/10000.03III B Distillation,DI,EDI,and/or RO,followed by 0.45µm ﬁltration.C 0.25 4.0200101050010/1000.25III CDistillation,DI,EDI,and/or RO,followed by 0.45µm ﬁltration.C 0.25 4.020010105001000/100IV Distillation,DI,EDI,and/or RO.D 5.00.2 5.0to 8.05050IV A Distillation,DI,EDI,and/or RO.D 5.00.2 5.0to 8.0505010/10000.03IV B Distillation,DI,EDI,and/or RO.D 5.00.2 5.0to 8.0505010/1000.25IVCDistillation,DI,EDI,and/or RO.D5.00.25.0to 8.05050100/10AType I grade of reagent water shall be prepared by distillation or other equal process,followed by polishing with a mixed bed of ion-exchange materials and a 0.2-µm membrane ﬁlter.Feed water to the ﬁnal polishing step must have a maximum conductivity of 20µS/cm at 298K (25°C).Type I reagent water may be produced with alternate technologies as long as the appropriate constituent speciﬁcations are met and that water so produced has been shown to be appropriate for the application where the use of such water is speciﬁed .BType II grade of reagent water shall be prepared by distillation using a still designed to produce a distillate having a conductivity of less than 1.0µS/cm at 298K (25°C).Ion exchange,distillation,or reverse osmosis and organic adsorption may be required prior to distillation,if the purity cannot be attained by single distillation.Type II reagent water may be produced with alternate technologies as long as the appropriate constituent speciﬁcations are met and that water so produced has been shown to be appropriate for the application where the use of such water is speciﬁed .CType III grade of reagent water shall be prepared by distillation,ion exchange,continuous electrodeionization,reverse osmosis,or a combination thereof,followed by polishing with a 0.45-µm membrane ﬁlter.Type III reagent water may be produced with alternate technologies as long as the appropriate constituent speciﬁcations are met and that water so produced has been shown to be appropriate for the application where the use of such water is speciﬁed.DType IV grade of reagent water may be prepared by distillation,ion exchange,continuous electrodeionization,reverse osmosis,electrodialysis,or a combination thereof.Type IV reagent water may be produced with alternate technologies as long as the appropriate constituent speciﬁcations are met and that water so produced has been shown to be appropriate for the application where the use of such water is speciﬁed .EElectrical conductivity at 25°C.FElectrical resistivity at 25°C.GpH at 25°C,not applicable to higher resistivity waters.HTotal organic carbon.ISodium.JChloride ion.KHeterotrophic bacteria count.LEndotoxin in endotoxin units permL.devices typically comprise semi-permeable ion-exchange membranes and permanently charged ion-exchange media(see Test Method D6529).3.2.3reverse osmosis(RO)—the separation process where one component of a solution is removed from another compo-nent byﬂowing the feed stream under pressure across a semipermeable membrane.RO removes ions based on electro-chemical forces,colloids,and organics down to150molecular weight.May also be called hyperﬁltration(see Terminology D6161)position and Characteristics4.1The types and grades of water speciﬁed in this Standard shall conform to the requirements in Table1.5.Test Methods5.1Electrical Conductivity and Resistivity—Refer to Test Methods D1125and D5391.5.2pH—Refer to Test Methods D1293and D5128.5.3Silica—Refer to Test Method D4517.5.4Sodium—Refer to Test Methods D6071.5.5Chlorides—Refer to Test Method D5542.5.6TOC—Refer to Test Methods D5173and D5997. 5.7Endotoxins—Refer to LAL Test Method.45.8Microbiological Contamination—Refer to Test Methods F1094.6.Keywords6.1laboratory analysis;reagent;waterAPPENDIX(Nonmandatory Information)X1.POTENTIAL REAGENT WATER ISSUESINTRODUCTIONThis Appendix is provided as a guide to various issues in the production,application,storage,and monitoring of Reagent Water.These issues are very complex and extensive.This guidance is not intended to be comprehensive or complete.Producers and users of Reagent Water are encouraged to seek out additional sources of guidance in this area.X1.1PreparationX1.1.1Historically,reagent water Types I,II,III,and IV have been linked to speciﬁc process for their production. Starting with this revision,these types of waters may be produced with alternate technologies as long as the appropriate constituent speciﬁcations are met and that water so produced has been shown to be appropriate for the application where the use of such water is speciﬁed.X1.1.2The preparation methods of the various grades of reagent water inﬂuences the limits of impurities.Therefore,the selection of an alternate technology in place of the technology speciﬁed in the Table1should be made taking into account the potential impact of other contaminants such as micro-organism and pyrogens,even if a grade is not speciﬁed.Such contami-nants were not necessarily considered by the performance characteristics of the technology previously speciﬁed.X1.2Use and ApplicationX1.2.1Type I and Type III Water:X1.2.1.1Contact with the ion-exchange materials may cause an addition of organic contaminants to the water.This will depend on the resin type/quality,quality of the regenera-tions(if regenerated),environmental conditions in which the water puriﬁcation system is used and actual system use(for example,duration of non-use periods).Practices may be put in place to decrease the risk or organic contamination:(1)Periodic rinsing of the puriﬁcation media to limit bacteriological(organic)contamination is recommended.(2)After each period of non-usage,drawing off a quantity of water is necessary before use.Refer to the supplier speci-ﬁcations for the recommended volume.(3)Synthetic activated carbon and/or UV(dual wave-lengths185nm and254nm)may be used in the polishing stages to decrease the level of organic contaminants(to reach Type I water speciﬁcations),and/or to reach lower organic levels.X1.2.1.2The quality of the water produced depends upon the type,age,and method of regeneration of the ion exchange materials(if regenerated).Likewise,theﬂow rate through the ion exchange resin bed will change the conductivity of the product water.The manufacturer’s instructions for resins or the resin cartridge bed should be followed.X1.2.1.3The use of the membraneﬁlter in the preparation of Type I and Type III water may add a small amount of organic components to the water initially produced.The amount of organic components released differs depending on the type and brand of the membraneﬁlter used.Then the membrane should be rinsed according to the manufacturer’s 4Published in the U.S.Pharmacopeia by The U.S.Pharmacopeial Convention,Inc.instructions.The use of a qualiﬁed membraneﬁlter on the organic release is recommended.X1.2.1.4Producing Type I water speciﬁcations is achieved utilizing a combination of puriﬁcation technologies.The choice of technologies can vary depending on the feed water quality,system usage and cost considerations.Particular atten-tion should be taken regarding the location and sequence of particular puriﬁcation technologies in the process,as these can have an impact on theﬁnal water quality.X1.2.2Type II Water:X1.2.2.1The description of Type II reagent water was intended to characterize product water from distillation pro-cesses.Therefore,the selection of an alternate technology in place of the one speciﬁed should be made by taking into account the potential impact of other contaminants(such as micro-organism and pyrogen)than those speciﬁed in Table1 for the Type II water.X1.2.2.2Type II grade of reagent water is typically sterile and pyrogen-free as produced and generally may be used whenever freedom from biological contaminants is desirable. However,the method of storage and handling of the water may itself result in contamination.X1.2.2.3Type II water is typically pyrogen-free as pro-duced,but should be tested in conformance with the require-ments of the referenced edition of United States Pharma-copeia,if proof is needed.X1.2.3All Types of Water:X1.2.3.1Biological contaminants may be important in the test procedure using any of the reagent waters speciﬁed.A classiﬁcation of bacterial levels is included and should be speciﬁed if it is of signiﬁcance to the test being performed. X1.2.3.2It should also be noted that the method used to prepare the different types of reagent water may or may not remove non-ionized dissolved gases.If non-ionized dissolved gases are of concern for the application considered,the selection of a method to produce water appropriate for the purpose and compliant with the Table1speciﬁcations for the type and grade of water should be considered.X1.2.3.3To obtain sterile water,any of the types of reagent water listed in this section may be produced,bottled,and heated to121°C for20min.This procedure is most easily carried out by autoclaving at103kPa(15psi)for20min. Alternatively,sterilizingﬁltration of any types of the reagent water listed with a validatedﬁlter may also produce sterile water when performed in aseptic conditions.The user should choose the appropriate sterilization technique for the intended use.X1.3MonitoringX1.3.1The limits of Table1apply to the water sampled at the point of use or,when for practical reasons and/or to avoid contamination(for example connection of an equipment after a0.2µmﬁlter),as close as possible to the point of use and witha regular veriﬁcation of a low impact of the puriﬁcation steps and/or equipment placed downstream of the monitoring sam-pling point.X1.3.2Because atmospheric gases and impurities rapidly recontaminate exposed water,an on-line sensor should be employed for determining the electrical conductivity of reagent water Types I,II,and III.As atmospheric organic compounds and those from sampling vials rapidly contaminate exposed puriﬁed water,an on-line TOC monitor should be preferred for determining the TOC level of Type I and Type II water.X1.3.3Quality and system performance parameters should be regularly reported and registered.Follow-up of trends in the quality and performance parameters should be performed regularly to check any variations in performance of the water puriﬁcation installation and to be able to anticipate any failures.X1.3.4The monitoring of different parameters should be performed at a frequency deﬁned by the user to ensure with a high degree of conﬁdence that the water quality used is always compliant with the speciﬁcations and the purpose.X1.4Storage and DistributionX1.4.1Generally speaking,storage of the puriﬁed water will cause a loss of the speciﬁed characteristics.The impact will be different depending on the water type and grade produced(resistivity characteristics for example,will be rap-idly impacted as soon as Type I water is be stored).Water types,other than Type I,can be stored if particular attention is taken regarding the materials,design of the storage system and time of storage.The material of the storage reservoir in contact with water should be selected to minimize the release of extractables.X1.4.1.1The design of the storage reservoir should be fully drainable,either opaque or placed in an environment which limit bacterial growth by the effects of light.X1.4.1.2The storage container should be adequately pro-tected from air contaminants(particles and CO2,especially when water is drawn)and from bacteriological contamination. This should be achieved by airﬁltration,inert gas blanketing, UV irradiation,chemical sanitization,heating above80de-grees C,or a combination thereof.It should be recognized that the mere fact that the water is stored will likely reduce its purity despite attempts to prevent contamination.Storage should be sized to ensure a good turnover of water.X1.4.1.3Manual or automatic draw-off and periodic saniti-zation should be performed in particular after long periods of non-use.The periodicity of such draw-offs and sanitization should be deﬁned by the user depending on the water puriﬁ-cation system usage and water use.This periodicity can be deﬁned during a qualiﬁcation phase.After each sanitization, veriﬁcation of the absence of the sanitization agent should be performed.X1.4.2If a distribution system is used to transfer the water to a laboratory,it should be of special design to minimize contamination.Gravity feed is the preferred method(if pos-sible),since pumps are a potential source of contamination. X1.4.2.1If circulating systems are employed,the pumps should be designed to limit any contamination.X1.4.2.2The piping materials,ﬁttings,faucets,and joints should be designed to limit any contamination.X1.4.2.3Outlets should be protected by UV or by micro-ﬁltration(absolute0.22µmﬁlter)or other means to prevent “back contamination”by airborne biologicalimpurities.X1.4.2.4A loop distribution design is preferred to an antenna distribution,which can constitute a dead legs during periods of non-use.X1.4.2.5Positive pressure should be maintained in the distribution systems to avoid any retro-contamination.X1.4.2.6Microbiological proliferation should be minimized by suitable choice of periods of recirculation,ﬂow rate,and/or temperature.X1.5HandlingX1.5.1Extreme care should be taken in handling reagent water during analyses.Depending on the water type required and the applications performed,container material and clean-ing procedures must be chosen appropriately.Practices D5245 and D4453should be consulted.X1.5.2Laboratory-ware should be carefully selected ac-cording to the application.Low release plastic-ware,such as PFA or TFEﬂuorocarbon(except for analysis ofﬂuoride)or HDPE laboratory-ware should be used for ion-sensitive appli-cations and high purity glass containers may be preferable for organic-sensitive applications.X1.6Maintenance and CalibrationX1.6.1Periodic calibration(if pertinent)of the different measuring instruments should be performed to ensure the validity of the values obtained.X1.6.2Periodic preventive maintenance should be per-formed to ensure the long-term performance and reliability of the water puriﬁcation system.Follow-up of trends in the quality and performance parameters should be performed regularly to check any variations in performance of the installation and to be able to anticipate any failures.X1.6.3The frequency of system calibration and mainte-nance of the system should be deﬁned by the user depending on the importance of the water in applications,but should not be performed less than once a year.X1.7ValidationX1.7.1Because quality assurance is the key to ensure safety,efficiency and reliability,validation is becoming in-creasingly important.The validation process can be divided into4major qualiﬁcation steps:X1.7.1.1Design Qualiﬁcation(DQ)—The Design Qualiﬁ-cation is carried out before the selection of water puriﬁcation system is made and consists of deﬁning the water types required depending on the applications,and deﬁning the technology(ies)to be used,including the monitors to verify water quality.The design of the installation should also be deﬁned according to requirements.All steps should be docu-mented.X1.7.1.2Installation Qualiﬁcation(IQ)—The Installation Qualiﬁcation should take place after the installation of the system and consists of verifying and documenting that the installation was performed according to the predetermined speciﬁcations.This requires that the calibration of the various measuring instruments be veriﬁed.The actual installation should be compared with an installation drawing to ensure that no future installation modiﬁcation be performed without suit-able control management.Veriﬁcation of the availability of all documentation required to use and maintain the system should also be done.Documented veriﬁcation of the water puriﬁcation system may be performed to ensure that the installation was performed according to speciﬁcations.X1.7.1.3Operational Qualiﬁcation(OQ)—The Operational Qualiﬁcation is performed after installation of the system and consists of ensuring that the system is operating according to the predetermined speciﬁcations.Tests should be conducted to verify that the hydraulic,monitoring and electronic functions (including system alerts)of the systems are working according to the speciﬁcations.X1.7.1.4Performance Qualiﬁcation(PQ)—The Perfor-mance Qualiﬁcation should be carried out after that the installation and operational qualiﬁcation have been performed to document that the system is performing according to the predetermined speciﬁcations.During this qualiﬁcation step veriﬁcation of the appropriateness of the speciﬁcations,deﬁned according to the applications,and veriﬁcation of the water quality produced should be conducted.X1.7.2Re-qualiﬁcation should be conducted on a regular time-basis and also each time components are replaced which can affect the quality or the quantity of water.X1.7.2.1The frequency of re-qualiﬁcation depends on the importance of puriﬁed water in applications but cannot exceed one year.This ensures complete annual veriﬁcation of the system alerts and calibration of the measuring instrument.X1.7.2.2A preventive maintenance(see Maintenance and Calibration section)should be conducted regularly and all actions should be documented in a dedicated system logbook.ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentioned in this ers of this standard are expressly advised that determination of the validity of any such patent rights,and the risk of infringement of such rights,are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed everyﬁve years and if not revised,either reapproved or withdrawn.Your comments are invited either for revision of this standard or for additional standards and should be addressed to ASTM International Headquarters.Your comments will receive careful consideration at a meeting of the responsible technical committee,which you may attend.If you feel that your comments have not received a fair hearing you should make your views known to the ASTM Committee on Standards,at the address shown below.This standard is copyrighted by ASTM International,100Barr Harbor Drive,PO Box C700,West Conshohocken,PA19428-2959, United States.Individual reprints(single or multiple copies)of this standard may be obtained by contacting ASTM at the above address or at610-832-9585(phone),610-832-9555(fax),or service@(e-mail);or through the ASTM website().。

(完整)ASTM B858 06 翻译

ASTM B 858 06Standard Test Method forAmmonia Vapor Test for Determining Susceptibility toStress Corrosion Cracking in Copper Alloys用氨蒸气试验测定铜合金对应力腐蚀裂纹敏感性的试验方法标准1。

使用范围1.1 本测试方法描述了针对锻造铜合金产品，可能因应力腐蚀而开裂的残余应力的鉴定方法。

使用了氨蒸汽来进行该加速腐蚀试验。

1.2 本测试仅用于已知在氨蒸汽环境下对应力腐蚀裂纹敏感的铜合金制作的产品。

意图是制造一种可复制的恶劣环境来鉴定。

注: 我们知道裂纹机制的关键步骤是在样件上表面形成一种富含铜离子复合体的冷凝膜。

1。

3环境恶劣程度取决与腐蚀溶剂的PH值。

在附录A1里面给了四种不同的暴露环境，及根据不同环境风险程度采取的恰当的溶剂PH值。

1。

3.1 测试的PH值应当在产品规范里标注，或者由供应商及采购商相互协商一致，根据采取的合金牌号及其适用环境。

1.4 单位–测试值采取国际单位制标注，本标准内容不使用其他单位符号.1.5本标准没有描述进行本测试的一些安全注意事项。

请使用者自己评估相关的安全及健康因素来自行决定是否适用。

2。

参考文献2。

1 ASTM 标准：B 154 Test Method for Mercurous Nitrate Test for Copper Alloys铜合金硝酸亚汞试验法B 846 Terminology for Copper and Copper Alloys 铜及铜合金术语D 1193 Specification for Reagent Water 试剂规范3。

术语3。

1 相关的铜及铜合金术语请参照标准 B 846.3。

2 定义：3.2.1 外加应力：在施加外部负荷引起并存在于物体内部的应力4. 测试方法综述4.1 把准备好的测试样本放置于密闭容器，暴露在规定PH值环境温度的氨蒸汽环境中24小时。

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