EPZ-6438_LCMS_25148_MedChemExpress
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File ..30-1 2017-06-30 11-02-05\BIZ2017-630-WYQ7.D Tgt Mass (CHM):
Injection Date : 30 Jun 17 12:56 pm +0800 Seq. Line : 22
Sample Name : BIZ2017-630-WYQ7 Location : P2-B-04
Acq. Operator : CLJ_701 Inj : 1
Spec. Reported : MS Integration Inj Volume : 1 ul
Acq. Method : D:\chem32\1\DATA\20170630\20170630-1 2017-06-30 11-02-05\1-POS-3MIN.M
Analysis Method : D:\CHEM32\1\DATA\20170630\20170630-1 2017-06-30 11-02-05\1-POS-3MIN.M
Catalog No : HY-13803 Batch#25148 A-RP-186
Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)
Gradient: 5% to 95%B within 1.3 min
Flow Rate :1.8ml/min
Column :SunFire C18, 4.6*50mm,3.5um A-RP-186
Oven Temperature : 45C
min
0.511.522.5
mAU
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DAD1 B, Sig=214,4 Ref=off
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DAD1 C, Sig=254,4 Ref=off
1.1211.1881.3061.3471
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0.511.522.5
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MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
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Ion 573.3, MSD1 573.3,Target Mass 572.3 +H Positive, EIC=573:574
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Integration Results for DAD1 B, Sig=214,4 Ref=off
RetTim Width Area Height Area% MS(+)
|-------|--------|--------------|--------------|--------|------|
1.14 0.02 2.08 1.89 0.11 ND
1.19 0.02 1790.99 1525.23 97.36 287
1.31 0.02 27.87 24.19 1.51 287
1.35 0.02 7.54 5.48 0.41 397
1.43 0.02 11.17 8.43 0.61 ND
Integration Results for DAD1 C, Sig=254,4 Ref=off
RetTim Width Area Height Area% MS(+)
|-------|--------|--------------|--------------|--------|------|
1.12 0.05 0.85 0.16 0.06 ND
1.19 0.02 1308.85 1126.86 98.20 287
1.31 0.02 16.72 13.32 1.25 287
1.35 0.03 3.54 2.93 0.27 397
1.42 0.03 2.91 0.12 0.22 ND
Integration Results for MSD1 TIC, MS File
RetTim Width Area Height Area% MS(+)
MS Report from Instrument: LCMS-02
LCMS-02 6/30/2017 13:18:00 CLJ_701
Page 1 of 3
|-------|--------|--------------|--------------|--------|------|
1.21 0.04 719486.69 321839.81 88.52 287
1.35 0.06 93319.45 25596.95 11.48 397
MS Report from Instrument: LCMS-02
LCMS-02 6/30/2017 13:18:00 CLJ_701
Page 2 of 3
Ret. Time: 1.21 <<<< POSITIVE SPECTRA >>>>
m/z
200300400500600700800900
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ES-API Positive
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Ret. Time: 1.35
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200300400500600700800900
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ES-API Positive
398.1 681.3 340.0 305.0 612.1 1
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130.2 206.0 4
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MS Report from Instrument: LCMS-02
LCMS-02 6/30/2017 13:18:00 CLJ_701
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