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Compact Enclosures AX 产品说明书

COMPACT ENCLOSURES AX Technical detailsCompact enclosuresContentsCompact enclosures AX, sheet steelBasic enclosure AXWall-mounted enclosure AX ITwith 482.6 mm (19") mounting anglesCommand panel AX with handle stripsCommand panel AX for desktop TFT up to 24"Model No. AX Width mm Height mm Depthmm Camlock 3-point locking systemPage 1031.0003803002101– 4 – 51033.0003003002101– 4 – 51034.0003004002101– 4 – 51037.0004008003002– 4 – 51038.0003806002102– 4 – 51039.0006003802101– 4 – 51045.0004005002102– 4 – 51050.0005005002102– 4 – 51054.0006006002502– 4 – 51055.0008006003002– 6 – 71057.0005007002502– 4 – 51058.0006008002502– 4 – 51059.0006008004002– 4 – 51060.0006006002102– 4 – 51073.0007607603002– 6 – 71076.0006007602102– 4 – 51077.0007607602102– 6 – 71090.00060010002502– 4 – 51091.00060010004002– 4 – 51100.00010007602102–12 – 131110.000100010003002–12 – 131114.00010001,400300–◾14 – 151115.00010001,400400–◾14 – 151116.00012001200400–◾14 – 151130.00010007603002–12 – 131180.00080010003002– 6 – 71181.00080010004002– 6 – 71213.00010001200300–◾14 – 151214.00010001200400–◾14 – 151260.0006001200300–◾8 – 91261.0006001200400–◾8 – 91280.0008001200300–◾10 – 111281.0008001200400–◾10 – 111338.0003806003502– 4 – 51339.0006003803501– 4 – 51350.0005005003002– 4 – 51360.0006006003502– 4 – 51376.0006007603502– 4 – 51380.0003803802101–4 – 5Model No.AX Width mm Height mm Depth mm Page 7641.350600380350207643.350600600350207645.350600760350207646.40060080040020Model No.AX Width mm Height mm Depth mm Page 6315.150300300210216315.250380300210216315.350380380210216315.450500500210216315.650600600210216320.050300200155226320.350380380210226320.450500500210226320.550600380210226320.65060060021022Model No.AX Width mm Height mm Depth mm Page 6321.05065045015523Compact enclosures AX, stainless steelBasic enclosure AXModel No. AX Width mm Height mm Depthmm Camlock 3-point locking systemPage 1003.0003003002101–16 – 171005.0003003802101–16 – 171006.0003803802101–16 – 171007.0005005002102–16 – 171008.0003806002102–16 – 171009.0006003802101–16 – 171010.0006006002102–16 – 171011.0003803002101–16 – 171012.0006007602102–16 – 171013.0005005003002–16 – 17Model No. AX Width mm Height mm Depthmm Camlock 3-point lockingsystemPage1014.0007607603002–16 – 171015.0004005002102–16 – 171016.00080010003002–16 – 171017.0008001200300–◾181018.000100010003002–191019.00010001200300–◾191302.0003003802101–16 – 171303.0003803802101–16 – 171304.0006006002102–16 – 171305.00010001200300–◾19Compact enclosuresCompact enclosures Compact enclosures AX, sheet steelBasic enclosure AXwith cam lock and one gland plateSection B – BSection A – ADrilled holes for eyebolts(only for 1059.000/1091.000)Drilled holes for base/plinth(only for 1059.000/1091.000)Door interior viewCentral hinge, only where H1 > 800 mmCentral embossed half-shear,only where B1/H1 ≥ 500 mmNot applicable to B1 = 300 mmOne central cam where H1 ≤ 400 mmTwo cams where H1 > 400 mmCompact enclosuresCompact enclosures AX, sheet steelBasic enclosure AXwith cam lock and one gland plate Model N o. AXWidth dimensionsmmHeight dimensionsmm Depth dimensionsmmMounting platemm Gland plate mm B1B2B3B4B5B6B7H1H2H3H4H6N T1T2T3T7F1F2G1G2TypeMOType 1031.000380374332.7289.5305340303300294256.51502606209.7187.0189.0113330280275250233914921033.000300294252.7209.5225260220300294256.51502606209.7187.0189.0113250200275250225614911034.000300294252.7209.5225260220400394356.525036010209.7187.0189.0113250200375350225614911037.000400395352.2309.532536026580079575665076026300.7277.5278.7185345300775750130122151038.000380374332.7289.5305340303600594556.545056018209.7187.0188.5113330280575550233914921039.000600594552.7509.5525560498380374336.525034010209.7187.0188.5113550500355330253414941045.000400394352.7309.5325360303500494456.535046014209.7187.0189.0113350300475450233914921050.000500494452.7409.5425460411500494456.535046014209.7187.0188.5113450400475450244714931054.000600594552.2509.552556049860059455645056018250.2227.5228.7113550500575550253414941057.000500495452.2409.542546041170069565655066022250.7227.5228.7113450400675650244714931058.000600595552.2509.552556049880079575665076026250.7227.5228.7113545500775750153414941059.000600595552.2509.552556040080079575665076026400.7377.5378.7185545500775750143622171060.000600594552.2509.552556049860059455645056018210.2187.5188.7113550500575550253414941076.000600595552.2509.552556049876075571660072024210.7187.5188.7113550500735710253414941090.000600595552.2509.5525560498100099595685096034250.7227.5228.7113545500975950153414941091.000600595552.2509.5525560400100099595685096034400.7377.5378.7185545500975950143622171338.000380374332.2289.5305340265600594556.545056018350.2327.5328.7185330280575550230122151339.000600594552.2509.552556040038037433625034010350.2327.5328.7185550500355330243622171350.000500494452.2409.542546036550049445635046014300.2277.5278.7185450400475450240122161360.000600594552.2509.552556040060059455645056018350.2327.5328.7185550500575550243622171376.000600595552.2509.552556040076075571660072024350.7327.5328.7185550500735710243622171380.000380374332.7289.5305340303380374336.525034010209.7187.0189.011333028035533023391492EnclosureB1=Enclosure width (overall width)B2=Door widthB3=Clearance width, enclosure opening B4=Clearance width between door profilestripsB5=Mounting distance, door profile strips B6=Mounting distance, enclosures B7=Gland plate openingH1=Enclosure height (overall height)H2=Door heightH3=Clearance height, enclosure opening H4=Overall height, 25 mm pitch patternof holesH6=Mounting distance, enclosuresN =No. of 25 mm pitch patterns of holes T1=Overall depth T2=Enclosure depthT3=Installation depth (distance from insideof door to mounting plate)T7=Gland plate openingMounting plateF1=Mounting plate width F2=Centre-to-centre spacingof the attachment holes G1=Mounting plate height G2=Centre-to-centre spacingof the attachment holes Gland plateM =Gland plate width O =Gland plate depth Type = Size of gland plateMounting plate type 1, with edge foldMounting plate type 2, without edge foldDetail YSection C – CCompact enclosuresCompact enclosures AX, sheet steel Basic enclosure AXwith cam lock and two gland platesDoor interior viewCentral hinge, only where H1 > 800 mm Central embossed half-shear,only where B1/H1 ≥ 500 mmNot applicable to B1 = 300 mmDrilled holes for eyebolts(only for 1055.000/1180.000/1181.000)Drilled holes for base/plinth(only for 1055.000/1180.000/1181.000)Section B – BSection A – ACompact enclosuresCompact enclosures AX, sheet steelBasic enclosure AXwith cam lock and two gland plates Model No.AXWidth dimensionsmmHeight dimensionsmm Depth dimensionsmm Mounting platemm Gland platemmB1B2B3B4B5B6B7H1H2H3H4H5H6NT1T2T3T4T7F1F2G1G2Type MO Type1055.000800795752.2709.572576026560059555645056018518300.7277.5278.7187.5185750700575550230122151073.000760755712.2669.568572026576075571660072018524300.7277.5278.7–185705660735710130122151077.000760755712.2669.568572030376075571660072011324210.7187.5188.7–113705660735710133914921180.000800795752.2709.5725760265100099595685096018534300.7277.5278.7187.5185745700975950130122151181.000800795752.2709.5725760265100099595685096018534400.7377.5378.7287.518574570097595013012215EnclosureB1=Enclosure width (overall width)B2=Door widthB3=Clearance width, enclosure opening B4=Clearance width between door profilestripsB5=Mounting distance, door profile strips B6=Mounting distance, enclosures B7=Gland plate openingH1=Enclosure height (overall height)H2=Door heightH3=Clearance height, enclosure opening H4=Overall height, 25 mm pitch patternof holesH5=Mounting distance, enclosuresN =No. of 25 mm pitch patterns of holes T1=Overall depth T2=Enclosure depthT3=Installation depth (distance from insideof door to mounting plate)T4=Spacing between holes for base/plinth T7=Gland plate openingMounting plateF1=Mounting plate width F2=Centre-to-centre spacingof the attachment holes G1=Mounting plate height G2=Centre-to-centre spacingof the attachment holes Gland plateM =Gland plate width O =Gland plate depthType = Size of gland plateMounting plate type 1, with edge foldDetail YSection C – CMounting plate type 2, without edge foldCompact enclosuresCompact enclosures AX, sheet steel Basic enclosure AXwith 3-point locking system and one gland plateDrilled holes for eyeboltsDrilled holes for base/plinthSection B – BSection A – ADoor interior viewCentral hinge, only where H1 > 800 mm Central embossed half-shear,only where B1/H1 ≥ 500 mmCompact enclosuresCompact enclosures AX, sheet steelBasic enclosure AXwith 3-point locking system and one gland plateModel No.AXWidth dimensionsmmHeight dimensionsmm Depth dimensionsmm Mounting platemm Gland platemmB1B2B3B4B5B6B7H1H2H3H4H5H6NT1T2T3T4T7F1F2G1G2Type MO Type1260.000600595552.2459.54755604001200119511561050534.7116042300.7277.5277.2187.518554550011751150143622171261.000600595552.2459.54755604001200119511561050534.7116042400.7377.5377.2287.51855455001175115014362217EnclosureB1=Enclosure width (overall width)B2=Door widthB3=Clearance width, enclosure opening B4=Clearance width between door profilestripsB5=Mounting distance, door profile strips B6=Mounting distance, enclosures B7=Gland plate openingH1=Enclosure height (overall height)H2=Door heightH3=Clearance height, enclosure opening H4=Overall height, 25 mm pitch patternof holesH5=Distance from bottom edge of doorto bottom edge of lock plate H6=Mounting distance, enclosuresN =No. of 25 mm pitch patterns of holes T1=Overall depth T2=Enclosure depthT3=Installation depth (distance from insideof door to mounting plate)T4=Spacing between holes for base/plinth T7=Gland plate opening Mounting plateF1=Mounting plate width F2=Centre-to-centre spacingof the attachment holes G1=Mounting plate height G2=Centre-to-centre spacingof the attachment holes Gland plateM =Gland plate width O =Gland plate depth Type = Size of gland plateMounting plate type 1, with edge foldDetail YSection C – CCompact enclosuresCompact enclosures AX, sheet steel Basic enclosure AXwith 3-point locking system and two gland platesDrilled holes for eyeboltsDrilled holes for base/plinthDoor interior viewCentral hinge, only where H1 > 800 mm Central embossed half-shear,only where B1/H1 ≥ 500 mmSection A – ASection B – BCompact enclosures AX, sheet steelBasic enclosure AXwith 3-point locking system and two gland platesModel No.AXWidth dimensionsmmHeight dimensionsmm Depth dimensionsmm Mounting platemm Gland platemmB1B2B3B4B5B6B7H1H2H3H4H5H6NT1T2T3T4T7F1F2G1G2Type MO Type1280.000800795752.2659.56757602651200119511561050534.7116042300.7277.5278.7187.518574570011751150130122151281.000800795752.2659.56757602651200119511561050534.7116042400.7377.5378.7287.51857457001175115013012215Detail YSection C – CEnclosureB1=Enclosure width (overall width)B2=Door widthB3=Clearance width, enclosure opening B4=Clearance width between door profilestripsB5=Mounting distance, door profile strips B6=Mounting distance, enclosures B7=Gland plate openingH1=Enclosure height (overall height)H2=Door heightH3=Clearance height, enclosure opening H4=Overall height, 25 mm pitch patternof holesH5=Distance from bottom edge of doorto bottom edge of lock plate H6=Mounting distance, enclosuresN =No. of 25 mm pitch patterns of holes T1=Overall depth T2=Enclosure depthT3=Installation depth (distance from insideof door to mounting plate)T4=Spacing between holes for base/plinth T7=Gland plate opening Mounting plateF1=Mounting plate width F2=Centre-to-centre spacingof the attachment holes G1=Mounting plate height G2=Centre-to-centre spacingof the attachment holes Gland plateM =Gland plate width O =Gland plate depth Type = Size of gland plateMounting plate type 1, with edge foldCompact enclosures AX, sheet steel Basic enclosure AXwith cam lock, two-doorDrilled holes for eyebolts (not applicable to 1100.000)Drilled holes for base/plinth (not applicable to 1100.000)Section A – ASection B – BDoor interior viewCentral hinge, only where H1 > 800 mm Central embossed half-shear,only where B1/H1 ≥ 500 mmCompact enclosures AX, sheet steelBasic enclosure AXwith cam lock, two-doorModel No. AX Width dimensions mmHeight dimensions mm Depth dimensions mm B1B2B3B4B5B6B7B8B9H1H2H3H4H6N T1T2T3T4T71100.0001000495952.4409.5425960411359.537576075571660072024210.7187.5188.7– 1131110.0001000495952.4409.5425960365359.5375100099595685096034300.7277.5278.7187.51851130.0001000495952.4409.5425960365359.537576075571660072024300.7277.5278.7187.5185Model No. AX Mounting plate mmGland plate mmF1F2G1G2Type M O Type 1100.000945900735710144714931110.000945900975950140122161130.00094590073571014012216EnclosureB1=Enclosure width (overall width)B2=Door widthB3=Clearance width, enclosure opening B4=Clearance width between door profilestrips, hinged door (left-hand door) B5=Mounting distance, door profile strips,hinged door (left-hand door)B6=Mounting distance, enclosures B7=Gland plate openingB8=Clearance width between door profilestrips, locked door (right-hand door)B9=Mounting distance, door profile strips,locked door (right-hand door)H1=Enclosure height (overall height)H2=Door heightH3=Clearance height, enclosure opening H4=Overall height, 25 mm pitch patternof holesH6=Mounting distance, enclosuresN =No. of 25 mm pitch patterns of holes T1=Overall depth T2=Enclosure depthT3=Installation depth (distance from insideof door to mounting plate)T4=Spacing between holes for base/plinth T7=Gland plate opening Mounting plateF1=Mounting plate width F2=Centre-to-centre spacingof the attachment holes G1=Mounting plate height G2=Centre-to-centre spacingof the attachment holes Gland plateM =Gland plate width O =Gland plate depth Type = Size of gland plateDetail YSection C – CMounting plate type 1, with edge foldCompact enclosures AX, sheet steelBasic enclosure AXwith 3-point lock system, double-doorDrilled holes for eyeboltsDrilled holes for base/plinthSection A – ASection B – BDoor interior viewCentral hinge, only where H1 > 800 mm Central embossed half-shear,only where B1/H1 ≥ 500 mmCompact enclosures AX, sheet steelBasic enclosure AXwith 3-point lock system, double-door Model No.AX Width dimensions mmHeight dimensions mm Depth dimensions mm B1B2B3B4B5B6B7B8B9H1H2H3H4H5H6N T1T2T3T4T71213.0001000495952.4409.5425960365359.53751200119511561050534.7116042300.7277.5278.7187.51851114.0001000495952.4409.5425960365359.53751,400139513561250634.7136050300.7277.5278.7187.51851214.0001000495952.4409.5425960365359.53751200119511561050534.7116042400.7377.5378.7287.51851115.0001000495952.4409.5425960365359.53751,400139513561250634.7136050400.7377.5378.7287.51851116.00012005951152.4509.55251160400459.54751200119511561050534.7116042400.7377.5378.7287.5185Model No.AX Mounting plate mmGland plate mmF1F2G1G2Type M O Type1213.00094590011751150140122161114.00094590013751350140122161214.00094590011751150140122161115.00094590013751350140122161116.000114511001175115014362217EnclosureB1=Enclosure width (overall width)B2=Door widthB3=Clearance width, enclosure opening B4=Clearance width between door profilestrips, hinged door (left-hand door) B5=Mounting distance, door profile strips,hinged door (left-hand door)B6=Mounting distance, enclosures B7=Gland plate openingB8=Clearance width between door profilestrips, locked door (right-hand door)B9=Mounting distance, door profile strips,locked door (right-hand door)H1=Enclosure height (overall height)H2=Door heightH3=Clearance height, enclosure opening H4=Overall height, 25 mm pitch patternof holesH5=Distance from bottom edge of doorto bottom edge of lock plate H6=Mounting distance, enclosuresN =No. of 25 mm pitch patterns of holesT1=Overall depth T2=Enclosure depthT3=Installation depth (distance from insideof door to mounting plate)T4=Spacing between holes for base/plinth T7=Gland plate opening Mounting plateF1=Mounting plate width F2=Centre-to-centre spacingof the attachment holes G1=Mounting plate height G2=Centre-to-centre spacingof the attachment holes Gland plateM =Gland plate width O =Gland plate depth Type = Size of gland plateDetail YSection C – CMounting plate type 1, with edge foldCompact enclosures AX, stainless steel Basic enclosure AXwith cam lock, single-doorSection B – BSection A – ADetail Y Section C – CDoor interior viewCentral hinge, only where H1 > 800 mmCentral embossed half-shear,only where B1/H1 ≥ 500 mmNot applicable to B1 = 300 mmCompact enclosures AX, stainless steelBasic enclosure AXwith cam lock, single-door Model No.AX Width dimensions mmHeight dimensions mm Depth dimensions mm Mounting plates mm B1B2B3B6B10H1H2H3H6H10T1T2T3F1F2G1G2Type 1003.000300294256.5260225300294256.5260205209.4187.0189.925020027525021005.000300294256.5260225380374336.5340285209.4187.0189.925020035533021006.000380374336.5340305380374336.5340285209.4187.0189.933028035533021007.000500494456.5460425500494456.5460405209.4187.0189.945040047545021008.000380374336.5340305600594556.5560505209.4187.0189.933028057555021009.000600594556.5560525380374336.5340285209.4187.0189.955050035533021010.000600594556.0560525600594556560505209.4187.5189.955050057555021011.000380374336.5340305300294256.5260205209.4187.0189.933028027525021012.000600595556.0560525760755716.5720665209.4187.5189.955050073571021013.000500494456.0460425500494456.5460405300.4277.5280.945040047545021014.000760755716.0720685760755716.5720665300.4277.5280.970566073571011015.000400394356.5360325500494456.5460405209.4187.0189.935030047545021016.000800795756.07607251000995956.5960905300.4277.5280.974570097595011302.000300294256.5260225380374336.5340285209.4187.0189.925020035533021303.000380374336.5340305380374336.5340285209.4187.0189.933028035533021304.000600594556.0560525600594556.5560505209.4187.5189.95505005755502EnclosureB1=Enclosure width (overall width)B2=Door widthB3=Clearance width, enclosure opening B6=Mounting distance, enclosures B10=Distance between threaded bolts H1=Enclosure height (overall height)H2=Door heightH3=Clearance height, enclosure opening H6=Mounting distance, enclosures H10=Distance between threaded boltsT1=Overall depth T2=Enclosure depthT3=Installation depth (distance from insideof door to mounting plate) Mounting plateF1=Mounting plate widthF2=Centre-to-centre spacingof the attachment holes G1=Mounting plate height G2=Centre-to-centre spacingof the attachment holesMounting plate type 1, with edge foldMounting plate type 2, without edge foldCompact enclosures AX, stainless steel Basic enclosure AXwith 3-point lock system, single-doorDoor interior viewCentral hinge, only where H1 > 800 mmCentral embossed half-shear,only where B1/H1 ≥ 500 mmSection B – BSection A – AModel No.AXWidth dimensions mm Height dimensions mm Depth dimensions mm Mounting plates mm B1B2B3B6B10H1H2H3H5H6H10T1T2T3F1F2G1G2Type 1017.000800795756760675120011951156534.711601150300.4277.5280.4745700117511501EnclosureB1=Enclosure width (overall width)B2=Door widthB3=Clearance width, enclosure openingB6=Mounting distance, enclosuresB10=Distance between threaded boltsH1=Enclosure height (overall height)H2=Door heightH3=Clearance height, enclosure openingH5=Bottom edge of door to bottom edgeof lock plateH6=Mounting distance, enclosuresH10=Distance between threaded boltsT1=Overall depthT2=Enclosure depthT3=Installation depth (distance from insideof door to mounting plate)Mounting plateF1=Mounting plate widthF2=Centre-to-centre spacingof the attachment holesG1=Mounting plate heightG2=Centre-to-centre spacingof the attachment holesMounting plate type 1, with edge foldDetail Y Section C – CCompact enclosures AX, stainless steel Basic enclosure AXwith cam lock, double-doorwith 3-point locking system, double-doorSection B – BSection A – AWith 3-point lock system where H1 > 1000 mmWith cam lock where H1 ≤ 1000 mmMounting plate type 1, with edge foldDetail YSection C – CEnclosureB1=Enclosure width (overall width)B2=Door widthB3=Clearance width, enclosure openingB6=Mounting distance, enclosuresB10=Distance between threaded bolts,adjacent doorB11=Distance between threaded bolts,locked doorH1=Enclosure height (overall height)H2=Door heightH3=Clearance height, enclosure openingH5=Bottom edge of door to bottom edgeof lock plateH6=Mounting distance, enclosuresH10=Distance between threaded boltsT1=Overall depthT2=Enclosure depthT3=Installation depth (distance frominside of door to mounting plate)Mounting plateF1=Mounting plate widthF2=Centre-to-centre spacingof the attachment holesG1=Mounting plate heightG2=Centre-to-centre spacingof the attachment holesDoor interior viewCentral hinge, only where H1 > 800 mmCentral embossed half-shear,only where B1/H1 ≥ 500 mmModel No.AXWidth dimensions mm Height dimensions mm Depth dimensions mm Mounting plates mm B1B2B3B6B10B11H1H2H3H5H6H10T1T2T3F1F2G1G2Type 1018.00010004959569604253751000995956–960905300.4277.5280.49459009759501 1019.0001000495956960425375120011951156535.411601105300.4277.5280.4945900117511501 1305.0001000495956960425375120011951156535.411601105300.4277.5280.4945900117511501Compact enclosures AX Wall-mounted enclosures AX ITwith 482.6 mm (19") mounting angles, depth-variableSection A – ASection B – BDetail XModel No. AX IT Height dimensions mmDepth dimensions mmU H1H2H3H4H5H6T1T2T27641.3507380374336333255340350327.52787643.35012600594556553475560350327.52787645.35016760754716711635720350327.52787646.40016800794756711650760400377.5316For earth railDK 7113.000 For 482.6 mm (19") socket strip, 1 U DK 7240.XXX For 482.6 mm (19") socket strip, 2 UDK 7000.630Compact enclosuresCompact enclosures AX Command panel AXwith handle strips, service access from the frontModel No. AXWidth dimensions mm Height dimensions mmB B1B2B3H H1H2H3H5H6H7H86315.150345300294211301300294245––175161 6315.250425380374291301300294245––175161 6315.350425380374291381380374325––275261 6315.450545500494411501500494445300265375361 6315.650645600594511601600594545400365475461 Not applicable to AX 6315.150Section A – AEnclosureB=Overall width with handle stripsB1=Enclosure widthB2=Door widthB3=Maximum usable mounting space in the widthH=Overall height with handle stripsH1=Enclosure heightH2=Door heightH3=Maximum usable mounting space in the heightH5=Lock spacingH6=Clearance height between positioning bracketsH7=Mounting distance between mounting bracketsH8=Clearance height between mounting bracketsCompact enclosures Compact enclosures AXCommand panel AXwith handle strips, service access from the rearModel No. AXWidth dimensions mm Height dimensions mmB B1B2B3H H1H2H3H7H86320.050352.53002942442062001941507561 6320.350432.5380374324386380374330275261 6320.450552.5500494444506500494450375361 6320.550652.5600594544386380374330275261 6320.650652.5600594544606600594550475461Section A – AAX 6320.350, AX 6320.450, AX 6320.550, AX 6320.650AX 6320.050Section A – AEnclosureB=Overall width with handle stripsB1=Enclosure widthB2=Door widthB3=Maximum usable mounting space in the widthH=Overall height with handle stripsH1=Enclosure heightH2=Door heightH3=Maximum usable mounting space in the heightH7=Mounting distance between mounting bracketsH8=Clearance height between mounting bracketsCompact enclosuresCompact enclosures AXCommand panel AXfor desktop TFT up to 24"Monitor infinitely adjustable in the heightSection B – BSection A – AAX 6321.050 Monitor infinitely adjustable in the depthX W W 00195E N 1907◾Enclosures ◾Power Distribution ◾Climate Control ◾IT Infrastructure ◾Software & ServicesYou can find the contact details of allRittal companies throughout the world here./contact。

Thermo Scientific Accela LC Systems 产品说明书

Complete Chromatography SolutionsNo LimitsThermo Scientiﬁc Accela LC SystemsConventional HPLC and UHPLC applicationsUnsurpassed ultra high pressure quaternary capabilities Total temperature management Extremely low system delay volume Industry leading LC/MS solutionPart of Thermo Fisher Scientiﬁcc h r o m a t o g r a p h y™systems DetectorsThermo Scientiﬁc Accela PDA detector provides the highest sensitivity available with our proprietary Thermo Scientiﬁc LightPipe technology. The PDA collects and displays three simultaneous single wavelength channels concurrent with 3-D Spectral data for sample identiﬁcation and automated purity analysis. The Thermo Scientiﬁc Accela UV/Vis Detector combines the economy and reliability of variable wavelength detection with the sensitivity of LightPipe ™technology,with a variety of optional ﬂow cells. The easy-to-use Thermo Scientiﬁc Accela Refractive Index Detector is designedspeciﬁcally for the detection of compounds that have poor absorption in the UV range.The Thermo Scientiﬁc MSQ Plus mass detector complements data obtained with other Accela detectors for the rapid identiﬁcation and mass conﬁrmation of chromatographic peaks. Combine the Accela Systems with the wide range of Thermo Scientiﬁc Mass Spectrometers for a complete suite of LC/MS capabilities.SoftwareUse our Chromatography or Mass Spectrometry Data Systems such as Thermo Scientiﬁc ChromQuest or Xcalibur to fully control Accela for LC or LC/MS applications. These advanced data systems ensure complete control of Accela instrument operation, data acquisition, comprehensive data analysis and reporting. Whether Accela is used as a stand-alone LC or as part of a fully integrated LC/MS system, our comprehensive software solutions provide complete automation and data handling. Other multi vendor software solutions can be used for control and data acquisition when employing Accela as a stand-alone system.Accela System. Combined HPLC/ UHPLC operation to 1,250 bar with unmatched gradient accuracy and extremely low delay volume.From HPLC to UHPLC –HPLCHypersil GOLD 1.9 µm, 100×2.1 mm%B659595Peak width (s)1.081.161.211.241.261.301.30 Proprietary LightPipe technology provides up to 5x thedetection sensitivity of a conventional PDA detector.Accela PumpsThe world’s most accurate and precise HPLC and UHPLC pumps.Unique and innovative Force Feedback Control (FFC) technology enables the delivery of accurate and precise flow and gradients under all operating conditions by continuously adjusting valve timing and pumping efficiency based on the measured compressibility of the actual solvents providing the flexibility of a quaternary pump with unparalleled performance.•Accela 600 pump: ﬂow rate up to 5 mL/min and a maximumoperating pressure of 600 bar.•Accela 1250 pump: maximum ﬂow rate of 2 mL/min and amaximum operating pressure of 1,250 bar.Accela Pumps Advantages•Quaternary capability. Beneﬁt: ﬂexibility for methoddevelopment and multi-method operation, possibility to carry out complex separations employing ternary and quaternary gradients.•Extremely low delay volume. Beneﬁt: enables fast gradients,which translates into shorter run times and therefore higher throughput and faster method development.•Equipped with sensors for adjusting valve timing andpumping efﬁciency that are not in contact with the mobile phase. Beneﬁt: stable baselines, greatest ﬂow and gradient accuracy, no problems with sensor response variations over time due to contact with mobile phase.•Flow accuracy equal or better than ±0.5% for the entirepressure and ﬂow rate operating range of the pump.Beneﬁt: performance not compromised due to different run conditions; enhanced run-to-run reproducibility.•Gradient accuracy equal or better than ±0.5% for theentire pressure and ﬂow rate operating range of the pump.Beneﬁt: performance not compromised due to different ﬂow or pressure conditions; enhanced run-to-run reproducibility.•Pump pulsation lower than 0.5 bar without the need of apulse dampener. Beneﬁt: lowest pulsation over entire range for smooth baselines which translates intoenhanced detection.The Accela System routinely provides peak widths of one second and shorter (FWHH),which challenges the scan speeds and duty cycles of many mass spectrometers. Our industry-leading ion trap mass spectrometry technology provides maximum data for even the sharpest chromatographic peaks without compromising data quality.The Fastest LC Meets the Fastest Ion TrapAccelerating the capabilities of the world’s fastest ion traps with reduced run times and increased sensitivity.Optimize the efﬁciency of MS n identiﬁcation.LTQ Velos Dual-pressure Linear Ion Trap Novel dual-pressure trap technology in the LTQ Velos enables the identiﬁcation of more low-abundance compounds in less time.Accela is designed to optimize the efﬁciency of separation in the column regardless of column length. Whether short columns for targeted analysis, or long columns for complex mixtures, Accela easily handles the resulting backpressure, allowing you to work at optimal column ﬂow rates using a variety of column lengths. Coupling Accela to a linear ion trap mass spectrometer provides fast, accurate MS n data of the most complex metabolic compounds and products.•Accela maximizes metabolic application ﬂexibility byaccommodating the backpressures of many different column lengths •Industry leading MS/MS cycle speed provides more data in less time•Intelligent precursor ion selection withautomated Data Dependent MS n provides data on targeted and unpredicted analytesThermo Scientiﬁc LTQ VelosWith new S-Lens ion guide technology, a revolutionary dual-pressure linear ion trap, and predictive automatic gain control, the LTQ Velos ™is the fastest, most-sensitive ion trap available today. It enables the identiﬁcation and quantiﬁcation of low-abundance compounds in half the time, providing conﬁdence in every result.Thermo Scientiﬁc LTQ XLThe LTQ XL ™combines exceptional sensitivity with tremendous ﬂexibility.Multiple dissociation techniques as well as MALDI and ETD add-ons enable the generation of extensive structural information for challenging proteomics and metabolism applications.Thermo Scientiﬁc LCQ FleetThe LCQ Fleet ™ion trap makes excellent full-scan MS n sensitivity,ruggedness, and reliability cost effective. It delivers rich information for routine analysis of complex samples and integrates seamlessly with fast HPLC systems under an easy-to-use single point of control.The exceptional separation efficiency of Accela with Hypersil GOLD columns greatly enhances both speed and sensitivity of quantitation for high throughput analysis. 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Additionally, by separating the analyte from the matrix,charge competition in the API source is reduced, increasing ionization efficiency, resulting in increased sensitivity.High Speed Separations with Enhanced QuantitationAccela, coupled to Thermo Scientific quadrupole mass spectrometers, provides sensitivity, specificity, and speed in quantitation.The bottom chromatogram shows increased LC/MS sensitivity through chromatographicfocusing of the peak compared to theoriginal top chromatogram.Sample:Alprazolam 1.25 pgColumn:Hypersil GOLD, 5 µm, 100× 4.6 mm Mobile Phase:A: 0.1% Formic AcidB: Methanol with 0.1% Formic Acid Flow Rate:300 µL/minGradient:Time A% B% 0.0090.010.0 0.1590.010.0 1.15 5.095.0 2.15 5.095.0 2.2590.010.04.0090.010.0S ample:Alprazolam 1.25 pgColumn:Hypersil GOLD, 1.9 µm, 20× 2.1 mm Mobile Phase:A: 0.1% Formic AcidB: Methanol with 0.1% Formic Acid Flow Rate:1000 µL/min Gradient:Time A%B%0.0090.010.0 0.1590.010.0 1.15 5.095.0 1.35 5.095.0 1.3790.010.02.0090.010.0The Thermo Scientiﬁc TSQ Quantum Access MAXtriple stage quadrupole mass spectrometeranalyzes up to 300 SRMs per second, rapidly identifying and quantitating even the most complex mixtures.The Thermo Scientiﬁc TSQ Vantage triple stage quadrupole mass spectrometer delivers the highest sensitivity with the lowest chemical noise.The MSQ Plus ™single quadrupole mass detector has scan speeds up to 12,000 Da/sec,offering quick and clear mass identiﬁcation for even the fastest chromatographic peaks.High Resolution with Accurate MassHigh speed chromatography provides an additional degree of separationto the Thermo Scientiﬁc Orbitrap-based mass spectrometers with thebeneﬁt of sharp chromatography enhancing the dynamic range of eventhe most complex separations.Thermo Scientiﬁc Exactive –A new era inhigh-resolution benchtop mass spectrometryThe easy-to-use Exactive™LC/MS system deliversaccurate mass for every scan without the needfor data averaging. 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光催化降解有机污染物

Multi-layer three-dimensionally ordered Bismuth trioxide/Titanium dioxide nanocomposite:Synthesis and enhanced photocatalyticactivityLi Li a ,b ,c ,⇑,Xiandan Huang b ,a ,Jianqi Zhang b ,a ,Wenzhi Zhang b ,Fengyan Ma b ,Zhixin Xiao b ,Shuang Gai b ,Dandan Wang b ,Na Li baCollege of Materials Science and Engineering,Qiqihar University,Qiqihar 161006,PR China bCollege of Chemistry and Chemical Engineering,Qiqihar University,Qiqihar 161006,PR China cCollege of Heilongjiang Province Key Laboratory of Fine Chemicals,Qiqihar University,Qiqihar 161006,PR Chinaa r t i c l e i n f o Article history:Received 22September 2014Accepted 24November 2014Available online 5December 2014Keywords:Polystyrene EO 20PO 70EO 20Three-dimensionally ordered macroporous material Bi 2O 3/TiO 2Photocatalysis Crystal violeta b s t r a c tTaking polystyrene latex spheres (PS)and EO 20PO 70EO 20(P123)as dual templates,and TiO 2was used as substrate,a series of multi-layer three dimensionally ordered macroporous (3DOM)composites Bi 2O 3/TiO 2were successfully synthesized with sol–gel method and post-processing calcination.The fourier-transform infrared spectroscopy (FT-IR),X-ray diffraction (XRD),UV–vis diffuse reﬂectance (UV–vis/DRS),X-ray photoelectron spectroscopy (XPS),scanning electron microscopy (SEM),transmission electron microscopy (TEM),high resolution transmission electron microscopy (HR-TEM)and nitrogen adsorption–desorption measurements were employed to analyze the crystalline phase,chemical compo-sition,morphology,and surface physicochemical properties of as-synthetized samples.The results showed that as-composites were provided with obvious crystalline phase structure and periodically highly uniform ordered macroporous structure with mesoporous walls;moreover,of which was multi-layer three dimensionally ordered structure.As a result of unique optical properties of Bi 2O 3and compos-ite material structural characteristic being propitious to reactant molecular transmission and diffusion,the photocatalytic activities of 3DOM Bi 2O 3/TiO 2were enhanced,and the sample 3DOM Bi 2O 3/TiO 2-2was signiﬁcantly higher than that of direct photolysis,P25,Bi 2O 3,and other 3DOM Bi 2O 3/TiO 2-X (X =1,3,4)during the photocatalytic degradation of crystal violet under multi-modes such as UV,visible light,simulated solar light,and microwave-assisted irradiation.The centrifugal samples water solution phase of TOC analysis indicated that water solution products formed with continued ultraviolet radiation,the intermediates eventually mineralized,volatilized,or were converted to other products.In addition,the photocatalytic activity of 3DOM Bi 2O 3/TiO 2-2composite was basically kept even after three cycles.Meanwhile,the possible photocatalytic reaction mechanism of as-synthesized material based on the experimental results was proposed.Ó2014Elsevier Inc.All rights reserved.1.IntroductionIn recent years,the semiconductor photocatalyst technology shows potential application value owing to that is applied to envi-ronmental cleaning,solar energy conversion and H-energy produc-tion [1–5].Almost all difﬁcult to degrade organic pollutants have been ultimately completely mineralized into CO 2and H 2O under the action of semiconductor photocatalyst with light especially in the ﬁeld of degradation of organic pollutants.At present,the semi-conductor photocatalyst has been wide application such as anataseTiO 2and wurtzite ZnO.Although these kinds of semiconductor photocatalyst are cheap,non-toxic and high activity,they can only be excited under ultraviolet light,limiting their application at the same time [6–10].Thus,a variety of approaches have been explored to develop the visible light photocatalytic materials for the sake of absorbing maximum solar to photocatalytic degrada-tion,including phase/morphological control,ion doping,surface sensitization,noble metal loading,and heterostructure construct-ing.Among them,one of the most effective methods is that using narrow band gap semiconductor compounds with visible light cat-alyst material.Bi 2O 3is an important non-poisonous narrow band gap photosensitizer with a direct band gap of 2.1–2.8eV,and the high oxidation ability of electron holes of Bi 2O 3is regarded as an important condition for a kind of good photocatalytic materials./10.1016/j.jcis.2014.11.0620021-9797/Ó2014Elsevier Inc.All rights reserved.⇑Corresponding author at:College of Materials Science and Engineering,Qiqihar University,Qiqihar 161006,PR China.E-mail addresses:qqhrlili@ ,qqhrll@ (L.Li).However,too many opportunities for the recombination of photo-formed electrons and holes owing to the narrow band gap of Bi2O3 semiconductors and then application is limited[11–14].Accord-ingly,catalyst is prepared by the TiO2compounds with Bi2O3, exploiting the synergy to improve the utilization rate of catalyst for the light,so then to solve the aporia of Bi2O3electron holes eas-ily recombination have been deserves special attention[15,16].Furthermore,to further improve the photocatalytic activity by controlling morphological has been turned into the focus of studies in recent years,and more investigators have paid attention to the synthesis of three-dimensionally ordered macroporous(3DOM) structure[17–24].This is mainly that taking PS colloidal crystal template method to complete in the paper.3DOM materials are synthesized by the following steps:(i)a colloidal crystal template is synthesized by ordering monodisperse PS into a face-centered, close-packed array(opal structure),(ii)interspace of the colloidal crystal is thenﬁlled with the precursor of the destination product, either neat or in solution,that solidify in voids of the sphere tem-plates,and(iii)the orderly structure is produced after removing template by calcination method.The macropores are intercon-nected through windows that form as a result of contact between the template spheres prior to the inﬁltration of precursor solution [25].Due to the formation of three-dimensional macroporous materials caused by the precursor which is from transition process of liquid to solid,therefore,the level of order degree of the PS tem-plate and the physicochemical properties,dynamic viscosity,ﬂuid-ity and operating conditions of precursor play very important roles in the preparation of three dimensionally ordered macroporous material.In view of the above,our research group has developed a series of3DOM macroporous composite in several years.These3DOM composites mainly used the monodisperse PS sphere which was synthesized by emulsiﬁer-free emulsion polymerization technique as large-hole template.Although the large pore structure character-istics of composites are obvious,and the photocatalytic properties of composites have been improved,the holes on the distribution of the3DOM composites hole-wall are more general.In this study, a series of multi-layer3DOM Bi2O3/TiO2-X(X=1,2,3and4)com-posite materials with different Bi/Ti molar ratios have been synthe-sized using EO20PO70EO20(P123)as surface active agent via sol–gel method and post-processing calcination at the intrinsic experi-ment.The purposes of this experimental study are following:on the one hand,the P123is a kind of common triblock copolymer sur-face active agent with hydrophilic poly(ethylene oxide)and hydro-phobic poly(propylene oxide),which could be formed a containing soluble and insoluble core corona micelles and be able to dispersed precursor solution,and then the precursor solution soak into space of the PS template;on the other hand,under the effect of the tem-plate agents of PS spheres and P123,the structure of as-formed 3DOM would be more regular and compact,and the uniform mes-oporous wall is beneﬁcial to input and output of the reactant mol-ecules,so that the photocatalytic activities of the composite will be enhanced.In this study,the degradation effect of the as-synthesized 3DOM Bi2O3/TiO2-X composite on crystal violet(CV)selected as the model molecule has been investigated,under multiple modes including UV,visible light,microwave-assisted,and simulated solar light irradiation,respectively.The results revealed that the degra-dation effect of the3DOM Bi2O3/TiO2-2composite is higher than that of the other systematic photocatalysts.Moreover,the photo-catalytic performance of the3DOM Bi2O3/TiO2-2composite for var-ious organic pollutants and its catalytic cyclic process(recyclability of the photocatalyst)has been carried out under UV irradiation.In addition,based on the results of capture experiment,the possible photocatalytic reaction mechanism of3DOM Bi2O3/TiO2-X compos-ite has been speculated.2.Experimental2.1.MaterialsTitanium isopropoxide(TTIP,98%)and the triblock poly(ethyl-ene oxide)-block-poly(propylene oxide)-block-poly(ethylene oxide)copolymer(P123)(EO20PO70EO20,Mw=5800)were pur-chased from Energy Chemical Company.Styrene(St),potassium persulfate(K2S2O8),bismuth nitrate pentahydrate(Bi(NO3)3Á5H2O), Degussa P25,p-benzoquinone(BQ),tert-butyl alcohol(TBA),crys-tal violet(CV),methyl orange(MO),xylenol orange(XO),and sali-cylic acid(SA)were purchased from Guangfu testmart,China.All other reagents were analytical grade and used without further puriﬁcation.Water used in all experiments was deionized.2.2.Synthesis of polystyrene microsphere templateThe synthesis of monodisperse PS microsphere was performed by according to a slightly modiﬁed reported procedure[26,27]. Brieﬂy,during a typical experiment,phenylethylene(0.235mol), K2S2O8(0.33mmol),and deionized water(240mL)were taken into a clean three necked bottle equipped with a mechanical stirrer, thermometer with a temperature controller,bubbled with nitro-gen,stirred slowly and then placed in a water bath kept at70°C for7h and nitrogen was also imported continuously for7h, K2S2O8was as initiator.The resultant dispersion solution was sep-arated by centrifugation at1000rpm for24h,and then dried under room temperature.2.3.Synthesis of3DOM Bi2O3/TiO2-XThe sample3DOM Bi2O3/TiO2-X was prepared by sol–gel method using PS and P123as dual templates.In a typical synthesis, TTIP was dispersed in a mixture of ethanol and isopropanol (n ethanol:n isopropanol=4:1)containing P123(marked as solution A). After stirring for30min,Bismuth nitrate solution was added into solution A and then the as-obtained solution was marked as solu-tion B(n Bi(NO3)3Á5H2O:n TTIP=0.015:1;0.03:1;0.06:1and0.09:1). Subsequently,the mixed solution was inﬁltrated into the colloidal crystal template of PS and the sample was obtained byﬁltration. The obtained sample was dried at60°C and calcined in a mufﬂe furnace at600°C for7h(marked as3DOM Bi2O3/TiO2-X,X=1,2, 3,and4).2.4.Photocatalytic degradation of CVThe3DOM Bi2O3/TiO2-X composite materials’photocatalytic activities were evaluated by photocatalytic degradation of crystal violet dye under multi-modes including UV,visible light,micro-wave-assisted,and simulated solar light irradiation.A125W high pressure mercury lamp(k=313.2nm)was used as UV irradiation source.A400W xenon lamp(k P420nm)was used as visible source.The microwave discharge electrodeless lamp(MDEL,UV emission wavelength mainly located at280nm)had the power of15W which was taken as microwave-assisted irradiation light source and the output power of microwave reaction was600W.A photochemical reaction instrument equipped with a1000W xenon lamp(Shanghai bilon Instruments Co.,Ltd.;O3could be not produced during the photocatalytic reaction process.)was used for simulated solar light irradiation displaying strong consecutive spectra from UV to near IR region.CV was used as a model dye.Moreover,the reaction liquid volumes of four modes were90,220,90,and500mL,and the dos-age of the catalysts was0.15,0.30,0.15,and0.50g,respectively.14L.Li et al./Journal of Colloid and Interface Science443(2015)13–22Photocatalytic reaction device with a water jacket was used as the photoreactor except simulated solar light using circulating thermostated.The experiments were performed as follows:prior to irradia-tion,a certain amount of photocatalyst was suspended in90, 220,90,or500mL of CV(50mg LÀ1)solution by ultrasound ca. 10min,and then the suspensions were magnetically stirred for 30min in the dark to ensure the adsorption/desorption equilib-rium between CV and photocatalyst powders.The catalysts were removed by centrifugation after the completion of the reaction. First,the degradation was carried out under UV radiation as steps: the high pressure mercury lamp was placed into a jacketed quartz tube.The quartz tube was soaked into the solution which was con-tinuously magnetically stirred,and the suspensions were kept at constant temperature by circulating water through the jacket dur-ing the entire process.Second,the installation of the visible light degradation crystal violet was in accord with UV radiation except lamp source.Third,during the process of the simulated solar light irradiation,CV solution and photocatalyst were taken in a quartz photo-reactor.The reactor was placed8.5cm away from the light source.The suspensions were kept at room temperature by circu-lating thermostated ethanol through the jacket.Fourth,the micro-wave reactor employed for the degradation of CV was purchased from Yuhua Instrument limited company of China.It consists of a cylindrical glass reactor(capacity600mL)with a600mm long water reﬂux condenser,connected through a communication pipe. The MDEL was placed into the reaction solution and about2/3 parts of MDEL was dipped into reaction solution.Three silicone tubes were connected to the equipment,which could let water in and out and let air out through the hole on the microwave reactor. Air was bubbled into the solution through a sintered glassﬁlter,ﬁxed at the bottom of the reactor,not only for passing oxygen but also for mixing the catalyst and the solution.The suspension was maintained at room temperature by circulating solution through a cooler with peristaltic pump.At given time intervals, 3mL of suspension was sampled and centrifuged to remove the photocatalyst particles.Then,the absorption spectrum of the cen-trifugated solution was recorded using a TU-1901(China).The change of CV concentration was determined by monitoring the optical intensity of absorption spectra at590nm.To infer the photocatalytic oxidation pathways of3DOM Bi2O3/ TiO2-X,BQ(10mM)and TBA(10mM)were selected as scavenger agents for oxygen radical anionðOÀÅ2Þand hydroxyl radicals ( OH),respectively,for the photocatalytic degradation of CV over 3DOM Bi2O3/TiO2-2composite.The determination of concentra-tion of CV during the photocatalytic reaction in the presence of BQ or TBA was also determined by measuring the absorption of CV solution at590nm.2.5.CharacterizationThe phase and composition of the as-prepared samples were detected by Bruker-AXS(D8)X-ray diffractometer(XRD)studies using an X-ray diffractometer with Cu K a as X-ray radiation under 60kV and80mA and with the2h ranging from20°to80°.Fourier transform infrared(FT-IR)spectra were recorded by FT-IR spectro-photometer(PE Company,America).The morphologies and micro-structures of the as-prepared samples were investigated by scanning electron microscope(SEM)(Hitachi S-4300),transmission electron microscopy(TEM)(Hitachi H-7650)and high resolution transmission electron microscopy(acceleration voltage=200kV HR-TEM)(JEM-2100F).The samples were degassed at300°C over-night prior to the measurements,and the speciﬁc surface area was obtained by the Brunauer–Emmett–Teller(BET)method using a Quantachrome Nova Win II instrument.X-ray photoelectron spec-troscopy(XPS)was determined for an ESCALAB250Xi spectrometer equipping with Al K a radiation at300W.Binding energies(BE) were referenced to the C1s peak(284.6eV)of the surface adventi-tious carbon.UV–vis diffuse reﬂectance spectra(DRS)of the sam-ples were recorded with an UV–vis spectrophotometer(TU-1901) using BaSO4as reﬂectance standard.Total organic carbon(TOC)of the degraded CV solution under UV irradiation for10h was mens-urated by TOC analyzer(Germany TOC-liqui).3.Results and discussion3.1.FT-IR analysisFig.S1shows the FT-IR spectra of P123,PS,and3DOM Bi2O3/ TiO2-2composite.Fig.S1(b)shows the FT-IR spectrum of P123, the characteristic peaks of P123,which are consistent with the lit-erature reports[28,29].As shown in Fig.S1(a),the characteristic peaks of PS spheres in FT-IR spectra have authenticated that the styrene reacts to produce PS by polymerization,all of the speciﬁc peaks due to polystyrene locating around1594,1485,750, and693cmÀ1can be observed from the spectra.The peaks at 2922–3022cmÀ1are attributed to C–H groups,which belong to PS[30–32].The characteristic peaks of PS spheres and P123are not appeared in the FT-IR spectra of3DOM Bi2O3/TiO2-2 (Fig.S1(c)),indicating the templates are able to be removed by calcining.3.2.XRD analysisFor the sake of researching the crystalline structure of as-synthesized composite materials,Bi2O3,TiO2,and3DOM Bi2O3/TiO2-X samples with different Bi/Ti molar ratios were mea-sured by XRD analysis,the results as shown in Fig.1.All the char-acteristic diffraction peaks of3DOM Bi2O3/TiO2-X composite are mainly consistent with the anatase crystalline phase of TiO2(JCPDS 21-1272),indicating the3DOM Bi2O3/TiO2-X samples are based on TiO2anatase phase structure.However,there is one faintish diffraction peak of Bi2O3(JCPDS73-1126)situated at27.63°in the diffraction patterns of3DOM Bi2O3/TiO2-X,which is attributed to the low-content of Bi2O3,and indicating the interaction between Bi2O3and TiO2[33,34].The change trend of crystal grain size (Table1)about3DOM Bi2O3/TiO2-X is decreasedﬁrstly and then increased,of which3DOM Bi2O3/TiO2-2has relatively small crys-tallite size,which will exhibit higher photocatalytic activities [35–37].Furthermore,the diffraction peak of3DOM Bi2O3/TiO2-X at25.31°is signiﬁcantly broader than that of2h values of TiO2,L.Li et al./Journal of Colloid and Interface Science443(2015)13–2215suggesting that the crystal grain size of composite is signiﬁcantly smaller after Bi2O3compounded with TiO2,attributed to the growth of TiO2crystal inhibited by Bi[33].Meanwhile,it is obvious that the crystallization degree of3DOM Bi2O3/TiO2-X is decreased slightly with the increase of Bi/Ti molar ratio on account of the presence of Bi2O3disturbed the crystallization process during cal-cination[38].3.3.UV–vis/DRS analysisThe optical properties of the pure Bi2O3,TiO2,and3DOM Bi2O3/ TiO2-X with different Bi/Ti mole ratio values are revealed by the UV–vis diffuse reﬂectance spectra(UV–vis/DRS),as shown in Fig.2.According to Fig.2(a),there are no obvious absorption peaks of Bi2O3and TiO2remained in the3DOM Bi2O3/TiO2-X,and there is only one absorption band edge,which is attributed to the poor content of pared to TiO2,3DOM Bi2O3/TiO2-X samples are red-shifted to the visible region and at least red-shift50,60,85, and95nm with the increase of Bi content,respectively.To determine the nature of transition and to obtain the band gap of the sample material,following equation was used[39,40]: (a h m)n=K(h mÀE g),where a is the absorption coefﬁcient,K is the parameter that related to the effective masses associated with the valence and conduction bands,n is1/2for a direct transition, h m is the absorption energy,and E g is the band gap energy.Plotting (a h m)n versus h m based on the spectral response in Fig.2(b)give the extrapolated intercept corresponding to E g value(see Fig.2(b)).As shown in Fig.2(b),the band-gap energy of the sample decreased with the increase of the content of Bi.Band-gap energies of differ-ent3DOM Bi2O3/TiO2-X samples are similar to the pure Bi2O3,indi-cating that spectral sensitivity of3DOM Bi2O3/TiO2-X in the visible region is mainly caused by paring with TiO2,band-gap energies of3DOM Bi2O3/TiO2-X are signiﬁcantly smaller,which means that the composite3DOM Bi2O3/TiO2-X can absorb lower energy of photons,and to promote generate efﬁcient of photos in the whole system and the more photogenerated elec-tron hole pairs are involved in the photocatalytic reaction.Thus the photocatalytic activities of the samples will be improved.But owing to the band gap energy of composite products reduced with the increase of Bi content,so the recombination speed of photo-generated electrons and holes increased,and then the probability of photon will be reduced,resulting in the photocatalytic activity was not well as we had expected.3.4.XPS analysisTo further explore the chemical states of various elements in these samples,the3DOM Bi2O3/TiO2-X composites were character-ized by XPS analysis.Fig.3(a)presents four elements containing C, Bi,Ti,and O on the surface of3DOM Bi2O3/TiO2-2.The carbon ele-ment of sample surface is owing to organic impurities removed incompletely and the hydrocarbons related to the instrument itself [41].As shown in Fig.3(b)–(d),which are the XPS photoelectron spectra of different Bi/Ti molar ratio samples’various chemical elements.Fig.3(b)presents the Bi4f XPS spectra of the3DOM Bi2O3/TiO2-X,which could be observed that two peaks for the Bi4f of the3DOM Bi2O3/TiO2-X are located at the binding energies of 159.6and164.8eV[42,43],pertaining to Bi4f7/2and Bi4f5/2 respectively.Moreover,there is with a spin–orbit splitting of 5.3eV belonged to the characteristic of Bi3+[44].As shown in Fig.3(c),XPS of Ti(2p)has two peaks with binding energies of 459.1and464.9eV[45,46]attributed to Ti2p3/2and Ti2p1/2,indi-cating that Ti is presented in the+4valence state.The binding energies of O1s are530.4and532.5eV[47,48],corresponding toTable1Crystallite size,band-gap energy,BET surface areas,pore volumes,average pore diameters,pore diameter,pore shrinkage,andﬁrst-order rate constant of3DOM Bi2O3/TiO2-X.Sample3DOMBi2O3/TiO2-13DOMBi2O3/TiO2-23DOM Bi2O3/TiO2-33DOMBi2O3/TiO2-4D⁄(nm)14.410.011.716.0E g(eV) 2.76 2.73 2.58 2.53S BET(m2gÀ1)49.392.047.831.0V total(cm3gÀ1)0.2130.2310.2160.020D(nm) 3.27 3.60 2.99 3.36d(nm)106110120117d contraction(%)47454041.5k(minÀ1)0.029910.056880.023600.00394D⁄average crystallite sizes of samples were calculated from Scherrer equation.D represents the average pore diameter.16L.Li et al./Journal of Colloid and Interface Science443(2015)13–22emission from lattice oxygen and hydroxyls,respectively.These results demonstrated that the Bi2O3is mainly presented as a sepa-rate phase in the3DOM Bi2O3/TiO2-X,and the Bi species are not incorporated into the TiO2lattice.This could be attributed to the size of Bi3+ionic radius(103pm)is bigger than that of the Ti4+ionic radius(61pm),which inhibits the replacement of Ti by Bi in the TiO2crystal lattice[49,50].3.5.N2adsorption–desorption analysisTo evaluate surface physicochemical properties of as-synthe-sized composite materials,N2adsorption–desorption measure-ments were taken,as shown in Fig.4.According to the IUPAC nomenclature,the composite materials revealed the type IV pattern curve,representing the existence of the mesoporous-structure,which came from the particles accumulation of the hole-wall of3DOM Bi2O3/TiO2-X composite and the action of mes-oporous template P123[51].All of the hysteresis loops of3DOM Bi2O3/TiO2-X are H3type shape ascribed to the particle aggregation of3DOM Bi2O3/TiO2-X composite.The BET surface areas of the composites have been listed in Table1(the pore size distributions of3DOM Bi2O3/TiO2-X are shown in Fig.S2).Among the BET value, one of the3DOM Bi2O3/TiO2-2composites is obviously higher than that of other samples,and the nitrogen adsorption isotherm of 3DOM Bi2O3/TiO2-2composite also obviously has shifted upward [52,53],which indicating that the photocatalytic activity of the composite material will be improved.The difference for larger sur-face area of composites may be attributed to the concentration of precursors.The concentration is too high or low to be propitious to the formation of multi-layer three dimensionally ordered hole.3.6.SEM analysisFig.5shows the SEM images of PS spheres and3DOM Bi2O3/ TiO2-X composite.Fig.5(a)–(c)exhibits the SEM images of PS spheres with different scaleplate indicating the uniform size of the as-synthetized PS spheres with monodisperse and close-packed structure having an average diameter ca.200nm.The spheres of PS are accumulated from layer to layer,extruded recip-rocally and packed closely leading to macropore template of PS spheres with the hexagonal multilayer structured(Fig.5(a))attrib-uted to the self-assembly process.However,to compare with the PS spheres which were closely reciprocally extruded,the PS spheres without reciprocal extruding appear the original orbicular structure with tightly packed regular layers(Fig.5(a)).L.Li et al./Journal of Colloid and Interface Science443(2015)13–2217Fig.5(d)–(o)shows the SEM images of3DOM Bi2O3/TiO2-X com-posite under different scaleplate indicating that multi-layer3D macroporous structure of obtained is regular,and the pore is inter-connected by uniform windows.The pore-size of3DOM Bi2O3/ TiO2-X is listed in Table1with‘‘d’’.Compared with Fig.5(a)–(c), during the preparation of the3DOM Bi2O3/TiO2-X material by the colloidal crystal template method,the resulting pore diameters are obviously smaller than that of original PS spheres.The melting of PS sphere templates and the sintering of the metal oxide can result in the shrinkage of pore diameter during calcination,and the rate of shrinkage of pore diameter is also listed in Table1with ‘‘d contraction’’.Fig.5(d)–(o)shows the iconograph of the as-prepared 3DOM Bi2O3/TiO2-X composite obviously displayed there are three small holes symmetrically distributed in the bottom of each hole, and on the channel of each big hole is highly ordered hexagonal structure with reciprocally connecting to circumambient six large holes,which belonged to the3D ordered holes array structure.In addition,it is not difﬁcult toﬁnd as-prepared samples showing multilayer structure,which is attributed to PS spheres closely accumulated layer by layer in self-assembly process have been removed from by calcination.Although the structure of as-synthe-tized3DOM Bi2O3/TiO2-X is orderly regular arrangement with fewer defects,the partial faultage and the ruptured hole-wall are existed,which are mainly due to(1)the precursor complexes are heated unevenly,(2)and then the heating rate of system is relatively faster,volumes of gas escaped collectively during the cal-cination process of which was produced by heating PS and P123. The hole-windows of multi-layer3DOM Bi2O3/TiO2-X composite are hole-channel with adjacent big holes,and the forma-tion of hole-window is attributed to the reciprocal junction of PS template which is every last microsphere closed to three underly-ing microspheres,directly effecting the diffusion of substances in the big holes.Moreover,it is observed that NPs collectively constituted the hole-wall of the as-prepared multi-layer3DOM SEM images of PS(a–c),3DOM Bi2O3/TiO2-1(d–f),3DOM Bi2O3/TiO2-2(g–i),3DOM Bi2O3/TiO2-3(j–l),and3DOM Bi2O3/TiO2Bi 2O 3/TiO 2-X composite,and the accumulation of NPs with unﬁxed gap leads to the holes wall pertaining to mesoporous structure.Although the structure of as-synthetized multi-layer 3DOM Bi 2O 3/TiO 2-X is closely arranged regularly,the structure of three-dimensional ordered and hole-shrinkage could be affected (see Table 1)with the increase of Bi/Ti molar ratio.When Bi content is lower,the structure of as-synthetized 3DOM Bi 2O 3/TiO 2-1is not only regular ordered but also transparent as shown in Fig.5(d)–(f),and the multi-layer structure is relative obvious.The pore-wall is made up of uniform nanoparticles,and then the pore-wall is thinner.However,as-synthesized 3DOM Bi 2O 3/TiO 2-4sample still forms three ordered holes array structure,but the partial structure of 3DOM Bi 2O 3/TiO 2-4ranks loosely and nonuni-form (Fig.5(m)–(o))when the Bi content is higher.At the same time,the sample permeability becomes poorer,which will be inﬂu-enced the input and output of reactant molecules in a certain extent.In order to obtain more skeleton information of 3DOM Bi 2O 3/TiO 2-X composite,the as-synthetized 3DOM Bi 2O 3/TiO 2-2was analyzed by TEM and HR-TEM (Figs.S3and S4).Based on the above analysis,the structure and pore size of as-synthetized 3DOM Bi 2O 3/TiO 2-X samples are inﬂuenced by Bi/Ti mole ratio.The distinctive dual pore structure of 3DOM Bi 2O 3/TiO 2-X composite is more conducive to the photocatalytic reaction.3.7.Photocatalytic activityIn order to investigate the photocatalytic performance of thebeen carried out.As shown in Figs.6(a)and in S6(a),the fastest rate of degradation of CV with different photocatalysts under UV mode is 3DOM Bi 2O 3/TiO 2-2composite (Bi/Ti =0.03:1).Fig.6(b)shows that the apparent ﬁrst-order rate constant k for 3DOM Bi 2O 3/TiO 2-2is relatively high compared to other photocatalysts (Table 1).In the course of visible light photocatalytic degradation of CV,the visible light activity of 3DOM composite material are higher,especially,the degradation efﬁciency of CV is the best when Bi/Ti =0.03:1,and which has been reached to 67.16%after 5h (Fig.6(c-1)).Fig.6(c-2)exhibits that the photocatalytic activity of 3DOM Bi 2O 3/TiO 2-2is signiﬁcantly higher than that of the other photocatalysts under microwave-assisted irradiation.According to Fig.6(c-3),the photocatalytic activities of the catalysts for the degradation of CV under the simulated solar light mode follow the order:3DOM Bi 2O 3/TiO 2-2>3DOM Bi 2O 3/TiO 2-1>3DOM Bi 2O 3/TiO 2-3>3DOM Bi 2O 3/TiO 2-4>Bi 2O 3>P25>direct photoly-sis after 300min.As shown in Fig.S6(b),with increasing reaction time,the absorbance located at maximum wavelength of 3DOM Bi 2O 3/TiO 2-2degradation of CV is reduced under the UV condition,and which are overall regularly changed.As shown in Fig.S6(c),the degradation ability for different structure dyes (CV,XO,MO and AR)of 3DOM Bi 2O 3/TiO 2-2are obvious.The little difference in the rate of photocatalytic degradation is due to the structure and complexity of the organic contaminants.Furthermore,to investi-gate the stable activity of 3DOM Bi 2O 3/TiO 2-2,the cyclic experi-ments were performed as shown in Fig.S6(d).After three runs for the photocatalytic degradation of CV at the reaction conditions,the activity of 3DOM Bi 2O 3/TiO 2-2composite shows relatively L.Li et al./Journal of Colloid and Interface Science 443(2015)13–2219。

Thermo Scientific Dionex IonPac AS14 产品说明书

Product SpecificationsThermo Scientific Dionex IonPac AS14Anion-Exchange ColumnThe Thermo Scientific ™ Dionex ™ IonPac ™ AS14 anion-exchange column is designed for the fast analysis of inorganic anions, including fluoride, acetate, chloride, nitrite, bromide, nitrate,phosphate, and sulfate. The Dionex IonPac AS14 column is suited for applications performed using the Dionex IonPac AS4A-SC and Dionex IonPac AS12A columns with the advantages of improved peak resolution and retention of fluoride. Solvent compatibility permits easy column clean-up after the analysis of complex matrices. The Dionex IonPac AS14A column can also be used for the fast, isocratic separation of the common inorganic anions. Refer to the Dionex IonPac AS14A column Product Specifications for more information.C H R O M A T O G R A P H YDetermination of Inorganic Anions in Diverse Sample Matrices• Source water and drinking water • Municipal and industrial wastewater • Industrial cooling water • Power plant waters• Hazardous waste extracts and dump site leachates • Acid rain• I norganic anions in foods and beverages • Anionic counterions in pharmaceutical preparations and synthetic peptides • Polymers such as polyols and polysulfonates • Kraft liquorsSuperior Chromatographic Performance• Universal column for inorganic anions. Designed to be used in Dionex IonPac AS4A, Dionex IonPac AS4A-SC, and Dionex IonPac AS12A column applications with equivalent linearity and precision.• Fast isocratic separation of fluoride, chloride, nitrite, bromide, nitrate, phosphate, and sulfate using a simple carbonate/bicarbo- nate eluent. Retains fluoride out of the water dip, free of interference from organic acids, with elution of sulfate in 13 min.• M eets or exceeds requirements of U.S. EPA Method 300.0 (A).• Superior retention and quantification of fluoride, glycolate, acetate, and formate.• Sodium tetraborate gradient optimizes difficult separations.• Solvent compatible. Solvent samples for determining contaminating anions. Use organic solvents to enhance analytesolubility, modify column selectivity, or for effective column clean-up.• Available in 4 mm or 2 mm formats. Use the 2 mm microbore column for economical operation.MinutesIsocratic Separation of Inorganic Anions onan Dionex IonPac AS14 Column in Less than 13 Minutes2High Efficiency Particle StructureThe Dionex IonPac AS14 column packing is a unique structure composed of a highlycrosslinked core and an anion-exchange layer grafted to the surface, as shown in Figure 1. The substrate for the Dionex IonPac AS14 column is a 9 μm diameter macroporous resin bead consisting of ethylvinylbenzene crosslinked with 55% divinylbenzene. The anion-exchange layer is functionalized with quaternary ammonium groups. The anion- exchange layer has a controlled thickness resulting in excellent mass transfercharacteristics and consequently very high efficiency peaks.Unique Selectivity and Increased CapacityThe Dionex IonPac AS14 column has a unique selectivity and increased capacity compared to the Dionex IonPac AS4A column. As shown in Figure 2, fluoride is well resolved from the system void and free from interference from acetate and formate. These features make the Dionex IonPac AS14 column ideal for routine inorganic anion determinations. The increased capacity of the Dionex IonPac AS14 column allows the injection of complex matrices or injection of up to 100 μL of sample, as shown in Figure 3.Figure 1. Structure of an Dionex IonPac AS14 column packing particle.Figure 2. Isocratic separation of inorganic anions on an Dionex IonPac AS14 column in less than 13 minutes.Figure 3. Determination of trace level anions in high-purity water using the Dionex IonPac AS14 column with a large loop injection.Column: Dionex IonPac AG14,Dionex IonPac AS14, 4 mm Eluent: 3.5 mM Sodium carbonate1.0 mM Sodium bicarbonate Flow Rate: 1.2 mL/min Inj. Volume: 10 µLDetection: Suppressed conductivity, Thermo Scientific ™ Dionex ™ ASRS ™-ULTRA AnionSelf-Regenerating suppressor, 4 mm, AutoSuppress ion ™, recycle mode Peaks: 1. Fluoride 5 mg/L (ppm) 2. Acetate 20 3. Chloride 10 4. Nitrite 15 5. Bromide 25 6. Nitrate 25 7. Phosphate 408. Sulfate3010µS0MinutesColumn: Dionex IonPac AG14,Dionex IonPac AS14, 4 mm Eluent: 3.5 mM Sodium carbonate1.0 mM Sodium bicarbonate Flow Rate: 1.2 mL/min Inj. Volume: 100 µLDetection: Suppressed conductivity,Dionex ASRS-ULTRA suppressor, 4 mm, Auto Suppression, external water mode Peaks: 1. Fluoride 50 µg/L (ppb) 2. Chloride 70 3. Nitrite 120 4. Bromide 250 5. Nitrate 250 6. Phosphate 8007. Sulfate25000.5µS246Minutes810123467512143Column: A: Dionex IonPac AG4A-SC,Dionex IonPac AS4A-SC, 4 mm B: Dionex IonPac AG14, Dionex IonPac AS14, 4 mm Eluent: A: 1.8 mM Sodium carbonate 1.7 mM Sodium bicarbonate B: 4.8 mM Sodium carbonate 0.6 mM Sodium bicarbonate Flow Rate: A: 2 mL/min B: 1.5 mL/min Inj. Volume: 10 µL Detection: Suppressed conductivity, Dionex ASRS-ULTRA suppressor, 4 mm, AutoSuppression, recycle mode Peaks: 1. Fluoride 5 mg/L (ppm) 2. Chloride 10 3. Nitrite 15 4. Bromide 25 5. Nitrate 25 6. Phosphate 407. Sulfate3010µS 014µS111222333Minutes444555666777A Dionex IonPac AS4A-SC columnB Dionex IonPac AS14 column89Column: Dionex IonPac AG14, Dionex IonPac AS14, 4 mm Eluent: 3.5 mM Sodium carbonate 1.0 mM Sodium bicarbonate Flow Rate: 1.2 mL/min Inj. Volume: 10 µL Detection: Suppressed conductivity, Dionex ASRS-ULTRA, suppressor, 4 mm, AutoSuppression, recycle mode Sample: Drinking water from Milpitas, CA Peaks: 1. Fluoride0.03 mg/L (ppm) 2. Bicarbonate 30 3. Chloride 3.1 4. Nitrate 0.15 5. Phosphate 0.046. Sulfate 4.413420.5µS0246Minutes810121456Ideal for the Determination ofInorganic Anions in Drinking Water and WastewaterThe Dionex IonPac AS14 column is the ideal column for compliance monitoring of drinking water and waste water. The Dionex IonPac AS14 column meets or exceeds therequirements of U.S. EPA Method 300.0 (A). As shown in Figure 4, fluoride is easily separated from the system void and can be determined even at very low concentrations. The Dionex IonPac AS14 column has significantly improved retention of fluoride compared to the Dionex IonPac AS4A column, as illustrated in Figure 5.Figure 4. The Dionex IonPac AS14 column is ideal for interference-free determinationof inorganic anions, including fluoride, in drinking water.Figure 5. Fast isocratic elution of inorganic anions. The increased capacity and unique selectivity of the Dionex IonPac AS14 column allows the retention of fluoride out of the water dip while eluting sulfate in less than 9 minutes.4Column: Dionex IonPac AG14,Dionex IonPac AS14, 4 mm Eluent: 3.5 mM Sodium carbonate0.8 mM Sodium bicarbonate Flow Rate: 1.2 mL/min Inj. Volume: 10 µLDetection: Suppressed conductivity,Dionex ASRS-ULTRA suppressor, 4 mm, AutoSuppression, recycle modePeaks: 1. Chloride0.3 mg/L (ppm) 2. Sulfate 0.93. Trifluoroacetic acid 6.505123101520Minutes0.4µSColumn: Dionex IonPac AG14,Dionex IonPac AS14, 4 mmEluent: 2 mM Sodium tetraborate for 6 min; 10 min gradient to17.5 mM Sodium tetraborate Flow Rate: 1.5 mL/min Inj. Volume: 25 µLDetection: Suppressed conductivity,Dionex ASRS-ULTRA suppressor, 4 mm, AutoSuppression, external water mode Peaks: 1. Fluoride 5 mg/L (ppm) 2. Glycolate 10 3. Acetate 20 4. Formate 10 5. Chloride 3 6. Nitrite 10 7. Bromide 10 8. Nitrate 10 9. Phosphate 1510. Sulfate1512µS022345678910146Minutes81012141618Determination of InorganicAcids and Low Molecular Weight Organic AcidsLow molecular weight organic acids and mono- and divalent inorganic anionscommonly encountered in the chemical and power industries can be determined in a single run. Figure 6 illustrates the separation of weakly retained anions such as fluoride, glycolate, acetate, and formate on the Dionex IonPac AS14 column by using a sodium tetraborate gradient.The Dionex IonPac AS14 column can be used to evaluate the mass balance of drugs and synthetic peptide preparations. Figure 7 illustrates the use of the Dionex IonPac AS14 column to determine the anionic counterion amount and type.Solvent Compatible PackingSince the Dionex IonPac AS14 column is 100% HPLC solvent compatible, organic solvents can be used for efficient column clean-up or to enhance sample solubility. Users save time and money by eliminating time consuming sample preparation steps. This feature allows complex matrices to be analyzed with minimal sample preparation and extends the utility of the column to new applications requiring solvents. Adding organic solvents to the eluent modifies columnselectivity and enables the elution of nonpolar analytes or contaminants from the column.Economical Microbore OperationThe Dionex IonPac AS14 column is available in the 2 mm format to provide the advantages of reduced operating costs with microbore operation.• Higher mass sensitivity compared to 4 mm separations. Ideal for limited sample volumes.• Reduced mobile phase consumption (3–4 times).• 4 mm applications can be directly transferred to the 2 mm format.Figure 6. Sodium tetraborate gradient separation of anions using the Dionex IonPac AS14 column.Figure 7. Determination of anionic counterions present in a gel permeation purified peptide.SPECIFICATIONSDimensions Analytical 2 × 250 mm and 4 × 250 mm Guard2 × 50 mm and 4 × 50 mm Maximum Operating Pressure 27.6 MPa (4000 psi)Mobile Phase Compatibility pH 2–12; 0–100% HPLC solventsSubstrate Characteristics Bead Diameter (µm) 9Pore Size Å 100Cross-Linking (%DVB)55Ion-Exchange Functional Group Surface-functionalized alkyl quaternary ammonium ion Functional Group Characteristics Medium-high hydrophobicCapacity 16 µeq (2 × 250 mm column)65 µeq(4 × 250 mm column)Column Construction PEEK with 10–32 threaded ferrule-style end fittings.All components are nonmetallic.Ordering InformationFor more information or to place an order, contact the Thermo Scientific Dionex Products office nearest you or your local distributor. Phone numbers and addresses for worldwide subsidiaries can be found in the About Us section of .For optimum ease-of-use and economy, the Dionex IonPac AS14 column should be used with the Thermo Scientific ™ Dionex ™ AERS 500 suppressor. The Dionex IonPac AS14 column offers improved performance for Dionex IonPac AS4A, Dionex IonPac AS4A-SC, and Dionex IonPac AS12A column applications.When performing sodium tetraborate gradient anion-exchange applications on the Dionex IonPac AS14 column, a Dionex IonPac ATC column should be installed between the gradient pump and the injection valve to remove anionic contaminants from the eluent.For concentrator work, use the Dionex IonPac AG14 guard column; Ultratrace Anion Concentrator Columns (Dionex IonPac UTAC-ULP1, UTAC-XLP1, UTAC-ULP2, or UTAC-XLP2 columns) or Trace Anion Concentrator Column (Dionex IonPac TAC-ULP1 column) when a single piston pump such as the Thermo Scientific Dionex AXP Auxiliary Pump (pulse damper required) is used for sample delivery. In addition to the concentrator columns listed above, use the Dionex IonPac UTAC-LP1, Dionex IonPac UTAC-LP2, or Dionex IonPac TAC-LP1 column when the sample is delivered using a syringe or alow-pressure autosampler, such as the Thermo Scientific Dionex AS-DV Autosampler.PS71397-EN 1014MAfrica +43 1 333 50 34 0Australia +61 3 9757 4300Austria +43 810 282 206Belgium +32 53 73 42 41Brazil +55 11 3731 5140Canada +1 800 530 8447China 800 810 5118 (free call domestic)400 650 5118Denmark +45 70 23 62 60Europe-Other +43 1 333 50 34 0Finland +358 9 3291 0200France +33 1 60 92 48 00Germany +49 6103 408 1014India +91 22 6742 9494Italy +39 02 950 591 Japan +81 6 6885 1213Korea +82 2 3420 8600Latin America +1 561 688 8700Middle East +43 1 333 50 34 0Netherlands +31 76 579 55 55 New Zealand +64 9 980 6700 Norway +46 8 556 468 00Russia/CIS +43 1 333 50 34 0Singapore +65 6289 1190Sweden +46 8 556 468 00 Switzerland +41 61 716 77 00Taiwan +886 2 8751 6655UK/Ireland +44 1442 233555USA +1 800 532 4752/chromatography©2014 Thermo Fisher Scientific Inc. All rights reserved. ISO is a trademark of the International Standards Organization.All other trademarks are the property of Thermo Fisher Scientific and its subsidiaries. Specifications, terms and pricing are subject to change. Not all products are available in all countries. Please consult your local sales representative for details.Thermo Fisher Scientific, Sunnyvale, CA USA is ISO 9001:2008 Certified.Dionex IonPac AS14 ColumnsPart NumberDionex IonPac AS14 Analytical Column (4 × 250 mm) 046124Dionex IonPac AG14 Guard Column (4 × 50 mm) 046134Dionex IonPac AS14 Analytical Column (2 × 250 mm) 046129Dionex IonPac AG14 Guard Column (2 × 50 mm) 046138Trace Anion Concentrator ColumnsPart NumberDionex IonPac TAC-2 Trace Anion Concentrator (3 × 35 mm) 043101Dionex IonPac TAC-LP1 Trace Anion Concentrator (4 × 35 mm)046026Dionex IonSwift MAC-100 Monolith Anion Concentrator (0.5 × 80 mm) (for use with Capillary IC) 074702Dionex IonPac TAC-LP1 Trace Anion Concentrator (4 × 35 mm) 046026Dionex IonPac TAC-ULP1 Trace Anion Concentrator (5 × 23 mm)061400Dionex IonPac UTAC-LP1 Ultra Trace Anion Concentrator Low-Pressure (4 × 35 mm) 063079Dionex IonPac UTAC-ULP1 Ultra Trace Anion Concentrator Ultra Low-Pressure (5 × 23 mm) 063475Dionex IonPac UTAC-XLP1 Ultra Trace Anion Concentrator Extremely Low-Pressure (6 × 16 mm) 063459Dionex IonPac UTAC-LP2 Ultra Trace Anion Concentrator Low-Pressure (4 × 35 mm) 079917Dionex IonPac UTAC-ULP2 Ultra Trace Anion Concentrator Ultra Low-Pressure (5 × 23 mm) 079918Dionex IonPac UTAC-XLP2 Ultra Trace Anion Concentrator Extremely Low-Pressure (6 × 16 mm) 072781Anion Trap ColumnsPart NumberDionex IonPac ATC-3 Anion Trap Column (9 × 24 mm) (for use with 4 mm columns) 059660Dionex IonPac ATC-3 Anion Trap Column (4 × 35 mm) (for use with 2 mm columns)079932Product Specifications。

BCYE Agar Base 产品说明书

BCYE AGAR BASE (7728)Intended UseBCYE Agar Base is used for the isolation of Legionella spp.Product Summary and ExplanationIn 1977, McDade et al. identified Legionella pneumophila as the causative agent of Legionnaires’ disease, a multisystem disease manifested primarily by pneumonia.1,2In 1978 a new medium, F-G Agar, resulted in improved growth of L. pneumophila, a very fastidious organism.3 Freely et al. modified F-C Agar by substituting yeast extract as a vitamin source and replacing starch with activated charcoal, producing Charcoal Yeast Extract (CYE) Agar.4 In 1980, Pasculle et al. reported that CYE Agar could be improved by the addition of ACES (N-2-acetamido-2-aminoethane sulfonic acid) buffer.5 One year later, Edelstein further increased the sensitivity of the medium by adding the potassium salt of alpha-ketoglutaric acid.6Principles of the ProcedureYeast Extract provides sources of nitrogen, carbon, and vitamins in BCYE Agar Base. Activated Charcoal decomposes hydrogen peroxide, a metabolic product toxic to Legionella spp., and may also collect carbon dioxide and modify surface tension. ACES Buffer is added to maintain the proper pH for optimal growth. α-Ketoglutarate stimulates organism growth. Ferric Pyrophosphate supplies iron. Agar is the solidifying agent. BCYE Agar is supplemented with L-Cysteine, an essential amino acid incorporated to satisfy specific nutritional requirements of Legionella spp. Selective agents can be added if necessary.Formula / Liter Supplements / 10 mLYeast Extract ........................................................................... 10 g L-Cysteine (4%), sterileACES Buffer ............................................................................ 10 gCharcoal, Activated ................................................................ 1.5 gα-Ketoglutarate .......................................................................... 1 gFerric Pyrophosphate ........................................................... 0.25 gAgar ......................................................................................... 15 gFinal pH: 6.9 ± 0.2 at 25︒CFormula may be adjusted and/or supplemented as required to meet performance specifications.Precaution1. For Laboratory Use.2. IRRITANT. Irritating to eyes, respiratory system, and skin.Directions1. Suspend 38 g of the medium in 900 mL of purified water.2. Adjust pH to 6.9 with 1N KOH.3. Add water to bring volume to 1000 mL.4. Heat to boiling with stirring to dissolve.5. Autoclave at 121︒C for 15 minutes. Cool to 45 - 50︒C.6. Aseptically add 10 mL of a sterile solution of L-Cysteine (4%).7. Mix and add inhibitor solutions if required.8. Dispense with agitation.Quality Control SpecificationsDehydrated Appearance: Powder is homogeneous, free flowing and grey-black.Prepared Appearance: Prepared medium is opaque and black.PI 7728, Rev 1, February 2011PI7728, Rev 1, February 2011Expected Cultural Response: Cultural response on BCYE Agar at 35 ± 2︒C and examined for growth and fluorescence under long-wave UV light at 66 – 72 hours incubation.Test ProcedureCulture the organism immediately upon arrival to the laboratory. Culture specimens from swabs by rolling the swab over a third of the agar surface. Streak remainder of the plate to obtain isolated colonies. Incubate inoculated plates at 35 ± 2︒C for a minimum of 3 days. Growth is usually visible within 3 - 4 days, but can take up to 2 weeks.ResultsLegionella pneumophila produces small to large, smooth, colorless to pale, blue-grey, slightly mucoid colonies that fluoresce yellow-green under longwave UV light. A gram stain, biochemical tests, and serological procedures should be performed for confirmation of L. pneumophila .StorageStore sealed bottle containing the dehydrated medium at 2 - 30°C. Once opened and recapped, place container in a low humidity environment at the same storage temperature. Protect from moisture and light by keeping container tightly closed.ExpirationRefer to expiration date stamped on the container. The dehydrated medium should be discarded if it is not free flowing, or if appearance has changed from the original color. Expiry applies to medium in its intact container when stored as directed.Limitations of the Procedure1. Due to nutritional variation, some strains may be encountered that grow poorly or fail to grow on thismedium.2. Biochemical tests and serological procedures must be performed to confirm presence of L. pneumophila .Packaging BCYE Agar Code No.7728A 500 g 7728B 2 kg7728C 10 kgReferences1. McDade, Shepard, Fraser, Tsai, Redus, Dowdle and the Laboratory Investigation Team. 1977. N. Engl. J. Med. 297:1197.2. Edelstein. 1985. In Lennette, Balows, Hausler and Shadomy (eds.). Manual of clinical microbiology, 4th ed. ASM. Washington, D.C.3. Freely, Gorman, Weaver, Mackel and Smith. 1978. J. Clin. Microbiol. 8:320.4. Freely, Gibson, Gorman, Lansford, Rasheed, Mackel and Baine. 1979. J. Clin. Microbiol. 10:437.5. Pasculle, Freely, Gibson, Cordes, Myerowitz, Patton, Gorman, Carmack, Ezzell and Dowling. 1980. J. Infect. Dis. 141:727.6.Edelstein. 1981. J. Clin. Microbiol. 14:298.Technical InformationContact Acumedia Manufacturers, Inc. for Technical Service or questions involving dehydrated culture media preparation or performance at (517)372-9200 or fax us at (517)372-2006.。

GC-2014C Clarity培训教材

11
岛津 GC-2014C 气相色谱仪（Clarity 工作站）培训教材
Clarity 工作站基本操作
1.1 程序开始
岛津 Clarity 工作站的主要优点之一是可以不需要长时间的准备和设置即可立刻进行测定。 • 点击桌面上的图标或通过选择开始 – 所有程序 – ClarityShimadzu –
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岛津 GC-2014C 气相色谱仪（Clarity 工作站）培训教材
单次分析对话框在进样针将样品输入 GC 进样口后，点击 GC 控制面板上的“Start”按钮以启动分析。
当运行时，当前测定时间和运行标记会在岛津 Clarity 工作站窗口下方状态栏中显示。
1.5 分析监控
运行标记及运行时间
2 双流路 FID（流量控制器）
3 毛细管柱 TCD 下面以填充柱单 FID 为例介绍。
4 毛细管柱单检测器（用于单 FID、ECD、FPD、FTD）
5
岛津 GC-2014C 气相色谱仪（Clarity 工作站）培训教材
单填充柱，单 FID 检测器操作步骤
1、检查色谱柱、进样垫、衬管是否装好 2、开载气：开钢瓶总阀，减压阀压力设为 0.7Mpa（0.6~0.8Mpa） 3、开电源：开 GC-2014C 主机电源，开 CBM-102 电源，开电脑，双击桌面 CS-LIGHT Real Time Analysis 实时分析工作站 4、调节载气一次稳压用压力（primary）500Kpa 和二次稳压用压力 DINJ 左侧（carrier L） /二次稳压用压力 DINJ 右侧（carrier R）（一般情况下不用调）
ClarityShimadzu 色谱工作站命令启动程序。

ISO25000 SoftWare Quality Measurement

page 6
Carnegie Mellon Software Engineering Institute
SQuaRE: Architecture
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All Ballots closing Mid-April to Early May
Editors assigned but no drafts out 25010, Quality Model 25023, External Quality Measures

ZEISS Axioscope 物料实验室 upright light 微观显微镜说明书

ZEISS AxioscopeYour Microscope for Research and Routine in the Materials LabProduct Information Version 1.0The Axioscope upright light microscope was designed specifically to meet the most common optical imaging requirements of materials laboratories.Coded and automation features make it particularly well suited to routine tasks that place high demands on data quality and reproducibility. But Axioscope doesn’t stop there. It is also capable of handling advanced optical microscopy for materials science studies.Axioscope is a turnkey solution for metallography and materials science in research and industry – with functions for determining grain size, phases and layer thickness as well as for the classification of graphite particles. Analyze your samples with established contrast techniques. Advanced light management ensures that your samples are always optimally illuminated.With its versatility to handle many daily tasks, Axioscope has a good chance of becoming the preferred instrument of your laboratory staff.Ready to serve both Research and Routine Investigations› In Brief › The Advantages › The Applications › The System› Technology and Details › ServiceSimpler. More Intelligent. More Integrated.Affordable High PerformanceEveryday life in the materials laboratory is charac-terized by both routine tasks and challenging detailed investigations. While microscopes for routine applications quickly reach their limits when high performance imaging and enhanced contrast techniques are required, high-priced research microscopes offer a range of perfor-mance that is rarely fully exploited. Axioscope – with its outstanding usability and advanced auto-mation features – is ideal for demanding routine tasks. And, even at its attractive price, it also offers powerful capabilities commonly associated with more advanced research light microscopes.Digital IntegrationOne of the best reasons to select ZEISS is theircomprehensive integration platform that allowsdata from all ZEISS microscopes to be connected.Combine Axioscope with the ZEISS Axiocamcamera portfolio and ZEISS ZEN 2 core imagingsoftware, and Axioscope now becomes a powerfuldigital documentation system. From device control– to image capture, analysis and documentation –to archiving your valuable analytics, Axioscopedelivers a fully digitized workflow. In addition,Axioscope can be integrated into correlativeworkflows via Shuttle & Find.Reliable ResultsWith coded components and advanced lightmanagement, Axioscope delivers trustworthy,reproducible results. The motorized Axioscope 7gives you the ability to fully automate investigativeworkflows. Perform repetitive tasks with presetparameters, automatically navigate to regions ofinterest on the sample, or capture images withextended depth of field. Axioscope packs a lot ofpower and reliability into its small footprint, so itis quick to become the lab favorite.Axioscope in a connected laboratory environmentMultiphase analysis with ZEISS ZEN 2 coreAxioscope for polarization› In Brief› The Advantages› The Applications› The System› Technology and Details › ServiceMeet Routine Microscopy Demands—without Compromise to Advanced Inspection NeedsZEISS is well known for their expertise in developing light microscope solutions. The Axioscope product familytakes a well-defined position in the ZEISS materials lab solution portfolio: Axioscope is the right choice ifyour routine inspection tasks place high demands on usability, reproducibility and automation – and you alsoneed advanced optical microscopy for materials analysis and metallography. Being a complete materiallaboratory solution, Axioscope is also the first choice from an economic point of view.ZEISS PrimotechCompact manual microscope for material and geoscience educationZEISS AxioscopeEncoded and motorized microscope for highlyproductive materials research and routineZEISS Axio ImagerHigh-end microscope system for advancedmaterials researchZEISS Axio Lab.A1Manual routine microscope for thematerials laboratory with ergonomicoperation› In Brief› The Advantages› The Applications› The System› Technology and Details › ServiceA Turnkey Metallography SolutionAxioscope is performance-ready, with all features working in concert to deliver a complete metallography solution for the materials laboratory: cameras as the most important interface for digitizing your sample data, lenses with application-specific properties, and an imaging software specially developed for materials research and metallography.ZEN 2 core: Imaging Software with Integrated Materials ModulesZEN 2 core is your command center for automated imaging and analysis functions. Modules for the deter-mination of grain sizes, phases and layer thicknesses, as well as for the classification of graphite particles, enable ZEN 2 core to provide all meaningful metallographic applications under a uniform user interface.ZEISS objective lensesSelect the objectives that fit your application, imaging perfor-mance or cost requirements and imaging performance.ZEISS Axiocam camerasChoose from a wide range of microscope cameras to get the resolution, color fidelity and processing speed you need.Cast iron analysis with ZEISS ZEN 2 core50 µm› In Brief› The Advantages › The Applications › The System› Technology and Details › ServiceEasy to Use for Powerful Workflow EfficienciesErgonomic Operating ConceptAxioscope is designed to make everyday opera-tions as comfortable and safe as possible. Impor-tant controls – like focus drive, stage drive, light manager and image capture – are arranged on both sides such that they can be operated without overworking either hand.Axioscope controlsEasy Image AcquisitionUsing the snap button, digital image acquisition is easy. Simply press this ergonomically located button, and you can acquire images while main-taining control over position, magnification or contrast. In this way, the microscopic examination can be fully documented, while you always keep the sample in view.Perfect Control of All Stage AxesThe innovative operating concept of Axioscope 7, the motorized product version, gives you full control over all stage movement, without having to take your hands off the microscope or relying on external controllers. With the simple press of a button, you can switch the focus drives between Z-axis control and XY stage control. With the XY control activated, you can move the stage along the X axis with the right focus drive and along the Y axis with the left focus drive.Axioscope 5: Snap button for image acquisition on both sides Axioscope 7: Snap button (right) and stage control button (left)› In Brief› The Advantages › The Applications › The System› Technology and Details › ServiceCoded Components Assure Reliable and Reproducible ResultsFull Confidence in Your DataThe coded components of the microscope not only make your work easier and more comfortable, but also ensure that erroneous operation and the associated falsification of the examination results can be largely ruled out.Modern Light ManagementThe system detects changes to objectives or contrast techniques, then adjusts dependent parameters – such as light intensity and scaling – automatically. This allows multi-faceted routine workflows to be processed more quickly and easily. Using process parameters that you or others have stored, anyone can reproduce an exact workflow at any time and achieve comparable results, independent of individual users’ operating habits or preferences.Light manager controlAutomatic adjustment of the light intensity after changing the objective (upper right)Automatic adjustment of the light intensity after changing theobjective and contrasting technique (upper right)10× (Brightfield)50× (Brightfield)50× (Darkfield)100 µm 20 µm› In Brief› The Advantages › The Applications › The System› Technology and Details › ServiceMotorization Facilitates AutomationMotorization of the X, Y and Z axesAxioscope 7, the motorized model in the Axioscope product family, enables you to automate much of your work process. Benefit from higher productivity, repeatable processes based on predefined parameters, and better comparability of results. Full motorization of the X, Y, and Z motion axes opens many opportunities for advanced imaging:Extended Depth of Field:• Automatically acquire multiple images at different focus positions (Z-stack) and combine them to create an image with enhanced depth of field.Panorama Images:• Create composite images of larger sample areas in just a few clicks.Tiles & Positions:• Record exact, highly resolved images of multiple field of views by automatically scanning predefined areas.Correlative Microscopy:• Examine samples with different light and electron microscopes. Relocate regions of interest automatically using the Shuttle & Find module of ZEN 2 core.Metal bump, imaged with Extended Depth of FieldTiles & Positions: Overview image of a cam with predefined area(left);. Acquired image of the predefined area (right)› In Brief› The Advantages › The Applications › The System› Technology and Details › ServiceConnect and CorrelateThe Connected LaboratoryZEN 2 core helps you to make your laboratory even more productive. With workflow solutions that connect data from different microscopes, ZEN 2 core delivers more meaningful information. And thanks to its archive and database connectivity features, you keep your valuable data together across instruments, laboratories, and locations.Shuttle & FindShuttle & Find is the ZEISS correlative microscopy interface, designed specifically for use in materials analysis and industrial QA.Shuttle & Find allows you to:• Transfer samples between ZEISS light and electron microscope systems faster than ever • Relocate regions of interest automatically • Improve efficiency and throughput • Collect the maximum relevant information • Make well informed material decisionsConnected laboratory environment with Axioscope (1), ZEISS EVO electron microscope (2) and Smartzoom 5 digital microscope (3). In a multi-modal workflow, the sample to be examined is passed on from microscope to microscope (4). ZEN 2 core (5) ensures consistent data exchange between all involved devices, off-line analysis workstations (6), and remote laboratories (7).› In Brief› The Advantages › The Applications › The System› Technology and Details › ServiceZEISS Axioscope at Work: Contrast TechniquesVersatile Options: The Contrast TechniquesA multitude of contrast options have been implemented in the Axioscope in order to meet the special requirements of materials microscopy. Such variety of reflected- and transmitted-light techniques is unusual in this performance class.Brightfield – contrast method to identify size and shape of different phases Darkfield – contrast method to enhance the visibility of phase boundariesC-DIC (Circular Differential Interference Contrast) – relief-like appearance of the surface shows structures like scratches Polarization Contrast – the colors are connected with chrystallo-graphic orientation of the different phases100 µm Reflected light:• Brightfield• Darkfield• Polarization• DIC• C-DIC• FluorescenceTransmitted light:• Brightfield• Polarization• Darkfield• DIC• PlasDIC• Phase contrast› In Brief› The Advantages› The Applications› The System› Technology and Details › ServiceZEISS Axioscope at Work: MetallographyTypical tasks and applications• Imaging and analysis of microstructure of metal materials• Quantitative microstructure analysis• Evaluation according to international standards • Grain size analysis • Multiphase analysisGet these benefits from ZEISS Axioscope • Reveal microstructural information using different contrast methods.• Use brightfield contrast to get information about the overall number, size and shape of features within a material.• Enhance grain boundaries and particle edges with darkfield contrast to reveal sharper fea-tures and clearer definition of interfaces. • With Circular Differential Interference Contrast(C-DIC) your sample surface appears as a 3D relief. You can easily detect polishing marks. • Encoded components assure¬ that you always get the right light intensity and scaling to provide reproducible results.Cast Iron Analysis – Size and Shape Distribution› In Brief › The Advantages › The Applications › The System› Technology and Details › ServiceZEISS Axioscope at Work: MetallographyGrain Size Analysis – Planimetric Method Grains Size Analysis – Intercept Method Porosity Analysis with Multi-Phase ModuleComparative Diagrams – sample comparison with wall charts Cast Iron Analysis – Segmentation of graphite particlesLayer Thickness Measurement› In Brief › The Advantages › The Applications › The System› Technology and Details › ServiceAxioscope 5Manual microscope with coded components for reproducible and reliable results in the analysis ofmaterial cuts, thin sections, and fracture surfacesThe ZEISS Axioscope FamilyZEISS Axioscope 5ZEISS Axioscope 5 for Polarization ZEISS Axioscope 7The Axioscope product family offers instrument variants for routine tasks and advanced research applications. Each configuration has been optimized for specificapplications with all relevant contrast techniques available to support your microscopic inquiry. Attention to ergonomics assures that all users benefit from comfortableand easy operation.Axioscope 5 for PolarizationManual microscope with coded componentsfor reproducible and reliable results in typicalapplications for polarization microscopy: geology,mineralogy and metallographyAxioscope 7Microscope with coded and motorized compo-nents for material microscopy tasks that requireadvanced imaging capabilities and workflowautomation› In Brief› The Advantages› The Applications› The System› Technology and Details› ServiceThe ZEISS Axioscope FamilyAxioscope VarioThe most flexible material microscope in the Axioscope family, Axioscope Vario is the ideal solution for more unusual specimens. Axioscope Vario is designed for reflected-light and fluores-cence applications, with extended specimen space that accommodates large objects up to 380 mm. An important operating advantage is the crank device at the top of the stand’s column. This crank allows users to continuously adjust the vertical position of the microscope body by hand, without need for special tools. The metal base plate further reduces vibration to provide the stability required for all materials investigations.ZEISS Axioscope Vario› In Brief › The Advantages › The Applications › The System› Technology and Details › ServiceMicroscope • Axioscope 5• Axioscope 5 for Polarization • Axioscope 7 • Axioscope Vario Objectives • EC-EPIPLAN• EC-Epiplan-NEOFLUAR • EC-Epiplan-APOCHROMATYour Flexible Choice of ComponentsIllumination • LED 10W• HAL 100W (Halogen)Cameras • Axiocam 105• Axiocam 305 • Axiocam 503• Axiocam 506• Axiocam 512Software • ZEN 2 core •Matscope› In Brief › The Advantages › The Applications › The System› Technology and Details › ServiceSystem Overview› In Brief› The Advantages› The Applications› The System› Technology and Details› ServiceSystem Overview› In Brief› The Advantages› The Applications› The System› Technology and Details› ServiceProduct Dimensions: Axioscope› In Brief› The Advantages› The Applications› The System› Technology and Details› ServiceTechnical Specifications› The Advantages› The Applications› The System› Technology and Details› ServiceTechnical Specifications› The Advantages› The Applications› The System› Technology and Details› ServiceTechnical Specifications› The Advantages› The Applications› The System› Technology and Details› Service>> /microserviceBecause the ZEISS microscope system is one of your most important tools, we make sure it is always ready to perform. What’s more, we’ll see to it that you are employing all the options that get the best from your microscope. You can choose from a range of service products, each delivered by highly qualified ZEISS specialists who will support you long beyond the purchase of your system. Our aim is to enable you to experience those special moments that inspire your work.Repair. Maintain. Optimize.Attain maximum uptime with your microscope. A ZEISS Protect Service Agreement lets you budget for operating costs, all the while reducing costly downtime and achieving the best results through the improved performance of your system. Choose from service agreements designed to give you a range of options and control levels. We’ll work with you to select the service program that addresses your system needs and usage requirements, in line with your organization’s standard practices.Our service on-demand also brings you distinct advantages. ZEISS service staff will analyze issues at hand and resolve them – whether using remote maintenance software or working on site. Enhance Your Microscope System.Your ZEISS microscope system is designed for a variety of updates: open interfaces allow you to maintain a high technological level at all times. As a result you’ll work more efficiently now, while extending the productive lifetime of your microscope as new update possibilities come on stream.Profit from the optimized performance of your microscope system with services from ZEISS – now and for years to come.Count on Service in the True Sense of the Word› In Brief › The Advantages › The Applications › The System› Technology and Details › ServiceN o t f o r t h e r a p e u t i c , t r e a t m e n t o r m e d i c a l d i a g n o s t i c e v i d e n c e . N o t a l l p r o d u c t s a r e a v a i l a b l e i n e v e r y c o u n t r y . C o n t a c t y o u r l o c a l Z E I S S r e p r e s e n t a t i v e f o r m o r e i n f o r m a t i o n .E N _42_011_255 | C Z 04-2018 | D e s i g n , s c o p e o f d e l i v e r y , a n d t e c h n i c a l p r o g r e s s s u b j e c t t o c h a n g e w i t h o u t n o t i c e . | © C a r l Z e i s s M i c r o s c o p y G m b HCarl Zeiss Microscopy GmbH 07745 Jena, Germany ********************/axioscopemat。

科纳斯自动进样瓶和附件说明书

3Cronus ® Vials are manufactured to conformto a strict range of criteria and set newstandards for quality and reproducibility ®With Cronus ®Vials you will achieveconsistent and reliable results,time after time...Save MoneySave the EnvironmentTake Advantage with Cronus ® Advantage PacksCronus ® Advantage Packs consist of a box of 5,000 vials and pre-assembled caps and septa – this saves on unnecessary packaging and saves you money!Crimp Cap Vial Advantage Packs page 4Snap/Crimp Cap Vial Advantage Packs page 79mm Screw Cap Vial Advantage Packs page 10®3Septa Selection Guide24Vial Cross Reference Chart25Autosampler & Vial Compatibility Guide 26Product Index30Crimp Cap Vials4Snap/Crimp Cap Vials68mm Screw Cap Vials89mm Screw Cap Vials1010mm Screw Cap Vials (Wide Mouth)1212x32mm VialsOther VialsMicrotiter Plates and Seals23Plates & Seals Limited Volume Inserts22MicrosamplingMicrosampling Vials2015x45mm Vials14Headspace Vials16Sample Storage Vials18Volatile Organic Analysis (VOA) Vials15Shell Vials19Vial Racks and Tainers194Crimp Cap Vials, 12x32mmPart No.Description QuantityVZS-02CC-100100 PackVZS-02CA-100100 PackVZM-15CCC-100Champagne Vial, 1.5ml, Clear Glass100 PackVZM-15CAC-100Champagne Vial, 1.5ml, Amber Glass100 PackVZM-15CBC-95Champagne Vial, 1.5ml, Black Glass95 PackVZM-03CCF-100X-Vial, 350μl Fused Insert, Clear Glass100 PackVZM-03CAF-100X-Vial, 350μl Fused Insert, Amber Glass100 PackVZP-02CCF-100X-Vial Precision, 250μl Precision FusedInsert, Clear Glass100 PackVZP-02CAF-100X-Vial Precision, 250μl Precision FusedInsert, Amber Glass100 PackVZM-15CCC-100VZM-15CAC-100VZM-15CBC-95VZM-03CCF-100VZM-03CAF-100VZP-02CCF-100VZP-02CAF-100VZS-02CC-100VZS-02CA-10011mm Assembled Crimp Caps and SeptaPart No.Description QuantityVCA-1103CS-100Silver PTFE/Red Rubber Septa100 PackVCA-1104CS-100Silver PTFE/Silicone Septa100 PackVCA-1104MS-100Silver magnetic sealPTFE/Silicone Septa100 PackVCA-1105CS-100Silver PTFE/Sil/PTFE Septa100 PackVCA-1106CS-100Silver Pre-slit PTFE/Sil Septa100 Packmagnetic crimp capsVCA-1105CS-100VCA-1104CS-100/VCA-1104MS-100VCA-1106CS-100VCA-1103CS-100Why Choose Crimp Cap Vials?Crimp Cap Combo and Advantage PacksPart No.Description QuantityVKS-0203-CCS-100Clear Glass, 1.8ml + Crimp Cap,PTFE/Red Rubber Septum100 PackVKS-0203-CAS-100Amber Glass, 1.8ml +Crimp Cap,PTFE/Red Rubber Septum100 PackVKB-0203-CCS-5000Clear Glass, 1.8ml + Crimp Cap,PTFE/Red Rubber Septum5000 PackVKB-0203-CAS-5000Amber Glass 1.8ml + Crimp Cap, PTFE/Red Rubber Septum5000 PackVKS-0203-CCS-100VKB-0203-CCS-5000Under-crimpedOver-crimpedCorrect Vial CrimpingAchieve accurate results with correctly crimped vials.Correctly Crimped Vial®Electronic Vial Crimpers and Decappers Description5Inserts for Crimp Cap VialsVIN-0202C-100VIN-0103C-100VIS-0302C-100Crimpers & DecrimpersPart No.Description311950-xx*VTC-11VTD-11Why Choose Snap/Crimp Cap Vials?6Snap/Crimp Cap Vials, 12x32mmPart No.Description QuantityVZS-02SC-100100 PackVZS-02SA-100100 PackVZM-15SCC-100100 PackVZM-15SAC-100100 PackVZM-15SBC-9595 PackVZM-03SCF-100100 PackVZM-03SAF-100100 PackVZP-02SCF-100X-Vial Precision, 250μl Precision Fused Insert,Clear Glass100 PackVZP-02SAF-100X-Vial Precision, 250μl Precision Fused Insert,Amber Glass100 PackVZM-01SPV-100Microsampling Vial, 250μl, Conical Bottom,Polypropylene100 PackVZM-05SPV-100Microsampling Vial, 300μl, Conical Bottom,Polypropylene100 PackVZM-15SPX-100MaxVial, 750μl, Polypropylene100 PackVZM-07STX-100MaxVial, 750μl, TPX (clear plastic)100 PackVZS-02SA-100VZS-02SC-100VZM-15SCC-100VZM-15SAC-100VZM-15SBC-95VZM-03SCF-100VZM-03SAF-100VZP-02SCF-100VZP-02SAF-100 VZM-01SPV-100VZM-05SPV-100VZM-15SPX-100VZM-07STX-100Inserts for Snap/Crimp Cap VialsVIS-0302C-100VIN-0202C-100VIN-0103C-10011mm Assembled Snap Caps and Septa®7Snap Cap Combo PacksQuantityVKS-0204-SCR-100Snap Cap Advantage PacksQuantity VKB-0203-SCR-50005000 Pack VKB-0204-SCB-50005000 Pack VKB-0204-SCR-50005000 Pack VKB-0204-SAR-50005000 Pack VKB-0205-SCB-50005000 Pack VKB-0205-SCR-50005000 Pack VKB-0206-SCR-50005000 Pack VKB-0208-SCR-50005000 PackVKB-0204-SCR-5000VCA-1106SR-100VCA-1108SR-100VCA-1104SR-100VCA-1103SR-100VCA-1102SN-1000VCA-1104SB-100VCA-1105SB-100VCA-1105SR-1008mm Screw Cap Vials, 12x32mmPart No.DescriptionQuantityPolypropylenePolypropyleneVZM-0108PV-100VZM-0508PV-100VZM-1508CC-100VZM-1508AC-100VZS-0208C-100VZS-0208A-100 Why Choose 8mm Screw Cap Vials?8Septa for 8-425 Screw Thread CapsPart No.Description QuantityVCS-0808-1000VCS-0804-1000VCS-0806-1000 8mm Assembled Caps and SeptaPart No.Description QuantityVCA-0804TB-100VCA-0806TB-100VCA-0804TY-100 Caps for 8-425 Screw Thread VialsPart No.Description Quantity100 PackVCC-0801TB-1000VCA-0802TN-1000VCA-0832TB-100VCA-0801TY-1000®9 Sealing Screw CapsIt is important not to over-tighten screw caps.●●●●Over-Tightened Screw CapInserts for 8-425 Screw Thread VialsVIN-0201C-100VIS-0301C-100VIS-0201P-100VIN-0102C-10008mm Screw Cap Combo PacksVKS-0204-08CB-100Why Choose 9mm Screw Cap Vials?9mm screw thread vials have a 9-425 GPI thread and the closure is dimensionally equivalent to 11mm crimp cap vials.This means that they can be used in any autosampler that uses 11mm crimp cap vials (see page 4 for crimp cap vials).9mm screw caps have an advantage over 11mm crimp caps because 9mm screw caps can easily be applied and removedby hand and they can be reused.9mm Screw Cap Vials, 12x32mmPart No.Description Quantity109mm Screw Cap Combo PacksPart No.Description QuantityVKS-0205-09CB-100VKS-0204-09AB-1009mm Screw Cap Advantage PacksPart No.Description QuantityVKB-0203-09CB-50005000 PackVKB-0204-09CB-50005000 PackVKB-0204-09AB-50005000 PackVKB-0204-09CLK-5000Clear Glass 1.8ml + Blue KNURLED Screw Cap, PTFE/Silicone Septum5000 PackVKB-0205-09CB-50005000 PackVKB-0206-09CL-50005000 Pack®11Don’t over-tighten your screw caps!VIS-0201P-100VIN-0102C-1000VIN-0202C-100Inserts for 9-425 Screw Thread VialsVIS-0302C-1009mm Bonded Caps and SeptaVCB-0906TL-100VCB-0904TL-1009mm Assembled Caps and SeptaVCA-0903TL-100VCA-0904TY-100VCA-0904TG-100VCA-0906TL-100VCA-0903TG-100VCA-0904TR-100VCA-0904TB-100VCA-0906TB-100VCA-0903TB-100VCA-0904TLK-100VCA-0903TY-100VCA-0905TL-100VCA-0903TR-100VCA-0905TB-100VCA-0904TL-100VCA-0931TL-1001210mm Assembled Caps and SeptaPart No.Description QuantityVCA-1006TB-100VCA-1004TB-10010mm Screw Cap Vials, 12x32mmPart No.DescriptionQuantityVZM-0210PT-100VZM-1510CC-100VZM-1510AC-100VZM-0310AF-100VZM-0310CF-100VZS-0210A-100VZS-0210C-100Why Choose 10mm Screw Cap Vials?10mm (10-425) screw cap vials feature a wider opening than other screw top vials. This increased target area makes sample preparation easier . It also reduces the chances of bent or broken needles during sampling.Septa for 10mm Screw Thread CapsVCS-1006-1000VCS-1004-1000VCS-1008-1000®13Don’t over-tighten your screw caps!Inserts for 10-425 Screw Thread VialsVIS-0302C-100VIN-0103C-100VIN-0202C-100Caps for 10mm Screw Thread Vial sVCC-1001TB-1000VCA-1031TB-100VCA-1002TN-100VCA-1031TW-100VCS-1308-1000VCS-1304-1000Septa for 13-425 Screw Thread CapsPart No.Description QuantityWhy Choose 15x45mm Screw Cap Vials?15x45mm vials have a 13-425 GPI thread and can hold up to 4ml of sample. They are used by the Waters 48-position autosampler and many others – see the Autosampler & Vial Compatibility Guide on pages 26-29.1413-425 Assembled Caps and SeptaPart No.Description QuantityVCA-1304TB-100VCA-1306TB-10013-425 Screw Thread Vials, 15x45mmPart No.DescriptionQuantityVZS-0415A-100VZS-0415C-100VZM-3515CC-100VZM-3515AC-10015x45mm Champagne Vialsffering a 3.5ml capacity with adead volume of just 20μl ,15x45mm Champagne Vials can be used with both large and small samples . They offer an ideal alternative to limited volume inserts!800μl 20μl3.5mlNo support required1.5ml Champagne VialsCaps for 13-425 Screw Thread VialsPart No.Description QuantityVCA-1331TW-100VCA-1332TB-100VCA-1332TB-100VCC-1307TB-1000VCA-1302TN-1000VCC-1301TB-1000VCA-1331TW-100Septa for VOA CapsPart No.DescriptionQuantityVCS-2405-100VCS-2405-1000VCS-2405-100/VCS-2405-10009VZG-4024C-100VOA Screw Cap VialsPart No.DescriptionQuantityVZG-4024C-100VZG-4024A-100VZG-4024A-100Why Choose VOA Vials?VOA vials are specifically designed for use with volatile organic compounds, as recommended by EPA CFR Part 136 and under EPA 40 CFR 141. They are available in both clear and amber borosilicate glass and have a temperature range of -40°C to 125°C.Screw Caps for VOA VialsPart No.Description QuantityVCC-2401TB-100Black, Open top VCC-2401TB-1000Black, Open top VCC-2401TW-100White, Open topVCC-2401TB-100/VCC-2401TB-1000VCC-2401TW-10015VOA Screw Cap Combo PacksPart No.Description QuantityVKV-4004-24ABL-100VKV-4004-24CBL-100100 PackVKV-4004-24CBLVKV-4004-24CWL-100Headspace VialsPart No.DescriptionQuantityVZH-10CF-100VZH-10CR-100VZH-20CF-100VZH-20CR-10016Why Choose Headspace Vials?20mm Assembled Crimp Caps and SeptaPart No.Description Quantity Magnetic Crimp CapsVCA-2004MG-100VCA-2004PS-100VCA-2004BM-100VCA-2004MS-100VCA-2004CS-100VCA-2003CS-100Under-crimpedOver-crimpedCorrect Vial CrimpingAchieve accurate results with correctly crimped vials.Correctly Crimped Vial®Electronic Vial Crimpers and DecappersDescription320950-xx*1720mm Caps for Headspace Vials500 Pack Crimpers & DecrimpersDescriptionVTC-20VTD-20Heavy Duty Bench-top Vial Crimper for 11mm or 20mm caps20mm Septa and Stoppers for Headspace Caps1000 CaseVCC-2002CS-1000VCC-2002BM-500VCS-2004-1000VCS-2002GE-100018Sample Storage VialsVZG-0413C-100VZG-0815C-200VZG-0815A-200VZG-1215C-200VZG-1215A-200VZG-1618C-200VZG-1618A-200VZG-2220C-200VZG-4024C-100VZG-4024A-100VZG-0815C-200VZG-0413C-100VZG-0815A-200VZG-4024A-100VZG-4024C-100VZG-1618C-200VZG-1215C-200VZG-2220C-200VZG-1215A-200VZG-1618A-200Screw Caps for Storage VialsPart No.Description QuantityVCA-1331TW-100VCA-1332TB-100VCA-1531TW-100VCA-1532TB-100VCA-1831TW-100VCA-2031TW-100VCA-2431TW-100VCA-2031TW-100VCA-2431TW-100VCA-1831TW-100VCA-1532TB-144VCA-1531TW-100VCA-1332TB-100VCA-1331TW-100Shell VialsVKL-0103-GCC-2508x40mm, 1ml, Clear Glass (with closures)VKL-0202-GCC-10012x32mm, 2ml, Clear Glass (with closures)VKL-0402-GCC-10015x45mm, 4ml, Clear Glass (with closures)VKL-0103-GCC-250VKL-0402-GCC-100VKL-0202-GCC-100Assembled 15-425 Caps and SeptaVCA-1504TB-100VCA-1506TB-100VCA-1504TB-100VCA-1506TB-100®19 Vial RacksVTRW4815-115mm Vials, 48 Position, White Polypropylene12mm Vials, 50 Position, White PolypropyleneVial TainersVTBM-512x32mm Vials, 100 Position, Mixed Colours12x32mm Vials, 100 Position, NeutralVTBN-1VTBM-5VTRW5012-120Champagne Vials Champagne Vialsdon’t need inserts or supports and yet still handle small volumes ! These vials provide aneconomical and ﬂ exible solution – offering a 1.5ml capacity with a dead volume of just 15μl, Champagne Vials can be used with both large and small samples .The black opaque Champagne Vials are ideal for use with light-sensitive samples where the sample may react or degrade even when using amber glass.Part No.Closure Glass QuantityVZM-15CCC-100VZM-15CAC-100VZM-15CBC-95VZM-15SCC-100VZM-15SAC-100VZM-15SBC-95VZM-15CCC-100VZM-15SCC-100VZM-15SAC-100VZM-15SBC-95VZM-15CAC-100VZM-15CBC-95VZM-1508CC-100VZM-1509CC-100VZM-1510CC-100VZM-1510AC-100VZM-1509AC-100VZM-1509BC-95VZM-1508AC-100LARGE VOLUME 3.5ml Champagne VialsWhy Choose Microsampling Vials?Champagne Vials , X-Vials and X-Vial Precision are alternatives to limited volume inserts. They provide limited volumes without the need for separate inserts! All Cronus ® microsampling vials are 12x32mm in size and so will work with most autosamplers.150μl 15μl1.5mlNo supportrequired®VZM-03CCF-100VZM-03CAF-100VZM-03SCF-100VZM-03SAF-100VZM-0309CF-100VZM-0309AF-100VZM-0310AF-100VZM-0310CF-100are ideal for small samples with a nominalvolume of less than 300μl. They have a conical-tubular insertpermanently fused inside a standard 12x32mm autosampler vial.This makes the X-Vials very robust and guarantees correctvertical alignment – eliminating the possibility of needlebreakage. X-Vials cost less than the price of using a separatevial with an insert!VZM-03CCF-100VZM-03CAF-100VZM-03SCF-100VZM-03SAF-100X-Vial Precision contain a precision drawn insertwith a dead volume of just 5μl — ideal if you require totalsample recovery or your autosampler uses a side port needle.What’s more, the closure is an integral part of the insert thuseliminating any chance of sample evaporation.With all X-Vials the base level of the insert is the same as a normal12x32mm vial so you can use X-Vials without having to adjustyour autosampler.Part No.Closure Glass QuantityVZP-02CCF-100VZP-02CAF-100VZP-02SCF-100VZP-02SAF-100VZP-02CCF-100VZP-02CAF-100VZP-02SCF-100VZP-02SAF-10030μl5μl250μlPermanentlyﬁ xed & directlyclosed insert50μl10μl300μlPermanentlyﬁ xed insertPart No.DescriptionProﬁle VolumeDeadVolumeQuantityCrimp &Snap/Crimp8mmScrew9mmScrew10mmScrewWhy Choose Limited Volume Inserts?Selecting the correct insertSolventCompatibilityTargeted DeadVolumePriceInsert Proﬁ lesVIN-0201C-100VIS-0301C-100VIN-0202C-100VIN-0103C-100VIS-0302C-100VIS-0201P-100VIN-0102C-1000®MP096-1121MP384-1121MP096-1211Polypropylene Microtiter PlatesIdeal for:MP096-1111120μl Square100 Pack240μl SquareMicroplate Cap MatsBeneﬁ ts include:Part No.WellsWellShapeStyle Pre-Slit QuantityxxMM096-3351MM096-3041SEPTA SELECTION GUIDEOptimise performance and results by choosing the right septum for your application: PTFE●●●●●PTFE/Silicone●●●●Pre-slit PTFE/Silicone●●●PTFE/Silicone/PTFE●●●●PTFE/Red Rubber●●●●●Moulded Polypropylene●●●®PageVZM-1510AC-100®Continued overleaf...®8x40mmOrdering and Product InformationChromatography Consumables The Cronus ® range of products doesn’t stop at Vials and Caps, there are also extensive ranges of Syringe Filters and HPLC Columns:®Syringe FiltersCronus ® Syringe Filtersare available in a variety of sizes and they feature colour coding to provide easy identiﬁ cation, membrane size and porosity printed on every ﬁ lter , and membranes (including Nylon, PTFE, Regenerated Cellulose, Cellulose Acetate, PVDF , PES and Glass Fibre) to suit all types of sample.Cronus ® Sterile Syringe Filters are available with the popular Polyethersulphone (PES) and Cellulose Acetate (CA) membranes. Each ﬁlterisindividually packed and sterilised usingethylene oxide (EtO)./cronusﬁlters®HPLC ColumnsThe Cronus ® HPLC columns feature popular packing materials.The materials include L iChrosorb, L iChrospher, Partisil, Nucleosil,Superspher and also Spherisorb and Hypersil equivalent packing. Thecolumn hardware is of excellent quality and the pricing offers goodvalue for money./cronuscolumns®Your Local Distributor:SMI-LabHut LtdThe GranaryThe SteadingsMaisemoreGloucestershireGL2 8EYUKTel: +44 (0)1452 310210Fax: +44 (0)1452 300075Email: ****************Website: SMI-LabHut Ltd。

2014 Zeon Chemical Product Guide in Chinese

2
NIPOL® 丁腈橡胶 (NBR) 被推荐用于需耐油和耐溶剂的部件。为了确保在各种工作环境下的优良性能，瑞翁提供不同丙烯腈含量的多种 Nipol 丁腈橡胶。其耐燃油，耐油，和耐溶剂性能随聚合物中丙烯腈含量的增加而提高。低温柔性和弹性随聚合物中丁二烯含量增加而改进。不同品牌的 Nipol 丁腈橡胶可共混，加工成不同硬度和性能各异的制品.瑞翁提供的丁腈橡胶有粉末状，颗粒状，液体胶，和普通板块状，用于各种不同的应用中，尤其是需耐油，耐热及耐化学溶剂的环境。Nipol 丁腈橡胶特别适合于做热塑性和热固性塑料的改性剂。它们也用作涂料和胶粘剂的添加剂.
3
TABLE OF CONTENTS
Nipol® 丁腈橡胶 ………........................................................................ Pages 5-6 Nipol® 羧基丁腈橡胶 …………………............................................................ Page 6 Nipol® 三元共聚丁腈橡胶.................................................................................. Page 7 Nipol® 液态丁腈橡胶 ……………..................................................................... Page 7 Nipol® 粉末和颗粒丁腈橡胶 .............................................................................. Page 7 Zealloy® 热塑型塑料改性剂 ........................................................................... Page 8 DuoMod® 增韧剂 ............................................................................................ Page 8 Nipol® 共混聚合物和丁腈油聚橡胶 .................................................................. Page 8 Zetpol® 氢化丁腈橡胶 .................................................................................... Page 9 Zetpol® HP HNBR 高性能的氢化丁腈橡胶 ....................................................... Page 10

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Structure & reaction search of unstructured data (Word, PPT, Excel, OneNote, Chemical files, pdf, image files, etc.) Enable chemistry intelligence and biologics informatics in Microsoft SharePoint

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Scilligence Inventory
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Company Founded in 2010 Partner with Microsoft Life Science Team Core Values
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Scilligence PMF
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Small molecule and biologics research informatics Strong structure and sequence search capabilities Cross-platform, Zero-footprint (Windows, Mac, mobile platforms)
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Name-to-structure (e.g., Trade/IUPAC name, CAS#, Smiles) and structure-to-name Single & multi-step reactions, combi-chem, process optimization Compound registration easily integrated (e.g., RegMOL) Powerful structure, biosequence and keyword search Structurally searchable SAR table
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Flexible architecture to support all biology experiments Support biologics (peptides, genes, proteins, DNA/RNA, ADCs)
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RegMOL
Registration for Small Molecules & Biologics

Web-based and cross-platform: Windows, Mac, iPad/iPhone, Android, Linux… Register and manage samples
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Enable cheminformatics and bioinformatics in Office Interface with back-end databases Intuitive and efficient tools to analyze SAR and large datasets