Real time thermal propagtors for massive gauge bosons
法国SETARAM公司一直是全球顶级热分析及量热仪的制造

法国SETARAM公司一直是全球顶级热分析及量热仪的制造商,隶属于空中客车尖端配套商之一的法国KEP集团。
并于2006年设立法国塞塔拉姆仪器公司上海代表处。
长期以来都是空客集团SNECMA及法国原子能机构CEA的指定热分析技术及量热技术合作伙伴。
公司位于热分析和量热仪技术的发源地-法国,拥有世界上最著名的高温热分析及量热专家,是世界上第一个采用钨合金炉体制造1600°C综合热分析厂商(1965), 凭借50多年的技术传承和世界顶级用户的互动,塞塔拉姆公司在高温和超高温热分析领域以其独特的Eyraud光电天平技术、卡尔维三维量热技术及模块化设计一直处于行业领先地位。
塞塔拉姆产品在制药、生物、食品、石油和天然气、核能、过程安全和先进材料等领域正起着日益重要的作用。
可用于测试腐蚀、氧化、降解及混合反应和研究纳米材料、金属、陶瓷和合金的老化特性。
在生物制药、过程安全和能源开发研究领域,我们的系统广泛应用于多晶态、晶状体球蛋白、溶度测定、预测逃生时间、动力学研究、燃气水合物和钻井泥浆等研究过程。
塞塔拉姆通过非破坏性分析还开发出了表征核能废料的独特解决方案。
而2008年收购美国HY-Energy技术公司,也预示着储氢材料研究领域的全面涉足。
塞塔拉姆仪器公司在全球的主要市场(美国、法国、德国、意大利、瑞士和英国)都有直接销售渠道。
为满足用户的需要,2006年底在中国上海成立代表处,2008底建立技术中心及应用实验室,对销售人员的培训,技术支持和现场服务也一应俱全,同时拟通过该平台更好地向国内用户提供产品、培训应用方面的信息及支持。
热重分析仪(TGA) 测量物质的重量变化(在受控气氛内温度变化条件下)。
所有塞塔拉姆天平都满足最高的精确度和稳定性标准。
由热重分析仪(TGA) 所测的性质包括腐蚀,高温分解,吸附/解吸附,溶剂的损耗,氧化/还原反应,水合/脱水,分解,炭黑等高性能模块TGA热分析仪(室温/ 2400°C)SETSYS Evolution TGA具有单独加热炉和最宽广的温度范围(室温/ 2400°C)模块性: DTA, DSC, TGA, TMA 不同组合能在同一基本结构上互换。
梅特勒-托利多新型动态热机械分析仪DMA1及新一代热重分析仪TGA1隆重上市

梅特勒-托利多新型动态热机械分析仪DMA1及新一代热重
分析仪TGA1隆重上市
梅特勒
【期刊名称】《上海计量测试》
【年(卷),期】2012(000)006
【总页数】1页(P58-58)
【作者】梅特勒
【作者单位】托利多公司
【正文语种】中文
【相关文献】
1.梅特勒-托利多超越系列熔点仪全新上市——熔点仪新概念:自动测理与视频记录同步 [J],
2.梅特勒-托利多超越系列熔点仪全新上市——熔点仪新概念:自动测量与视频记录同步 [J],
3.2012梅特勒-托利多新型动态热机械分析仪DMA1及新一代热重分析仪TGA1隆重上市! [J],
4.梅特勒-托利多全新一代FiveEasy Plus^(TM)系列台式仪表于2012年3月隆重上市! [J],
5.梅特勒-托利多全新一代FiveEasy Plus^(TM)系列台式仪表于2012年3月隆重上市! [J],
因版权原因,仅展示原文概要,查看原文内容请购买。
聚苯乙烯ps质量法熔融指仪

聚苯乙烯ps质量法熔融指仪
聚苯乙烯PS质量法熔融指仪
聚苯乙烯PS质量法熔融指仪是一种采用聚苯乙烯PS的质量法来测定熔融指仪的仪器。
它由一个可控制聚苯乙烯PS温度的采样腔、一个用于安装聚苯乙烯PS的熔融测试仪和一个用于熔点测试的测温探头组成。
它的工作原理是:当聚苯乙烯PS温度上升时,它会在一定温度下熔化,即该聚苯乙烯PS的熔点。
在改变聚苯乙烯PS温度的同时,可以测量出该聚苯乙烯PS的熔点,从而确定该聚苯乙烯PS的质量。
聚苯乙烯PS质量法熔融指仪在实验室使用时常常与其他仪器结合起来,用于测量熔点、收缩率、晶向、光谱和拉伸强度等性能参数。
它可以用来评估聚苯乙烯PS的品质,并且可以帮助检测制造商是否达到质量标准,以及在产品开发和生产过程中起到质量控制的作用。
聚苯乙烯PS质量法熔融指仪的优点在于它可以快速准确的测量出聚苯乙烯PS的熔点,这样就可以准确判断其质量,而它的精度更高,更能满足客户的要求。
同时,由于它可以高温操作,因此它对于处理聚苯乙烯PS的耐候性、热稳定性和可持续性的测定也有极大的帮助。
- 1 -。
alsic电子封装材料热导率以及散热特性

AlSiC介绍 ALSIC微电子封装材料是西安明科微电子材料有限公司与西北工业大学合作开发的新一代电子产品。
明科公司(Xi'an Miqam Microelectronics Materials Co., Ltd)是目前国内唯一一家可以生产这种材料的企业。
铝碳化硅(AlSiC)金属基热管理复合材料,是电子元器件专用电子封装材料,主要是指将铝与高体积分数的碳化硅复合成为低密度、高导热率和低膨胀系数的电子封装材料,以解决电子电路的热失效问题。
AlSiC的性能特点■ AlSiC具有高导热率(170~200W/mK)和可调的热膨胀系数(6.5~9.5×10-6/K),因此一方面AlSiC的热膨胀系数与半导体芯片和陶瓷基片实现良好的匹配,能够防止疲劳失效的产生,甚至可以将功率芯片直接安装到AlSiC基板上;另一方面AlSiC的热导率是可伐合金的十倍,芯片产生的热量可以及时散发。
这样,整个元器件的可靠性和稳定性大大提高。
■ AlSiC是复合材料,其热膨胀系数等性能可通过改变其组成而加以调整,因此电子产品可按用户的具体要求而灵活地设计,能够真正地做到量体裁衣,这是传统的金属材料或陶瓷材料无法作到的。
■ AlSiC的密度与铝相当,比铜和Kovar轻得多,还不到Cu/W 的五分之一,特别适合于便携式器件、航空航天和其他对重量敏感领域的应用。
■ AlSiC的比刚度(刚度除以密度)是所有电子材料中最高的:是铝的3倍,是W-Cu和Kovar的5倍,是铜的25倍,另外AlSiC的抗震性比陶瓷好,因此是恶劣环境(震动较大,如航天、汽车等领域)下的首选材料。
■ AlSiC可以大批量加工,但加工的工艺取决于碳化硅的含量,可以用电火花、金刚石、激光等加工。
■ AlSiC 可以镀镍、金、锡等,表面也可以进行阳极氧化处理。
■ 金属化的陶瓷基片可以钎焊到镀好的AlSiC基板上,用粘结剂、树脂可以将印制电路板芯与AlSiC粘合。
TA Instruments产品介绍说明书

THERMAL ANALYSISDifferential Scanning Calorimetry (DSC) Q2000 4Q20 6DSC Technology 8Accessories 10Temperature Control Options 14Tzero ® & MDSC ®Technology 18Thermomechanical Analysis (TMA)Q400EM/Q400 98 Q400 Technology 100Modes of Deformation 102TMA Theory/Modes of Operation 104Applications 108Dynamic Mechanical Analysis (DMA) Deformation Modes & Sample Size 80Subambient Operation 81Q800 Technology 82Modes of Deformation 84Accessories 86DMA Theory 90Modes of Operation 91Vapor Sorption AnalysisVTI-SA + 58VTI-SA + Technology 60Q5000 SA 64Q5000 SA Technology 66Applications 72Simultaneous DSC/TGAQ600 50SDT Technology 52Applications 54Thermogravimetric Analysis (TGA)Q500 32Q50 34Q500/Q50 Technology 36TGA Accessories & Options 38Applications 44AnAlysis5958Vti-Sa + sPECiFiCATiOns Maximum Sample Weight 750 mg/5 gDynamic Range 100 mg/500 mg Weighing Accuracy +/- 0.1% Weighing Precision +/- 0.01% Sensitivity 0.1 µg/0.5 µg Signal Resolution 0.01 µg/0.05 µg Temperature Control Peltier Elements, Resistance Heaters Experimental Temperature Range 5 to 150°C Isothermal Stability +/- 0.1°C Relative Humidity Control Range See Figure Below Accuracy +/- 1% RH Humidity Control Closed Loop, Dew Point Analyzer Organic Solvent Capability Optional Camera/2.5x Microscope Accessory Optional Raman Probe Accessory Optional The VTI-SA + Vapor Sorption Analyzer is a continuous vapor flow sorption instrument for obtaining precision water and organic vapor isotherms at temperatures ranging from 5°C to 150°C at ambient pressure. The VTI-SA + combines the features of VTI’s original SGA design with almost two decades of field-proven performance: the isothermal aluminum block construction, the three isolated thermal zones and chilled-mirror dew point analyzer for primary humidity measurements with the field-proven TA Instruments thermobalance technology… all to provide precise and accurate gravimetric measurements with excellent temperature and RH stability.Temperature (˚C)R e l a t i v e H u m i d i t y (%R H )*Performance may vary slightly, depending on laboratory conditions6160Symmetrical Microbalance DesignResolution and Stability of the MicrobalancePrecision Humidity MeasurementsAs part of our standard design, the VTI-SA + employs a chilled mirror dew point analyzer (a NIST-traceable standard for humidity) to determine the absolute relative humidity at the sample. In applications where RH control is critical (as in most pharmaceutical studies), chilled-mirror dew point analyzers are the preferred method, because of the absence of drift and long term stability.Sorption Testing Using an Organic VaporThe VTI-SA + can also be configured for organic vapor sorption. In the VTI-SA +, the concentration of the organic vapor in the gas stream reaching the sample is determined by the fraction of gas going through the organic solvent evaporator and the fraction of dry gas.In competitive systems, assumptions are made that the evaporator is 100% efficient and that the temperature of the evaporator is constant from low to high concentrations. The VTI-SA + system measures the temperature of the organic solvent in the evaporator and uses this information together with the Wagner equation to control the organic vapor concentration in the gas phase. This method solves the issue of adiabatic cooling of the solvent, a major source of error in competitive systems.The solvent containers/evaporators are easily removed and exchanged so there is no need for decontamination or cleaning of the system when changing organic solvents or reverting to water sorption experiments. For safety, the evaporator compartment is purged with dry nitrogen and fitted with a combustible gas sensor with an audible alarm that, when triggered, shuts down the power to the analyzer.Simultaneous Microscope Camera or Raman Measurement Sample Chamber Design62Temperature Controlled Thermobalance Included Dynamic Range 100 mg Weighing Accuracy +/- 0.1% Weighing Precision +/- 0.01% Sensitivity < 0.1 µg Baseline Drift* < 5 µg Signal Resolution 0.01 µg Temperature Control Peltier Elements Temperature Range 5 to 85°C Isothermal Stability +/- 0.1°C Relative Humidity Control Range 0 to 98% RH Accuracy +/- 1% RH Autosampler – 10 samples** Included Platinum™ Software Included Sample PansQuartz or Metal-Coated Quartz 180 µLPlatinum 50, 100 µL Aluminum Sealed Pan 20 µL The patented Q5000 SA delivers the performanceand reliability required in a leading sorption analyzerin a compact, user-friendly design. The Q5000SA is designed for manual or automated sorptionanalysis of materials under controlled conditions oftemperature and relative humidity (RH ). Its designintegrates our latest high-sensitivity, temperature-controlled thermobalance with an innovative humiditygeneration system, multi-position autosampler,and powerful Advantage™ software with technique-specific programs and Platinum™ features. Q5000 SAsPECiFiCATiOns 65* Over 24 hours at 25˚C and 20 % RH with empty metal coated quartz pans ** Optional tray accommodates 25 samples for use with platinum and sealed aluminum pansHumidity Control Chamber67MFC N 2Thermobalance Autosampler Sample Crucibles6871Vapor Sorption analysis is an established technique for determining the effect on materials of exposure to controlled conditions of temperature and humidity. Isotherm and Isohume™ experiments are the most commonly performed analyses.All TA Instruments sorption analyzers perform a range of essential sorption experiments such as time-courses, isotherms (constant temperature, variable RH), and isohumidity (Isohume™) experiments (constant RH, variable temperature). Complex protocols with step changes in temperature and RH can be defined and saved for later use. Also, multiple experiments can be run sequentially without further operator assistance.In isothermal experiments, a weighed sample is “dried” externally, or preferably in the instrument, and exposed to a series of humidity step changes at constant temperature. The sample is staged at each humidity level until no further weight change is detected or a set time has elapsed. A data point is recorded, the humidity is changed in 5 or 10% controlled RH steps, and the process repeated in an increasing or decreasing procedure. Isohume experiments involve a series of temperature step changes at constant humidity and result in similar plots. They are used to determine how sample exposure to a given humidity results in a physiochemical change, such as a change in the sample’s hydration state. The curve shape provides useful information to this end.TA Instruments analysis software offers Sorption Analysis, BET Analysis, and GAB programs. In addition, the full power and flexibility of our renowned Universal Analysis software provides for easy data manipulation, advanced reporting, plotting, and file exporting capabilities. In addition, advanced data reduction of VTI-SA+ data can be performed using custom-designed data analysis packages. Analysis options include:• Kinetic analysis for the determination of rate constant of adsorption • Isosteric heat of adsorption using the Clausius-Clapeyron equation• Surface area calculation using the BET equation for either water or organic vaporsGraVimetric Vapor Sorption analySiS General practice73Hydrate FormationThe figure to the right contains the experimental results demonstrating the formation of a hydrate. The hydrate formation is characterized by a plateau in the desorption branch of the isotherm. In this example the hydrate is formed at around 45% RH. The sample adsorbs about 4.5% by weight water and does not lose the water of hydration until the RH is lowered below 25%. This hydrate would be considered as a labile or unstable hydrate.Characterization of Morphological StabilityExposure to elevated humidity can initiate morphological changes in some pharmaceutical materials, particularly in amorphous sugars. As the humidity is increased, the adsorbed water plasticizes the material and lowers the glass transition. When the glass transition temperature decreases to the experimental temperature, crystallization will typically occur. The data in the figure below show the behavior of amorphous lactose at 25°C under a constant increase in humidity. Note how the character in the measured weight signal is indicative of a variety of morphological changes including the glass transition and subsequent crystallization of the amorphous phase.72Evaluation of Amorphous StructurePharmaceutical scientists are often interested in determining the amount of amorphous material in a drug formulation. As the amorphous and crystalline forms are chemically identical, classical analysis techniques are often insensitive to amorphous content. The figure below shows the moisture sorption analysis of a generic drug in its amorphous and crystalline forms. As the amorphous form absorbs significantly more water, the Q5000 SA can be used to quantify relative amorphous content in drug mixtures.Analyzing Small Amounts of PharmaceuticalsWhen evaluating pharmaceuticals it is common for only small amounts of material to be available for conducting multiple analytical tests. Hence, the ability to work with small samples is critical. The low baseline drift of the Q5000 SA means that good results can be obtained on even 10-20 milligrams of a crystalline drug, such as prednisone, which adsorbs <0.1% moisture over a broad humidity range. The sorption results shown below represent about 15 micrograms of weight change full-scale. The reversibility (lack of hysteresis) in the sorption/desorption profile for prednisone (as well as the low level of moisture adsorbed) indicates that the moisture picked up by the material is adsorbed on the surface of the materialrather than being absorbed into its structure.5.00.01.02.03.04.0-1.0W e i g h t (% c h a n g e )Relative Humidity (%)W e i g h t (%)Relative Humidity (%)W e i g h t C h a n g e(%)0.000.080.060.040.02Relative Humidity (%)W e i g h t C h a n g e (%)75Packaging Film AnalysisIn addition to evaluation of the actual pharmaceutical formulations, sorption analysis can also be valuable in comparing the polymeric films which are being considered for packaging the drugs and other materials. The figure to the right shows comparative profiles for two different packaging materials undergoing temperature and relative humidity cycling. Film A adsorbs and desorbs moisture at a more rapid rate than the other film evaluated which suggests it may not be suitable for packaging moisture sensitive compounds.Rate of DiffusionThe VTI-SA + can be equipped with a diffusion cell which allows for the direct measurement of the permeability of a film or membrane for a particular solvent vapor. The cell consists of a cavity that is filled either with a desiccant or absorber, a gasketed lid for attaching the film to be tested, and a wire stirrup to hang the assembled cell on the hang-down wire of the balance. Any vapor permeating through the film gets absorbed immediately and the weight of the cell will increase until steady-state conditions are reached. The normalized rate of permeation is obtained from the slope of this line (weight per unit time) and the diameter of the permeating film.74Organic Vapor Sorption (VTI-SA +)With the organic vapor sorption capability, the VTI-SA +can obtain not only water sorption isotherms, but can also be used to measure organic vapor isotherms. The use of organic vapor increases the sensitivity of the sorption measurement for many pharmaceutical and polymer materials, and provides information on the specificity of solvent adsorption for many materials. In the first figure, the time course data for the adsorption of ethanol on activated carbon is shown. The sample is initially dried at 0% RH , then the relative pressure of the ethanol is stepped in 0.10 increments.This second figure shows the sorption isotherm plot for the carbon/ethanol experiment, excluding the initial drying step. The sample exhibits a significant adsorption at low solvent concentrations. This is typical of the particle and internal pore-size distribution of activated carbon which is designed to allow for rapid gas-phase adsorption with low pressure drop.7LPH PLQ:H L J K W-2108801006040200642TimeW e i g h t C h a n g e (%)R e l a t i v eH u m i d i t y (%)Rel Pressure (req)W e i g h t C h a n g e (%)35-5-515250600400200800Temperature (˚C)W e i g h t C h a n g e (%)R e l P r e s s (r e q )0.001.00.200.400.600.80001。
质谱 加热块英文

质谱加热块英文Mass Spectrometry and Heating Block: Revolutionizing Analytical TechniquesMass spectrometry is a powerful analytical technique that has revolutionized the field of scientific research. This technology, combined with the use of a heating block, has become an indispensable tool in various industries, from chemistry and biology to environmental science and forensics. In this comprehensive essay, we will explore the principles, applications, and advancements of mass spectrometry and its integration with heating block technology.At the heart of mass spectrometry lies the ability to separate and identify the components of a given sample based on their mass-to-charge ratio. This process involves the ionization of the sample, the separation of the ions based on their mass-to-charge ratio, and the detection of these ions by a specialized detector. The resulting mass spectrum provides a wealth of information about the chemical composition and structure of the analyte, allowing researchers to gain valuable insights into a wide range of scientific phenomena.One of the key components in mass spectrometry is the heatingblock, which plays a crucial role in the sample preparation and ionization processes. The heating block is a device that heats the sample to a specific temperature, facilitating the vaporization and ionization of the analyte. This step is particularly important for the analysis of thermally labile or high-molecular-weight compounds, as the heating block ensures the efficient conversion of the sample into a gas-phase form, which is essential for the subsequent mass spectrometric analysis.The integration of mass spectrometry and heating block technology has led to significant advancements in various fields of study. In the pharmaceutical industry, for example, mass spectrometry coupled with heating block analysis has become an indispensable tool for the characterization and quality control of drug compounds. By precisely controlling the temperature of the sample, researchers can accurately identify and quantify the active ingredients, impurities, and degradation products in drug formulations, ensuring the safety and efficacy of the final product.Similarly, in the field of environmental analysis, mass spectrometry and heating block technology have played a crucial role in the detection and quantification of pollutants, such as pesticides, heavy metals, and organic compounds, in air, water, and soil samples. The ability to vaporize and ionize these compounds using the heating block allows for their efficient separation and identification by themass spectrometer, enabling researchers to monitor environmental contamination and develop effective remediation strategies.In the realm of forensic science, mass spectrometry coupled with heating block analysis has become an invaluable tool for the identification and characterization of a wide range of evidence, including illicit drugs, explosives, and trace evidence. The heating block's ability to vaporize and ionize these complex samples, combined with the high sensitivity and selectivity of mass spectrometry, has revolutionized the way forensic investigators approach the analysis of evidence, leading to more accurate and reliable results.Beyond these traditional applications, the integration of mass spectrometry and heating block technology has also found its way into the field of biological research. Researchers have utilized this powerful combination to study the structure and function of proteins, lipids, and other biomolecules, providing insights into the underlying mechanisms of biological processes and the development of new therapeutic strategies.As technology continues to evolve, the capabilities of mass spectrometry and heating block instrumentation have also experienced significant advancements. The development of more sensitive and selective mass analyzers, coupled with the introductionof advanced ionization techniques and improved sample handling methods, has led to enhanced analytical performance and the ability to tackle increasingly complex analytical challenges.Moreover, the integration of mass spectrometry and heating block technology with other analytical techniques, such as chromatography and spectroscopy, has further expanded the scope of applications and the depth of information that can be obtained from a single analysis. This synergistic approach has enabled researchers to gain a more comprehensive understanding of the samples under investigation, leading to more accurate and reliable results.In conclusion, the integration of mass spectrometry and heating block technology has revolutionized the field of analytical science, providing researchers with a powerful tool for the identification, characterization, and quantification of a wide range of analytes. From the pharmaceutical industry to environmental monitoring and forensic investigations, this powerful combination has become an indispensable part of the scientific landscape, driving advancements and enabling groundbreaking discoveries across various disciplines. As technology continues to evolve, the future of mass spectrometry and heating block analysis promises even more exciting developments and applications that will shape the course of scientific research and discovery.。
顶尖科技 TT-N-851 恒温器使用说明书

Thermostat Quick Reference Thermostat Operation Thermostat OptionsContact Us and Warranty Registration2345Congratulations on purchasing a new thermostat. This thermostat was designed to the highest reliability and ease of use standards. Thank you for choosing TopTech.® U.S. Registered Trademark. Patents pending.Copyright © 2010 Pro1 IAQ, Inc. All rights reserved.Rev. 1026Table of ContentsPage1Need Help?For assistance with this productplease visit or call TopTech Customer Care toll-free at 888-776-1427 during normal business hours (Mon-Fri 9 AM - 6 PM Eastern).Una versión española de este manual puede ser descargadaen Battery information2On the back of the thermostat insert 2 AA Alkaline batteries (included).Pull the thermostat directly away from the wall to access the batteries. A firm tug will be required to remove the thermostat from the subbase mounted on the wall.Getting to know your thermostat2Fan Button 3System Button 4Button Access Door5Temperature Setpoint Buttons6Light Button (Glow in the dark)612345LCD1+1 will appear in the display when second stage of heat or cool is on. +2 will appear for third stage of heat.System operationindicators: The COOL, HEAT or FAN icon will display when the COOL, HEAT or FAN is on.NOTE: The compressor delay feature is active if these icons are flashing. The compressor will not turn on until the 5 minute delay has elapsed.Replace batteries when this indicator is shown.Indicates the current Displays the user selectable setpoint Use the “+” or “-” keys to select your desired room temperature. A copy of the OperatingManual can be downloaded at FanSystem3Easy to use controlsLCD Display:See page 2 for details about this display read out and icons.12345Glow in the Dark Light Button:The glow in the dark light button will self illuminate for several hours after exposure to ambient light. This button turns on the display light when pressed.Temperature Setpoint Buttons:Press the + or - buttons to select the desired room temperature.Fan Key:Select ON or AUTO . The ON key will run the fan continuously. The AUTO key will cycle the fan on only when the heating or cooling system is on.System Key:Selects the operation mode of your HVAC system. Selecting HEAT turns on the heat mode. Selecting COOL turns on the air conditioning mode. Selecting OFF turns both heating and cooling off. Selecting AUTO will turn the HEAT or COOL on as needed. (EM Heat will appear as an option if operating a heat pump. EM Heat setting will turn on Emergency Heat)12345A Note About Auto Changeover: Auto changeover will switch between heating and cooling as needed. It is very important to make sure the coolingsetpoint temperature is at least 3º above the heating setpoint temperature and that the heating setpoint temperature is at least 3º below the cooling setpoint temperature.Use the “+” or “-” keys to select your desired room temperature. A copy of the OperatingManual can be downloaded at FanSystemFilter Change ReminderIf your installing contractor has configured the thermostat to remind you when the air filter needs changed, you will see FILT in the display when your air filter needs changed. FILT will be shown in the display after your system has run long enough to require an air filter change.Resetting the filter change reminder:When FILT reminder is displayed, you should change your air filter and reset the reminder by holding down the FAN button for 3 seconds.4to reset filter reminder.5Name: ____________________________Address: ________________________________________________________City: ____________________________State: ____________________________Zip:_____________________Thermostat Model: _____________________Date Installed:_____________________Contact Us InformationTopTech Warranty Registration:TopTech by Pro11111 S. Glenstone Suite 2-100Spring eld, MO 65804Toll-free: 1-888-776-1427Toll Number (Outside the USA): 330-821-3600Web: Hours of Operation: Monday - Friday 9 AM - 6 PM EasternComplete form and mail to:TopTech by Pro11111 S. Glenstone Suite 2-100Spring eld, MO 65804。
激光导热分析仪LFA427

激光导热分析仪LFA 427简介:对于材料或组分的热传导性能描述,导热系数与热扩散系数是最为重要的热物性参数。
激光闪射法是导热测试领域最为广泛使用的一种方法,用于精确测量材料的热扩散系数并计算导热系数。
而耐驰公司推出的激光导热仪 LFA 427 则代表了世界范围内同类产品的最高水平。
LFA 427 具有高精度、高重复性、测量快速、样品支架种类丰富、测试气氛可自由设定等突出优点,其总的测量温度范围为 -120℃-2800℃。
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仪器直接测试的是随温度而变的热扩散系数,若结合比热值(通常使用DSC 404 F1 Pegasus®进行测试,也可在 LFA 427 上使用比较法测得)与密度(密度随温度的变化使用热膨胀仪 DIL 402 C 测量计算),则可进一步计算导热系数。
测量所使用的激光能量、脉冲宽度、气氛与真空均可自由选择,可以针对不同的样品性质设定最佳的测量条件。
本仪器拥有完全密封的系统,设计上注重节省空间,其安全等级达到了最高级(1级),操作时不需要任何特殊的安全措施。
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LFA 427 是最强大与灵活的 LFA 系统,适用于包括汽车制造、航空航天与能源技术在内的各种领域的常规材料与新型高性能材料的表征。
LFA 427 - 技术参数•温度范围:-120—400℃, RT ... 1300℃, RT ... 1500℃, RT ... 2000℃/2800℃(四种可选的炉体类型)•升降温速率:0.01-50 K/min(取决于相应炉体)•激光能量:20 J/pulse(功率与脉冲宽度可调)•使用红外检测器,进行非接触式的样品表面温升信号测试•热扩散系数范围:0.01-1000 mm2/s•导热系数范围:0.1—2000 W/m*K•样品直径:6—12.7 mm(另可选 20 mm 特殊规格)•样品厚度:0.1—6 mm•样品支架:氧化铝,石墨•熔融金属容器:蓝宝石•液体样品容器:铂金•气氛:惰性,氧化,还原,静态,动态•高真空密闭系统,真空度 10-5mbar用于片状固体样品测试的标准样品支架LFA 427 - 软件功能LFA 427 的测量与分析软件是基于MicroSoft Windows® 系统的Proteus® 软件包,它包含了所有必要的测量功能和数据分析功能。
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a r X i v :h e p -p h /9307229v 3 31 J a n 1994Imperial/TP/92-93/4312th January,1994hep-ph/9307229Real Time Thermal Propagators for Massive Gauge BosonsT.S.Evans ∗&A.C.Pearson †Blackett Laboratory,Imperial College,Prince Consort Road,London SW72BZ U.K.AbstractWe derive Feynman rules for gauge theories exhibiting spontaneous symmetry break-ing using the real-time formalism of finite temperature field theory.We also derive the thermal propagators where only the physical degrees of freedom are given thermal bound-ary conditions.We analyse the abelian Higgs model and find that these new propagators simplify the calculation of the thermal contribution to the self energy.1IntroductionSince the observation by Kirzhnits and Linde [1]that spontaneously broken symmetries may be restored at high temperatures,the subject has attracted wide attention.However,very little study has been made of theories containing spontaneous symmetry breaking at non-zero temperature using the so-called real time formalisms.This seems odd since in this formalism,dynamical quantities are more readily calculated as the thermal Green functions are given directly in terms of real times .We are only aware of one paper,by Ueda[2],that uses the real time formalism to study the abelian Higgs model at non-zero temperature.However,this work was done prior to the further development of real time methods by Niemi &Semenoff[3]and others.We therefore feel that a study of spontaneously broken gauge symmetries using the real time formalism is necessary.In this paper we begin by deriving the real time thermal propagator for a massive gauge boson in the covariant gauges.We find that there are two thermal contributions to the propagator.The first part is consistent with the interpretation of a field in a heat bath of real particles.However the second term acts as a counterterm to the finite temperature contributions from the unphysical goldstone modes.We then apply the the ideas of Landshoff&Rebhan[4]and only apply the thermal boundary conditions to the physical degrees of freedom.Previously,this method has only been applied to gauge theories where the full symmetry is maintained.In the final section ,we use the abelian Higgs model as a simple example.We analyse thecalculation ofthe one-loop corrections to the mass of the Higgs boson performed by Ueda[2].While we do not disagree with the the results therein,there were a number of mistakes in the form of the propagators used.We evaluate the propagators correctly.We also show that if we use propagators for which only the physical modes are thermalised,the calculation is greatly simplified.2Derivation of RTF PropagatorTo begin with let us consider a set of gauge fields A µa invariant under some gauge group.After symmetry breaking ,the free field lagrangian for these fields is of the form;L 0=−12M 2ab A µa A µb +1ζ−1)∂µ∂ν∆νρ(t −t ′)=g µρδC (t −t ′)(2)subject to the KMS condition[6].The subscript C denotes that we are considering the solutionto this equation along the contour in the complex time plane associated with the real time formalism[3,7,8,9](see fig.1).6ℑm (t )−ı1M 2A ( x ,t ;M 2)−A ( x ,t ;ζM 2)(3)where A ( x ,t ;M 2)=d 3¯keı k. xıexp(βω)−1(e −ıωt +e −βωe ıωt )Θ(t )+(e ıωt +e −βωe −ıωt )Θ(−t )is the solution of (2+M 2)A ( x ,t −t ′;M 2)=δC (t −t ′),ω2= k 2+M 2and∂Θ(t −t ′)M 2B∆(k )00−∆∗(k )B−k µk νk 2−M 2+ıε,Γ(k )=1e β|k 0|−1Consider the 1-1component of this propagator which is interpreted as the propagator betweenthe physical fields.Explicitly the 1-1component isı∆µν11(k )=−ık 2−ζM 2+ıε−g µν−k µk νe β|k 0|−1−k µk νe β|k 0|−1(6)It can be seen that the propgator splits into the T =0and T >0contributions.in the limitas T →0(β→∞)the T >0terms disappear and ∆µν11reduces to the zero temperature propagator.We note that there are two finite temperature contributions to the form of this propagator.The first term containing ‘δ(k 2−M 2)’may be interpreted as a contribution due to a heat bath of real particles of mass M .However,the second term contains the unphysical gauge parameter ζand its interpretation is not so straightforward.The second term acts as a counterterm to the unphysical contributions from the goldstone boson.This can be shown in two ways.Firstly,let us consider this model in the unitary gauge.In this gauge,the goldstone boson is gauged away and so we would expect there to be no counterterms in the photon propagator.The unitary gauge propagator satisfies the following equation.(2+M 2)gµν−∂µ∂ν∆νρ(t −t ′)=g µρδC (t −t ′)(7)Evaluating this equation we find∆µν(k )=−gµν−k µk νM 2B∆(k )00−∆∗(k )B−k µk νk 2−M 2+ıεgµν−(1−ζ)k µk νM 22πδ(k 2−M 2)∂M 2M 2=0(10)In momentum space this becomes,∆µν(k )=−g µν−k µk ν∂k 2+ıε.This is exactly the propagator for a photon first derived by Kobes,Semenoff,and Weiss in [5].3The abelian Higgs modelThe propagator we have derived for the massive gauge boson differs from the result used by Ueda (Eqn.3.8,[2]).However this work was done prior to the formulation of real time thermal field theory[7]using path integral methods devloped by Niemi &Semenoff[3].We would therefore like to reconsider the abelian Higgs model.The abelian Higgs model consists of a U (1)gauge field coupled to a complex scalar field described by the Lagrangian densityL =−16(Φ∗Φ)2where F µν=∂µA ν∂νA µand D µ=∂µ−ıeA µ.We choose ρ2<0so that spontaneous symmetry breaking occurs.Expanding Φabout its expectation value as Φ(x )=1√2,we may rewrite the lagrangian as L =L 0−V (A µ,φ,χ)where L 0=−12M 2A µA µ−12∂µφ∂µφ−12∂µχ∂µχ−M∂µχA µ(12)and V (A µ,φ,χ)is a potential term containing only cubic and quartic terms.M =ev and m 2=ρ2+1k 2−m 2+ıε+2πδ(k 2−m 2)k 2+ıε+2πδ(k 2)k 2−M 2+ıεgµν−(1−ζ)k µk νM 22πδ(k 2−M 2)M 22πδ(k 2−ζM 2)∂k 2ıe β|k 0|−1ı∆µνmod (k )=−ıe β|k 0|−1ζk µk νk 2−k µk νe β|k 0|−1+ıζk µk ν∂k 2+ıε+2πδ(k 2)k 2.As it was pointed out by Kobes,Semenoff&Weiss[5],these terms should instead be considered as derivatives of the delta function.As we find that the modified propagator used by Ueda is essentially correct,it is no surprisethat we agree with the result of the one-loop self energy corrections calculated in[2]and we shall not repeat the calculation here.However,we would like to consider this calculation using propagators for which only the physical degrees of freedom are given thermal boundary conditions[4].Using these propagators the modified propagators due to photon-goldstone mixing areı∆µν(k)=− ıeβ|k0|−1 gµν−kµkνk2+ıεζkµkνmodk2 ıReferences[1]D.A.Kirzhnits and A.D.Linde,Phys.Lett.42B(1972)472[2]Y.Ueda,Phys.Rev.D23(1981)1383[3]A.J.Niemi and G.W.Semenoff,Ann.Phys.(NY)152(1984)305;Nucl.Phys.B230(1984)181[4]ndshoff,A.Rebhan,Nucl.Phys.B383(1992)607.[5]R.L.Kobes,G.W.Semenoff,and N.Weiss,Z.Phys.C29(1985)371[6]R.Kubo,J.Phys.Soc.Japan12,(1957)570;P.C.Martin and J.Schwinger,Phys.Rev.115,(1959)1342[7]ndsman and Ch.G.van Weert,Phys.Rep.145(1987)141.;R.J.Rivers,Path In-tegral Methods in Quantum Field.Theory(Cambridge University Press,Cambridge, 1987);[8]A.C.Pearson,Why the real time formalism does not factorise,talk given at the3rdWorkshop on Thermal Field Theories and their applications in Physics,August1993, Banff,Canada;[9]T.S.Evans,A new time contour for thermalfield theories,Why the real time formalismdoes not factorise,talk given at the3rd Workshop on Thermal Field Theories and their applications in Physics,August1993,Banff,Canada.[10]P.Arnold,E.Braaten and S.Vokos,Phys.Rev.D46(1992)3576;P.F.Kelly,talk givenat the3rd Workshop on thermalfield theories and their applications in physics,August 1993,Banff,Canada[11]K.Takahashi,Z.Phys.C-Particles and Fields26601(1985)。