SY-2000S荧光硫说明书(英文版)

SY—2000N Chemiluminescentnitrogen detectorInstructions for use(V2.0)泰州市奥普特分析仪器有限公司TaiZhou City AoPuTe Analysis Instruments Co. Ltd.Recording1Foreword：SY-2000N Chemiluminescent nitrogen detector based on principle of chemiluminescence method combined with computer technology to develop next-generation precision laboratory instruments. Wide linear range, strong anti-jamming ability, simple, stable and reliable results, and highlight the advantages, which can be widely applied in petroleum, chemical industry, electric power, coal, food, environmental protection and other areas, is now more advanced sulfur analysis instrument.2The basic principle：SY-2000N Chemiluminescent nitrogen detector works as follows:1 ： SY-2000N Chemiluminescent nitrogen detector block diagramInstrument by the injector, cracking, ozone generators, reactor micro-current amplifier and, photoelectric conversion device, data processing system consists of several parts. When the sample is introduced after high temperature pyrolysis reactor, mixed with oxygen combustion and quantification of nitrogen compounds into NO, dehydration and carried by carrier gas dryer into the reaction Chamber, from ozone O3reaction excited NO2cm,Dang NO2﹡When you return to the ground state, issue a photon, the light received by a photomultiplier tube and consists of micro-current amplifier, data processing systems convert the displayed a luminous intensity is proportional to the signal, by measurement of chemiluminescence intensity to derive the total nitrogen content of the sample.The entire reaction can be represented as follows:High-temperatureR—N＋O2N O＋NO2+CO2＋H2ON O＋O3 N O2*＋O2N O2*N O2＋hγ'3Detailed technical parameters1Technical parameters:1.1Power supply voltage:AC220 v±10%1.2Power of the whole machine≤2200 W1.3Measuring range:0.1ppm—1%1.4Detection limit: 2 NG1.5Repeatability:Content of 0.1 ppm--1.0ppm Shi ±0.1ppmContents 1 ppm--10ppm Shi <10%Content >10 ppm Shi <5%1.6Baseline drift using : < 2uV/72h1.7Temperature range : room temperature ~1150 ° c1.8Temperature control accuracy: better than ±3° c1.9Cooling way: air cooler4Performance introduction4.1Wide range of application,Applies to total stability of light hydrocarbon gas, light oil or heavy oil Sulfur Determination of the content of.4.2Introduction of computer control and data processing.4.3Equipped with a printer directly prints analysis, analysis maps.4.4Instrument Dual CPU architecture functional,Performance and stability、Measuring accuracy of the results.4.5Combination of single-point calibration and multi-point calibration, automatically generated, save the calibration curve.4.6High measuring range (third gear attenuation).4.7High sensitivity (gain four).4.8Instrument software is simple, convenient, and easy to learn。

5System requirements5.1Environmental requirements:To ensure that the instruments can work properly, need to have the following environment conditions:1．Ambient temperature constant and cannot be above30degrees centigrade. 2．Must not contain corrosive gases in ambient air and dust, so as to avoid corrosion of parts, wiring short circuit.3．Spacious, airy instrumentation requirements, avoid direct exposure to sunlight.5.2Power requirements:1．Power supply voltage220V±5%/50HZ .2．Supply current is greater than15A.3．Have a good ground, resistance to ground is not more than3ω.5.3Air source:1．High purity oxygen:purity ≥99.9%2．High-purity argon gas: purity ≥99.9%6Equipment composition andinstallation6.1Opening inspection:After receiving the instrument user, against the packing list should be examined case-by-case, see if there are parts shortagesor damage occured, if there is a shortage or damage, should get in touch with the company.Note: before using this instrument, carefully read the instructions for all content, are familiar with the various components of the instrument, in order to avoid accidental operation damage the instrument, if service is required, it shall promptly notify the company.6.2System composition:6.2.1Hosts:1, response splitting part:Reaction. By two-stage Complete sample sulphide is converted S O2furnace computer control and display of temperature and the ambient temperature within the host, temperature control accuracy ±1%, flow control unit can control three way adjustment range is as follows: (cracked)50 ~ 500 ml/minO2(gas)30 ~ 300 ml/minO2(Carrier gas)30 ~ 300 mL/minArPart 2, detectorComplete the detection of fluorescence signals, amplification, and accept the computer control, to send the signal to the computer.6.2.2Computer system comprisingComputer systems including the host, monitor, printer, keyboard, mouse, and the corresponding computer software, dedicated data acquisition and control system. Complete temperature control, signal processing and control, intermediate and final results of the sample analysis.6.2.3Injector partsTo ensure constant speed sampling, the user can0.3 ul/sec≈1.2ul/sec Based on an analysis of requirements within the scope of selected sampling speed.6.2.4Pneumatic connectionsSystem air flow chart:5: System air flow chartNote: the instrument before use, clean all gas lines and fittings require.1．Flow control valve clockwise, will all flow to a minimum.Note: do not close the flow control valve, you should gently go can feel when there is resistance to, too much force can damage the valve.2． Inner diameter of3mm of stainless steel pipes, copper pipes or Teflon pipe imports argon argon gas source and host connected to source of oxygen and oxygen linked to imports.Note: requires source of oxygen with oxygen inlet connection between gas dryers (5A Molecular sieve).3.quartz cracked pipe installation（1）Host activities on both sides of the bezel is removed.（2）Saturate a cotton small amounts of solvent such as alcohol or acetone will wipe clean the tube wall, to remove the dirt and fingerprints.（3）Carefully place the Lysis tubes in cracking furnaces, the injector at the right side of the stove.（4）Splitting oxygen pipeline connected to the Lysis tube cracking oxygen imported, gas pipeline connected to the Lysis tube containing gas imports.（5）With four semi-circular ring of insulating ceramic (Lysis tube clips) to the Lysis tube and left end fixed.Note: you should enable the Lysis tube coaxial with the cracking furnace inside as much as possible, to ensure that pipe heat evenly.（6）Crystal cracked fitting the Lysis tube trailer, and connected to the equipment of the gas export and fitting clamp fitting and the Lysis tube end clamp.Note: to ensure the Lysis tube type ball grinding and not leak between the connector, you need to use sealing washers (silicone rubber).（7）Will host activities on both sides of the bezel installed.3.PTFE back panel of the pipeline will be connected to the gas-exportingand gas dryers, dryer with the host at the other end connected to the rear panel above the gas imports.More than pneumatic connection when the operation is complete, it is necessary to complete gas tightness check, to ensure that the gas leak, air flow has not stopped up, all gases from the exhaust only export outflows.6.2.5Electrical connection:1．In the back panel of the instrument's good ground earth terminal access. 2．Plug the supplied power cord into the power socket on the rear panel corresponds to.3．Connect the computer power cable in accordance with the operating instructions connect a computer system.Note: ensure all wiring connections and reliable, no loose.7Software installation and operating instructions7.1Install SY-2000N ProgramInstalling for the first time, follow these steps∶1． Power boot a computer into windowsXP operating systems2． The CD Setup and installation considerations for copying to your hard drive c:\SY in a subdirectory3.left mouse button double-click CD SETUP. EXEinto SY-2000N Setup.4.Follow the instructions in Setup, each click (Next) button, and thenclicking (Finish) button to complete the installation.Or basis directly from the CD Installation Notes install program. Note: the instrument is to give users in all application software is already installed, if the user is in use for some other reason you need to reinstall the SY-2000N program, you should uninstall the SY-2000N Setup andinstall SY-2000N Setup. How to uninstall please refer touninstalling SY-2000N Setup.7.2Uninstall SY-2000N SetupUninstall the SY-2000N Installer, follow these steps:1Open the WindowsXP [ Control Panel ], double-click [ add/territory remove programs ] icon, the system opens (adds HK remove programs) the dialog box.2In the dialog box list, select the "SY-2000N chemiluminescent nitrogen detector", and then click (add/territory remove) button, prompt box appears, select the "Yes" button to start thedelete SY-2000N chemiluminescent nitrogen detector program, then press OK button to complete the uninstall.8Start and quit SY-2000N programsOverviewInstall SY-2000N programUninstall SY-2000N programStart SY-2000N programsQuit SY-2000N programsSY-3000N Window and basic operation8.1OverviewThis chapter describes how to install the SY-2000N chemiluminescent nitrogen detector program. Prior please make sure Microsoft Windows XP or later is installed. If you do not use Windows menus, edit boxes, scroll bars, or dialog boxes you have questions, please refer to Windows XP operating system user's manual.Note:SY-2000N Installer Before installation, please keep it safe backup just in case.If you receive an upgraded version of the program, uninstall the original program, And then install the upgraded version of the program(See Uninstall SY-2000N programs).8.2StartYou can select the method to enter:1, Double-click windowsXP desktop SY-2000N shortcut icon chemiluminescent nitrogen detector:2、Click the windowsXP began , and then move the mouse pointer to pointto the program SY-2000N chemiluminescent nitrogen detector and its parent menu item under SY-2000N chemiluminescence nitrogen, and click the left mouse button on the menu.8.3ExitYou can select the method exit1． Select from the file menu (exit).2． Quick on the button bar, click the close button.9Power on:In accordance with the instructions for use keep full equipment electricity, gas, ground connection is good, check for leakage, or leakage, make sure that is correct, and then follow these steps to power on the system.（1）Gas purging:To ensure the instrument often work under, power should be gas before blowing to remove water vapour and other impurities in the gas. This is a new instrument and the instrument is not used for a long time is particularly important.Gas purging method: flow control valve counterclockwise, moved three meters are to15Notches, purging10Minutes or so.（2）Power upOpen the power distribution box, or total power supply distribution Board, reopening the entire instrument, instrument power up, boot the computer, enter the Windows The operating system.Note:Enter SY-2000N Program cannot run other applications, has exited other applications should be running and shuts down. Windows window then click on Start, and settings , and Control Panel , and powermanagement ,power schemes , and waiting for the State of the system , and turn off the monitor , And turn off hard disks , these four sets for the never option. Otherwise, the SY-2000N program may not run correctly to avoid damage to the instrument, such as over-temperature of cracking furnace, electric wire burned.（3）Gas flow selection①Cracking O2Airflow:This road O2Gas flow rate directly affects the size of the sampleconversion of oxidative pyrolysis, effects samples into sulphide in SO2rates. Analysis when making cracking o2gas in excess, to ensure full combustion of samples, Lysis tube does not generate carbon, while traffic also should not be too large, otherwise not conducive to theresponses, sample fluorescence transformation of sulfides as SO2intensity is reduced.General analysis of condition, can be cracked O2Air flow adjustmentto150~500ml/min Within the scope of.②Ar Airflow:Ar As the carrier gas, the volatile samples carry into the cracked pipe of high temperature parts, oxidative pyrolysis of samples. General requirements for Ar gas flow in the60~400ml/min range, users can high and low sulfur content of samples, sample size and cracking of o2gas flow, such as the size of the selection of suitable Ar gas flows.③O2Airborne gas flow:General analysis of liquid samples of relatively light distillate, gas can be without this road. When the samples are less volatile,and Ar gas by adding a certain amount of o2gas together as the carrier gas, can promote the gasification of the samples.（4）SY-2000N Program startsAs mentioned earlier, run SY-2000N Program, enter the standard sample, sample analysis.10Sample analysis:Analysis of liquid samples, for example the following describes the basic operation of samples and some problems should be noticed.1． Sample preparation:Analysis unknown samples by fluorescence analysis of sulfur method, first get the response value of an unknown sample, namely integration area and sulfur content of unknown sample results are based on the same points of reference materials in the condition area, reference materials and sample weight of unknown, unknown score calculated data such as size of the sample. Therefore, prior to the analysis of unknown samples, to pre-select a number of different concentration of standard samples, sample selection should pay attention to the following several points:（1）With suitable sulfur compounds as solute:（2）With the appropriate solvent, samples, and unknown samples in the sample matrix as close as possible.（3）Use within the warranty period of the standard sample, sample shelf life is one year, so that samples need to be kept. Solutes andsolvents are volatile substances the samples should be kept inrefrigerated containers, to prolong its service life.2． Sample analysisAs mentioned before sample analysis, first select the appropriate sample, sample curve, the concentration of the samples in the standard curve, to ensure sample analysis data is accurate and reliable, if the concentration of the samples in the standard curve in addition to and exceed the minimum sample concentration10%~20%, Or micro-current amplifier saturation (peak shape for flat peak, need to replace the quantum), asked to reselect the sample making standard curves.11Shutdown:Subject to the instrument after use, shut down by doing the following:1． Turn off the UV lamp power supply, cooling by temperature controller button, turn off the furnace power.2． Power down the host, injector, for a few minutes and pneumatic clean after, turn off the gas.3． For two hours, after the temperature dropped off fan switch.4． By balloon tips quit SY-2000N programs into Windows exit window, power off the computer, monitor, printer.5． Distribution box, or power Board total power is off.12Reaction chamber-cleaningBecause the instrument used for a long time. Reaction indoor residue deposits, resulting in a lower sensitivity, analysis results are not repeated, so users should be based on the use of regular cleaning Chamber. The sediment may be powdered or likely to be oily, its color may be yellow, Brown or black, which mainly depends on the type and operating conditions of the analysis sample, such as material feed speed too high, lack of oxygen, the oven temperature is too low.Cleaning process is as follows:1． Turn off all power switches.2． Open the cover, unplug the darkroom high voltage power and signal plugs, disconnected lines.3． Release the dark base and back panel screws, take out the darkroom later, release the dark end cap fixing screws. (Air road pipelines of end caps).Note: photomultiplier tube-side window shows up, the needs in-side window with a piece of black cloth to block the light.4． Remove Chamber cover screws, carefully removing the gland, filters, Quartz. If the "o"-ring broken, replace it with new.5． Cleaned the mirrors of wadded paper with high silica film and filters, wipe with clean soft cloth with no hair reaction indoor wall, if necessary, get scrubbed clean with acetone or ethanol, and oxygen blow dry.6． Reaction chamber-cleaning is complete, again in order to install.Note: when fixed optical filters, quartz, and action should be smooth, degree of tightening to ensure airtight, beware of filters, quartz plate rupture. Filters, quartz plate location do not install anti-, quartz reaction indoor wall that protects the filter.7． Fixed to the Chamber after Chamber, anechoic chamber attached to the detector, and connect all cables and gas pipelines to avoid leaks, leakage phenomenon.8． Cover the cover.13Instrument maintenance1． Long-term use of the system, pneumatic joints leakage may occur, users response to the gas as a whole do not regularly checked.2． Users should always check after cracking tube outlet port and with and without the carbon in the gas circuit. If cracking tubes of carbon deposition in, you can access oxygen combustion in high temperature conditions clear. If carbon deposits in the pipeline. The timely replacement of new line.3． Users should be required to replace the oxygen desiccant, to ensure that the system is functioning properly.Note:1. Air drier stuffing (5A molecular sieve ) Processing method : 500 Temperatures, activation of 4 Hours.4． Check the use of cracked pipes on a regular basis, if the cracked pipe wall becomes white and rough, instructions for quartz tube lifetime had to, it should be replaced immediately. Analysis of low concentration samples usually, demanding to the Lysis tube, cracked pipe inner wall roughness can lead to drop in its signal strength decreases, lower sensitivity, resolution, Lysis tube on low concentration sample analysis does not apply may also apply to the analysis of high content of samples. 5． Periodic cleaning Chamber, cleaning methods, see the fifth chapter. 6． Injector regularly driven screw Guide bar and add lubricant to reduce wear and noise.Workstation main interface:Workstation's main operations Description:1、Control keysA、Start: the instrument starts automatically sentenced peak, the measurementsignal points.B、End: end the analysis of standard samples, or samples, calculation of theaverage results, starting the next sample or specimen analysis.C、Save curve: saves the current curve curve data in the list.D、Exit: exits the application.2、Gas flow setting interface:Airflow can be adjusted for tuning key can also be entered in the edit box.OK Key to confirm.3、The amplification of the signal processing:The amplification of the signal is divided into two levels, first level: micro-current amplifier; second level: normal voltage amplifier. Magnification levels are available through the interface of the radio button selected.4、Temperature setting:Temperature can be adjusted for tuning key can also be entered in the edit box.OK Key to confirm.5、Toolbar buttons:Analysis is often used toolbar buttons are buttonsA、New construction: new analysis.B、Open: open curves that already exists, and call it.C、Save: save analysis results.D、Preview: print preview.E、Online: Instrumentation and computer communication.F、Status: setting the instrument's working state.G、Unit: mg/L PPm Unit conversion.H、Gain: instrumental measurement signal amplification and processing.I、Air flow: setting the airflow.J、Heating: heated up.K、Temperature: instrument stopped heating up.L、Ozone: ozone generator on and off.M、Exit: exits the application.。