GW_5074_LCMS_05142_MedChemExpress
CCG-1423_LCMS_14741_MedChemExpress
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 39Acq. Instrument : HY-LCMS-02 Location : Vial 37Injection Date : 1/19/2015 12:41:52 PM Inj : 1Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150119\20150119 2015-01-19 09-28-05\100-1000MS+3MIN( 0.02%FA).MLast changed : 1/19/2015 9:28:05 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_45-H01P(RP-HPLC).M Last changed : 1/19/2015 1:39:23 PM by Li Shan(LCMS-02) (modified after loading)Method Info : hplcCatalog No : HY-13991 Batch#14741 A-RP-124Additional Info : Peak(s) manually integratedmin0.511.52 2.53mAU200400600800 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...60\DATA\20150119\20150119 2015-01-19 09-28-05\BIZ2015-119-DJL1.D)1.6372.0362.189===================================================================== Area Percent Report =====================================================================Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDsSignal 1: DAD1 C, Sig=254,4 Ref=offPeak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.637 MM 0.0440 6.46704e-1 2.44930e-1 0.0233 2 2.036 MM 0.0430 1.14979 4.46148e-1 0.0414 3 2.189 MM 0.0432 2774.82788 1070.50586 99.9353Totals : 2776.62438 1071.19694===================================================================== *** End of Report ***=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 39Acq. Instrument : HY-LCMS-02 Location : Vial 37Injection Date : 1/19/2015 12:41:52 PM Inj : 1Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150119\20150119 2015-01-19 09-28-05\100-1000MS+3MIN( 0.02%FA).MLast changed : 1/19/2015 9:28:05 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_45-H01P(RP-HPLC).M Last changed : 1/19/2015 1:41:06 PM by Li Shan(LCMS-02) (modified after loading)Method Info : hplcCatalog No : HY-13991 Batch#14741 A-RP-124Additional Info : Peak(s) manually integratedmin0.511.522.53250005000075000100000125000150000175000200000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150119\20150119 2015-01-19 09-28-05\BIZ2015-119-DJL1.D) ES-API, Pos, Sca2.170MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.Reportable Ion Abundance: > 10%.Retention Mol. Weight Time (MS) MS Area or Ion2.170 1032280 477.00 I 457.10 I 456.00 I 455.00 I 172.15 I 130.20 I 105.10 Im/z10020030040050060020406080100*MSD1 SPC, time=2.144:2.199 of D:\AGLIENT 1260\DATA\20150119\20150119 2015-01-19 09-28-05\BIZ2015-119-DJL1.D ES-API,Max: 52740478.0518.0172.1456.0105.1458.0 477.0130.2455.0*** End of Report ***。
BMS-509744_LCMS_13091_MedChemExpress
File ..M32\1\DATA\20170316\CPK\CPK2017-316-13091.D Tgt Mass (EZX): 623.84 Injection Date : 16 Mar 17 4:18 pm +0800 Seq. Line : 0 Sample Name : CPK2017-316-13091 Location : P2-E-03 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M Catalog No: HY-11092 Batch#13091 Easy-Access Method: '1-POS-3MIN' 623.84 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min*0.511.522.5
mAU0250500750
*DAD1 B, Sig=214,4 Ref=off
1.3101.3271.4631.6191.7181.8841.997
min*0.511.522.5
mAU0100200300
*DAD1 C, Sig=254,4 Ref=off
1.2701.2941.3351.3481.4631.6441.7181.7971.8842.0852.106
Ispinesib_LCMS_14035_MedChemExpress
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 31Acq. Instrument : HY-LCMS-02 Location : Vial 28Injection Date : 12/3/2014 11:52:12 AM Inj : 1Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20141203\20141203 2014-12-03 09-19-06\100-1000MS+3MIN( 0.02%FA).MLast changed : 12/3/2014 9:19:06 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\DATA\20141202\20141202 2014-12-02 09-27-53\20-25A-80A,280.M (Sequence Method)Last changed : 12/3/2014 12:58:11 PM by Li Shan(LCMS-02) (modified after loading)Method Info : hplcCatalog No : HY-50759 Batch#14035 A-RP-32Additional Info : Peak(s) manually integratedmin0.511.522.53mAU200400600800 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...60\DATA\20141203\20141203 2014-12-03 09-19-06\BIZ2014-D03-DJL2.D)1.2331.6601.8111.9282.1122.2322.332===================================================================== Area Percent Report =====================================================================Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDsSignal 1: DAD1 C, Sig=254,4 Ref=offPeak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.233 MM R 0.0767 7.92390 1.25746e-1 0.2126 2 1.660 MF R 0.0582 3680.71851 1054.01758 98.7548 3 1.811 FM R 0.0464 29.57356 10.62216 0.7935 4 1.928 MM R 0.0442 2.51199 3.70863e-1 0.0674 5 2.112 MM R 0.0805 4.16557 8.62717e-1 0.1118 6 2.232 MM R 0.0133 7.54473e-2 9.48644e-2 2.024e-3 7 2.332 MM R 0.0520 2.16111 6.92374e-1 0.0580Totals : 3727.13008 1066.78630===================================================================== *** End of Report ***=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 31Acq. Instrument : HY-LCMS-02 Location : Vial 28Injection Date : 12/3/2014 11:52:12 AM Inj : 1Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20141203\20141203 2014-12-03 09-19-06\100-1000MS+3MIN( 0.02%FA).MLast changed : 12/3/2014 9:19:06 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\DATA\20141202\20141202 2014-12-02 09-27-53\20-25A-80A,280.M (Sequence Method)Last changed : 12/3/2014 12:59:50 PM by Li Shan(LCMS-02) (modified after loading)Method Info : hplcA-RP-32Additional Info : Peak(s) manually integratedmin0.511.522.53200000400000600000800000100000012000001400000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20141203\20141203 2014-12-03 09-19-06\BIZ2014-D03-DJL2.D) ES-API, Pos, ScaA r e a : 7.4202e +0061.673Catalog No : HY-50759 Batch#14035MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.Reportable Ion Abundance: > 10%.Retention Mol. Weight Time (MS) MS Area or Ion1.673 7420200 520.15 I 519.10 I 518.15 I 517.20 Im/z10020030040050060070020406080100*MSD1 SPC, time=1.634:1.725 of D:\AGLIENT 1260\DATA\20141203\20141203 2014-12-03 09-19-06\BIZ2014-D03-DJL2.D ES-API,Max: 608843520.2518.2 517.2*** End of Report ***。
WYE-354_LCMS_05047_MedChemExpress
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 40Acq. Instrument : HY-LCMS-02 Location : Vial 29Injection Date : 3/19/2015 12:15:07 PM Inj : 1Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150319\20150319 2015-03-19 09-00-09\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 3/19/2015 9:00:09 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\HY-303_17-H01RS(LCMS).M Last changed : 3/19/2015 1:43:31 PM by Li Shan(LCMS-02) (modified after loading)Method Info : HPLCCatalo No : HY-12034 Batch#05047 A-RP-132Additional Info : Peak(s) manually integratedmin0.511.52 2.53mAU 0100200300400 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...0\DATA\20150319\20150319 2015-03-19 09-00-09\CPK2015-319-05047.D)1.9752.077 2.204 2.284===================================================================== Area Percent Report =====================================================================Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDsSignal 1: DAD1 C, Sig=254,4 Ref=offPeak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.975 MM 0.1110 2.57448 3.86394e-1 0.2011 2 2.077 MM 0.0417 1264.46033 505.17441 98.7692 3 2.204 MM 0.0479 12.26776 4.26706 0.9583 4 2.284 MM 0.0430 9.14553e-1 3.54419e-1 0.0714Totals : 1280.21712 510.18228===================================================================== *** End of Report ***===========================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 40Acq. Instrument : HY-LCMS-02 Location : Vial 29Injection Date : 3/19/2015 12:15:07 PM Inj : 1Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150319\20150319 2015-03-19 09-00-09\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 3/19/2015 9:00:09 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\HY-303_17-H01RS(LCMS).M Last changed : 3/19/2015 1:45:26 PM by Li Shan(LCMS-02) (modified after loading)Method Info : HPLCCatalo No : HY-12034 Batch#05047 A-RP-132Additional Info : Peak(s) manually integratedmin0.511.522.53050000100000150000200000250000300000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150319\20150319 2015-03-19 09-00-09\CPK2015-319-05047.D) ES-API, Pos, Sc2.082MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.Reportable Ion Abundance: > 10%.Retention Mol. Weight Time (MS) MS Area or Ion2.082 1439827 496.80 I 495.90 Im/z100200300400500600020406080100*MSD1 SPC, time=2.054:2.109 of D:\AGLIENT 1260\DATA\20150319\20150319 2015-03-19 09-00-09\CPK2015-319-05047.D ES-API Max: 191360497.9496.8 495.9*** End of Report ***。
Miquelianin_LCMS_25140_MedChemExpress
File ..0629 2017-06-29 08-52-09\BIZ2017-629-WYQ5.D Tgt Mass (CHM): Injection Date : 29 Jun 17 2:07 pm +0800 Seq. Line : 60 Sample Name : BIZ2017-629-WYQ5 Location : P2-B-06 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\chem32\1\DATA\20170629\20170629 2017-06-29 08-52-09\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\DATA\20170629\20170629 2017-06-29 08-52-09\1-POS-3MIN.M Catalog No : HY-13930 Batch#25140 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min*0.511.522.5
mAU0200400600
*DAD1 B, Sig=214,4 Ref=off
1.2871.327
1.3921.581
min*0.511.522.5
mAU0200400
*DAD1 C, Sig=254,4 Ref=off
1.327
1.4831.5801.636
min0.511.522.5
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=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 112
Acq. Instrument : HY-LCMS-02 Location : Vial 69Injection Date : 1/15/2015 7:47:57 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150115\20150115 2015-01-15 09-25-46\100-1000MS+3MIN. M
Last changed : 1/15/2015 5:28:13 PM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_45-H01P(RP-HPLC).M Last changed : 1/16/2015 10:18:59 AM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc
Catalog No : HY-10542 Batch#05142 A-RP-32
Additional Info : Peak(s) manually integrated
min
0.5
1
1.52
2.53mAU 0
100200300400500600 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...0\DATA\20150115\20150115 2015-01-15 09-25-46\CPK2015-115-05142.D)
1.380
1.645
2.014
2.161
2.427
===================================================================== Area Percent Report =====================================================================
Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000
Do not use Multiplier & Dilution Factor with ISTDs
Signal 1: DAD1 C, Sig=254,4 Ref=off
Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------| 1 1.380 MM 0.0495 6.42098 2.16136 0.1687 2 1.645 MM 0.0471 13.03351 4.61549 0.3424 3 2.014 MF 0.0518 2077.23535 667.79926 54.5714 4 2.161 FM 0.0555 1706.59741 512.04071 44.8343 5 2.427 MM 0.0418 3.16856 1.26311 0.0832
Totals : 3806.45581 1187.87994
===================================================================== *** End of Report ***
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 112
Acq. Instrument : HY-LCMS-02 Location : Vial 69Injection Date : 1/15/2015 7:47:57 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150115\20150115 2015-01-15 09-25-46\100-1000MS+3MIN. M
Last changed : 1/15/2015 5:28:13 PM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_45-H01P(RP-HPLC).M Last changed : 1/16/2015 10:21:03 AM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc
Catalog No : HY-10542 Batch#05142 A-RP-32
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2
2.5
3
20000
400006000080000
100000120000140000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150115\20150115 2015-01-15 09-25-46\CPK2015-115-05142.D) ES-API, Pos, Sc
1.994
2.136
MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.
Reportable Ion Abundance: > 10%.
Retention Mol. Weight Time (MS) MS Area or Ion
1.994 114030 584.70 I 523.80 I 521.80 I 519.70 I 105.10 I
2.136 110932 52
3.70 I 521.70 I 519.75 I 105.10 I 102.20 I
m/z
100
200
300
400
500
600
700
800
9000
20
40
6080100*MSD1 SPC, time=1.963:2.018 of D:\AGLIENT 1260\DATA\20150115\20150115 2015-01-15 09-25-46\CPK2015-115-05142.D ES-API Max: 4793
545.6
279.1
352.3
830.2
223.1
297.0
101.1
586.6
564.8
520.7
130.1
584.7
523.8
105.1
521.8
m/z
1002003004005006007008009000
10203040
50
60
7080*MSD1 SPC, time=2.109:2.182 of D:\AGLIENT 1260\DATA\20150115\20150115 2015-01-15 09-25-46\CPK2015-115-05142.D ES-API
457.3
545.7
371.0
353.4
106.2
297.1
524.8
586.8 130.1
102.2
523.7
521.7
105.1
*** End of Report ***。